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Search results for: PAL WIERCONY
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Partial PLA composite surface activation by femtosecond laser ablation
Open Research DataThe dataset contains the studies on electrochemical activity of PLA composite (commercially available CB-PLA Protopasta), which was 3D printed in a form of 1x1cm electrodes. The electrodes were submitted to femtosecond laser ablation, etching a certain % of the electrochemically-exposed electrode size. The % value is in the name of each file. The goal...
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Partial PLA composite surface activation by femtosecond laser ablation
Open Research DataThe dataset contains the studies on electrochemical activity of PLA composite (commercially available CB-PLA Protopasta), which was 3D printed in a form of 1x1cm electrodes. The electrodes were submitted to femtosecond laser ablation operating with different parameters. These were: gas atmosphere (He or air, data in different subfolders), the percentage...
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The effect of wax foundation addition to PCL filaments on mechanical properties.
Open Research DataThe dataset includes the effect of wax foundation addition on the basic mechanical properties of the filaments. PCL and wax foundation addition at 10 and 15% were used for extrusion. The mechanical properties of the resulting filaments were evaluated by a double compression test using an Instron model 5543 universal testing machine. Parameters such...
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The electrochemical studies of CB-PLA surface activation by electrolysis in 1M NaOH
Open Research DataThe dataset contains the electrochemical studies performed under different conditions of surface activation of the CB-PLA 3D printed electrodes. The activation was performed by electrolysis in 1M NaOH solution under cycling polarization with different anodic or cathodic overpotentials (data in different subfolders). The file names contain the exact...
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Terrestrial Laser Scan and Survey Images - 3D Model - Palm House - MP1 - Leica
Open Research DataDataset description: Raw images from photogrammetric and terresttial laser scaning survey. Object: Palm House in Gdansk Oliwa ParkLocation: Gdansk, Pomorskie, PolandDrone type: DJI Mavic Pro 1Flight plan: Circle | Point Of InterestTarget Product: 3D ModelDate: 06.11.2018Direct georeferencing: yesMetadata data: Yes/GPSGCP: NoCamera Name: DJI FC220Lasser...
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Determination of changes in viscosity of poly(acrylic acid) PAA solutions depending on shear rate.
Open Research DataThe rheological characteristics of poly(acrylic acid) PAA solutions were based on viscosity measurements using a Brookfield viscometer, using LV SC4 - 27 spindles and shear rates from 1,7 to 39 s-1 (Fig. 1). PAA solutions with were prepared in water. The data allowed to characterize the used PAA and assess their functional parameters as rheology modifying...
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The electrochemical studies of CB-PLA electrode after surface activation by proteinase K digestion
Open Research DataThe dataset contains the electrochemical studies performed to evaluate surface activation of the CB-PLA 3D printed electrodes by enzymatic hydrolysis in a solution containing proteinase K (72h digestion period). Different enzyme concentrations were evaluated: 0.2, 0.4, 0.6 and 0.8 mg/ml. The studies were performed before surface activation, during and...
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Caffeine detection using CB-PLA electrode after Nd:YAG laser ablation in He atmosphere
Open Research DataThe dataset contains electrochemical studies in form of cyclic voltammetry (CV) and differential pulse voltammetry (DPV) of laser-activated 3D printed CB-PLA electrodes. The ablation of the 3D-printed CB-PLA electrodes was carried out using a pulsed LaserBlast 500 Nd:YAG laser (Quantel, France) operating at 1064 nm and a 6 ns pulse duration.
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The cyclic voltammetry studies of CB-PLA electrode after surface activation by electrolysis in 1M NaOH
Open Research DataThe dataset contains the electrochemical studies performed for surface activation of the CB-PLA 3D printed electrodes by electrolysis in 1M NaOH solution. The studies were performed after treatment at an anodic overpotential of 1V, found to be optimal for surface activation. The measurements were carried out with cyclic voltammetry (CV) under different...
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The XPS studies of the CB-PLA electrodes after different surface treatments (chemical, electrochemical, enzymatic)
Open Research DataThe dataset contains the Xray Photoelectron Spectroscopy results of the studies performed under different conditions of surface activation of the CB-PLA 3D printed electrodes. The activation was performed by hydrolysis in different solvents (DMF, 1M HCl, 1M NaOH), electrolysis in 1M NaOH, enzymatic treatment in polymerase or simultaneous electrolysis...
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Solar radiation (PAR, UV-B and UV-A) reaching the sea surface - Gdańsk Deep (2001-2005)
Open Research DataSolar radiation reaching the sea surface was measured in spring (2001, 2003, 2005) and autumn (2002, 2004). For measurements of the photosynthetic active radiation - PAR (400-700 nm), the Ejkelkamp SKP 210 / I 0896 13595 sensor was used, the UV-B radiation (280-315 nm) was measured with the Ejkelkamp SKU 430 0497 14854 sensor, while UV-A (315- 380 nm)...
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Ball on disk test AL(rf.)-Al2O3-r25
Open Research DataHard particle reinforced Al6061 alloy testing. Laser remelting and kinetic injection of particulate material. Ball on disc tribological test. Ball material: Al2O3. Ball diameter: 5 mm. Sliding path radius: 25 mm. Disk material: Al6061 not treated (reference).
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Ball on disk test AL(rf.)-Al2O3-r15
Open Research DataHard particle reinforced Al6061 alloy testing. Laser remelting and kinetic injection of particulate material. Ball on disc tribological test. Ball material: Al2O3. Ball diameter: 5 mm. Sliding path radius: 15 mm. Disk material: Al6061 not treated (reference).
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The electrochemical studies of CB-PLA electrode after surface activation by proteinase K digestion with different times and concentrations
Open Research DataThe dataset contains the electrochemical studies performed to evaluate surface activation of the CB-PLA 3D printed electrodes by enzymatic hydrolysis in a solution containing proteinase K. DIfferent proteinase K concentrations and digestion times were evaluated, as described in subfolder names. The studies were performed before surface activation, during...
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Surface activation by cyclic polarization in 1M HCl and its effects on the electrochemical response of CB-PLA 3D printed electrodes
Open Research DataThe dataset contains the electrochemical studies performed for surface activation of the CB-PLA 3D printed electrodes by electrolysis in 1M HCl solution. The studies were performed after treatment at different polarization ranges, as labeled in subfolder names. For each electrode the consecutive studies describe different samples, as labeled in subfolders:...
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XRD (X-ray Diffraction) patterns of PMH, PMD and simulated MIL-53(Al)
Open Research DataThese data contain XRD (X-ray Diffraction) patterns of PMH, PMD and simulated MIL-53(Al). The results were recorded by a Philipsdiffractometer using Cu Ka radiation. Sample abbreviations (PMH, PMD, MIL-53(Al)) are in agreement with the markings used in the linked publication.
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Simulations of flows in the coastal zone of the Baltic Sea
Open Research DataThe study area is located in the Southern Baltic, within Polish Marine Areas, adjacent to the coastline in the vicinity of Lubiatowo village, where The Coastal Research Station (CRS) – a field laboratory of the Institute of Hydro-Engineering of the Polish Academy of Sciences (IBW PAN) –is situated. The numerical reconstruction of the coastal flow was...
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Functional specialisation and economic upgrading in GVCs
Open Research DataThe dataset collected for selected Central Eastern European (CEE) countries (CZE, EST, HUN, LVA, LTU, POL, SVK, SVN) contains country-level and sector-level observations for the project implementation linked to the concept of functional specialization of economies. The aim of the project is to identify patterns of functional specialisation in global...
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Dual role of oxygen-related defects in the luminescence kinetics of AlNMn2+
Open Research DataThis dataset presents the impact of temperature and pressure on AlN:Mn2+ luminescence kinetics. Unusual behavior of Mn2+ optical properties during UV excitation is observed, where a strong afterglow luminescence of Mn2+ occurs even at low temperatures. When the temperature increases, the contribution of the afterglow luminescence is further enhanced,...
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AFM investigation of electrode fabricated by 3D printing
Open Research Data3D printing, also known as additive manufacturing, has enjoyed great interest in recent years due to the versatility of this method of producing various shapes and details. Due to the possibility of precise control of the shape and composition of the printed elements, the discussed technique can be widely used in electrochemistry, including electrochemical...
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The influence of microstructure on the corrosion resistance for some titanium-based alloys
Open Research DataThis dataset contains scanning electron microscopy (SEM) micrographs revealing the microstructure of some Ti-based alloys, namely: Ti-6Al-4V (file name: TiV), Ti-6Al-7Nb (file name: TiNb) and TC21 (file name: TiAlSnZrMoCrNbSi) alloys and their localized corrosion as a result of passive layer breakdown in a corrosive environment, ie. 0.9% NaCl solution...
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Compression test results of fused filamend fabricated polylactyde and polylactyde with carbon fiber filler
Open Research DataThe DataSet contains the results of the mechanical behaviour of cube specimens with dimensions 30 x 30 x 30 cm3. The specimens were additively manufactured with the fused filament fabrication (FFF) method. They used two different materials polylactide (PURE PLA) and polylactide with carbon fibre filler (PLA+CF). The specimens were segregated into three...
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Tensile test results of fused filamend fabricated polylactyde and polylactyde with carbon fiber filler
Open Research DataThe Dataset contains the results of the mechanical behaviour of dog-bone shaped specimens. The specimens were additively manufactured with the fused filament fabrication (FFF) method. They used two different materials polylactide (PURE PLA) and polylactide with carbon fibre filler (PLA+CF). The specimens were segregated into three groups - unsterilized,...
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Epitaph of Anna and Daniel Zierenberg in St. Mary's Church in Gdańsk
Open Research DataThe data set concerns epigraphy. It refers to the epitaph placed in St. Mary’s Church in Gdańsk, that is dedicated to Anna and Daniel Zierenberg. Daniel was particularly interested in activities for the education of Gdańsk and was one of those mayors who in 1596 established the foundation called Bibliotheca Senatus Gedanensis (today PAN BG). Data set...
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The profiles and spectrum of aqua solution of tannic acid by HPLC-DAD-MS analysis.
Open Research DataThe profiling of tannic acid is determined by examining the content and proportion / ratio of gallotannins [Aras et al. 2016, Clifford et al. 2007, Gauri et al. 2012, Nishizawa et al. 1982]. In order to check the ion mass distribution (TIC) in an aqueous solution of commercial tannic acid, a direct sample injection (TA) was performed into the mass spectrometer....
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Thermal stability analysis of poly(lactic acid)-carbon black-nanodiamond composite
Open Research DataThis dataset contains thermal stability tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include: thermogravimetric analysis (TGA)...
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Physicochemical studies (Raman) of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains Raman spectroscopy studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different temperatures...
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Scanning electron microscopy (SEM) images of boron-doped diamond thin films at poly(lactic acid)
Open Research DataThe dataset contains the photos obtained by scanning electron microscope(SEM), revealing the surface morphology and cross-section of boron-doped diamond electrodes on commercially available graphene-doped polylactide acid. The boron doping level expressed as the [B]/[C] ratio in the gas phase for these studies was 500 and 10,000 ppm. The top views of...
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Broadband dielectric spectroscopy studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains broadband dielectric spectroscopy studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different...
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Topography studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains topography studies with scanning electron microscope of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material...
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Electrochemical analyses of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains cyclic voltammetry studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different temperatures...
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Thermal analyses of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains thermal analyses (TGA, DTG, DSC) studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different...
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XPS data of MXene catalyst
Open Research DataData contain results from XPS measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using 48% HF etching agent (MXene HF). The X-ray spectroscopy (XPS) measurements were conducted using Mg Ka (hn = 1253.6 eV) radiation in a Prevac (Poland) system equipped with a Scienta SES 2002 (Sweden) electron...
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Rheology studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains MFR/MVR (melt flow rate) rheology studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The study aims to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different temperatures...
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Physicochemical studies (BET) of nanoparticles used for 3D printable conductive composites
Open Research DataThis dataset contains physico-chemical examination of fillers used to fabricate new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Geometric surface area of the nanoparticles was studied by Brunauer–Emmett–Teller (BET) adsorption/desorption isotherms. Investigated samples: CB Ensaco 250G, detonation...
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GC Chromatograms for isomerization of alpha-pinene
Open Research DataData contain results of the catalytic tests for the isomerization of alpha-pinene for the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y,...
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Physicochemical studies (Raman, XRD) of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains physico-chemical examination of a new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include Raman spectroscopy and X-ray diffraction...
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Rheology studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains rheology measurements carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was performed by melt mass-flow rates (MFR)....
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Mechanical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains mechanical tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was dynamic mechanical analysis (DMA). The measurements...
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The topography of carbon black-polylactide composite 3D printed electrodes after femtosecond laser ablation
Open Research DataThis dataset contains a series of scanning electron microscopy images revealing the topography of 3D printed carbon black-polylactide composite electrodes after laser ablation with a femtosecond laser. Different laser powers were investigated, namely: 10%, 25%, 50%, 75% and 100%. The CB-PLA electrodes were 3D printed using an Ender printer. Femtosecond laser NKT Photonics, Origami XP parameters: power at 100%...
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TGA data of MXenes catalysts
Open Research DataData contain results from TGA measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. ...
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Adsorption and desorption of N2 measurement of MXenes catalysts
Open Research DataData contain results from adsorption and desorption of N2 measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y...
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XRD patterns of MXenes catalysts
Open Research DataData contain results from XRD measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios....
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Raman spectra of MXenes catalysts
Open Research DataData contain results from Raman spectroscopy of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. ...
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SEM images of MXene catalysts
Open Research DataData contain results SEM measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. MAX...
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Impedance and cyclic voltammetry studies of GPLA electrodes after laser ablation
Open Research DataThe 3D printed GPLA electrodes present a brand new opportunity for electrode material for electrochemical biosensors. In order for the electrodes to be considered viable for electroanalysis studies, the pretreatment procedure must be applied in order to etch PLA matrix and reveal graphene filler. The following dataset presents an approach towards such...
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Raman spectroscopy analysis of poly(lactic acid)-carbon black composite treated by femtosecond laser
Open Research DataThe dataset contains the Raman spectroscopy measurements of commercially available carbon black-filled poly(lactic acid) 3D printed electrodes after femtosecond laser ablation. These results were utilized in the manuscript published in Electrochimica Acta: 10.1016/j.electacta.2022.140288
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New 3D printable filaments with nanodiamonds, physicochemical additives characteristics and electrochemical activity
Open Research DataThis dataset contains the physicochemical analyses (XRD, Raman spectroscopy, BET analyses) and electrochemical analyses (CV, EIS) for a new 3D-printable composite has been developed dedicated to electroanalytical applications. Two types of diamondised nanocarbons - detonation nanodiamonds (DNDs) and boron-doped carbon nanowalls (BCNWs) - were added...
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Electrochemical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains electrochemical investigation on electrodes 3D printed using a new composite composed of poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The presented results contain:1. electrochemical characterisation...
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Hydrometeorological and hydrochemical conditions in the Gulf of Gdańsk in the vicinity of Vistula river mouth in July of 1977
Open Research DataSome results of the complex measurements in the coastal zone of the Gulf of Gdańsk in the vicinity of the Vistula river mouth are included in this archival data set. The measurements were carried out by Institute of the Oceanography of the University of Gdańsk (IO UG) in July of 1977. The list of parameters includes wind direction and speed, Secchi...