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Search results for: LIQUID BISMUTH
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Macro-nutrients recovery from liquid waste as a sustainable resource for production of recovered mineral fertilizer: Uncovering alternative options to sustain global food security cost-effectively
PublicationGlobal food security, which has emerged as one of the sustainability challenges, impacts every country. As food cannot be generated without involving nutrients, research has intensified recently to recover unused nutrients from waste streams. As a finite resource, phosphorus (P) is largely wasted. This work critically reviews the technical applicability of various water technologies to recover macro-nutrients such as P, N, and...
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Characterization of GM3 Gangliosides in Human Milk throughout Lactation: Insights from the Analysis with the Use of Reversed-Phase Liquid Chromatography Coupled to Quadrupole Time-Of-Flight Mass Spectrometry
PublicationGangliosides are complex lipids found in human milk that play important structural and biological functions. In this study, we utilized reversed-phase liquid chromatography coupled to quadrupole time-of-flight mass spectrometry to evaluate the molecular distribution of GM3 in human milk samples collected at distinct lactation stages, ranging from colostrum to advanced lactation samples. Throughout lactation, GM3 d40:1 emerged as...
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An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products
PublicationIn the current research, a fast and sustainable air-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction followed by UV–Vis spectrophotometry measurements was optimized for the extraction and determination of melamine in milk and milk-based products. The central composite design was applied for the optimization of factors affecting the recovery of melamine. Quantitative extraction of...
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Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector
PublicationFabric Phase Sorptive Extraction (FPSE) combined with high pressure liquid chromatography using to diode array detection (HPLC-DAD) was applied for the simultaneous determination of bisphenols (BPA, BPB, BPC, BPE, BPF, BPS) in juice pouches. The FPSE procedure was optimized with regards to the critical parameters that affect the performance of the method including the selection of the FPSE membrane type and size, adsorption time,...
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublicationThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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Preparation and evaluation of 1,3-alternate 25,27-dibenzyloxy-26,28-bis-[3-propyloxy]-calix[4]arene - bonded silica stationary phase for high performance liquid chromatography
PublicationOtrzymano nową fazę stacjonarną na bazie dibenzyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej, chemicznie związaną z żelem krzemionkowym. Przeprowadzano badania selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu i pochodnych fenoli. Zaprezentowano wyniki badania wpływu pH fazy ruchomej oraz stężenia metanolu na zdolność rozdzielczą nowej fazy stacjonarnej.
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Tick-borne encephalitis – lipid peroxidation and its consequences
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Tick-borne encephalitis - lipid peroxidation and its consequences
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Lipid peroxidation products as potential bioindicators of Lyme arthritis
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The onset of lipid peroxidation in rheumatoid arthritis: consequences and monitoring
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Lipid peroxidation as a consequence of diabetes: effects of different treatment
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Plasma Lipid Composition and Risk of Developing Cardiovascular Disease
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ERCC1-deficient cells and mice are hypersensitive to lipid peroxidation
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1,4-DHP-lipid parameters and rod like micellae
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Lipid-protein interactions in membranes: a molecular modelling study
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The effect of a miniature argon flow rate on the spectral characteristics of a direct current atmospheric pressure glow micro-discharge between an argon microjet and a small sized flowing liquid cathode
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Coupling of cold vapor generation with an atmospheric pressure glow microdischarge sustained between a miniature flow helium jet and a flowing liquid cathode for the determination of mercury by optical emission spectrometry
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Critical evaluation of recent achievements in low power glow discharge generated at atmospheric pressure between a flowing liquid cathode and a metallic anode for element analysis by optical emission spectrometry
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The improvement of the analytical performance of direct current atmospheric pressure glow discharge generated in contact with the small-sized liquid cathode after the addition of non-ionic surfactants to electrolyte solutions
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Application of gas flow headspace liquid phase micro extraction coupled with gas chromatography-mass spectrometry for determination of 4-methylimidazole in food samples employing experimental design optimization
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Multi-Objective Genetic Algorithm (MOGA) As a Feature Selecting Strategy in the Development of Ionic Liquids’ Quantitative Toxicity–Toxicity Relationship Models
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Effect of ionic liquids on the structural, thermal, andin vitrodegradation properties of poly(ε-caprolactone) synthesized in the presence ofCandida antarcticalipase B
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Ionogel fibres of bis(trifluoromethanesulfonyl)imide anion-based ionic liquids for the headspace solid-phase microextraction of chlorinated organic pollutants
PublicationIonogels, a family of hybrid materials in which ionic liquids (ILs) are confined in a sol–gel network, are receiving much attention in a variety of scientific and technological fields. In this work, ionogels derived from three different ILs based on the anion bis(trifluoromethanesulfonyl)imide (TFSI), namely 1-butyl- 3-methylpyridinium bis(trifluoromethanesulfonyl)imide ([C4C1Py][TFSI]), 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesulfonyl)imide...
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Ultrasound-Assisted Solvent Extraction of a Porous Membrane Packed Sample for the Determination of Tobacco-Specific Nitrosamines in the Replacement Liquids for E-Cigarettes
PublicationThe content of tobacco-specific nitrosamines (TSNAs) possessing carcinogenic properties has been an important area of research since replacement liquids were introduced for e-cigarettes. A method for determining N′-nitrosonornicotine (NNN), 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK), N′-nitrosoanatabine (NAT), and N′-nitrosoanabasine (NAB) in replacement liquids for electronic cigarettes was developed using liquid chromatography–tandem...
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Superconductivity and appearance of negative magnetocaloric effect in Ba1–xKxBiO3 perovskites, doped by Y, La and Pr
PublicationRecently, substantial attention is given to the bismuth-based perovskites for variety of electronic applications. The perovskites are used for quantum dots displays (QLED), photovoltaic systems and superconducting (HTS) devices. In this paper comprehensive studies of Ba1–xKxBi1–yREyO3 bismuth perovskites (REBKBO, RE = Y , La or Pr) are reported. Apart from structural anomalous behavior at low temperatures, the electronic properties...
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Impact of Temperature and Nanoparticle Concentration on Turbulent Forced Convective Heat Transfer of Nanofluids
PublicationTheoretical analysis of the influence of nanoparticles and temperature on the average Nusselt (Nu) number and the average heat transfer coefficient (HTC) during the turbulent flow of nanofluid in a horizontal, round tube was carried out. The Nu number is a function of the Reynolds (Re) number and the Prandtl (Pr) number, which in turn are functions of the thermophysical properties of the liquid and the flow conditions. On the other...
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Chromatographic Examinations of Tea's Protection Against Lipid Oxidative Modifications
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Phosphatidylcholine with conjugated linoleic acid in fabrication of novel lipid nanocarriers
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Lipids and Lipid Mediators Associated with the Risk and Pathology of Ischemic Stroke
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Carotenoid binding to proteins: Modeling pigment transport to lipid membranes
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Membrane structure and interactions of peptide hormones with model lipid bilayers
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WETTABILITY OF CHITOSAN-MODIFIED AND LIPID/POLYPEPTIDE-COATED PEEK SURFACES
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Effect of lipid phase composition on autoxidation of water - in - oil emulsion
PublicationW pracy przedstawiono ocenę procesu autooksydacji emulsji W/O ze szczególnym uwzględnieniem składu fazy olejowej emulsji na postęp reakcji. Zbadano również wpływ wybranych antyoksydantów i emulgatorów na stabilność sporządzonych układów emulsyjnych.
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Preparation and evaluation of 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silics gel high performance liquid chromatography stationary phase
PublicationA 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silica gel stationary phase (CalixBzF10) was synthesized, structurally characterized, and used as a selector in liquid chromatography. The selectivity study of this phase was done by using fluorine-containing compounds (fluorobenzenes, fluoro-pyrimidine bases), as well as non-fluorinated analytes (non-steroidal anti-inflammatory drugs,...
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Wykorzystanie membran na etapie ekstrakcji analitów organicznychz ciekłych próbek środowiskowych i płynów biologicznych = Analytical applications of membrane extraction for liquid sample preparation in biomedical and environmental analysis
PublicationPrzedstawiono informacje dotyczące technik ekstrakcji membranowej wykorzystywanych do oznaczania związków organicznych w ciekłych próbkach środowiskowych i biologicznych. Szczególną uwagę zwrócono na podstawy teoretyczne oraz możliwości ich połączenia z technikami oznaczeń końcowych oraz obszarom praktycznego ich wykorzystania.
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The antagonistic role of chaotropic hexafluorophosphate anions and imidazolium cations composing ionic liquids applied as phase additives in the separation of tri-cyclic antidepressants
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Solvation of ionic liquids based on N-alkyl-N-methylmorpholinium cations in N,N-dimethylformamide and dimethyl sulfoxide – A volumetric and acoustic study
PublicationApparent molar volumes and molar isentropic compressibilities for N-ethyl-N-methylmorpholinium and N-decyl-N-methylmorpholinium tetrafluoroborates in N,N-dimethylformamide (DMF) and dimethyl sulfoxide (DMSO) have been determined from density and speed of sound measurements over the temperature range T = (298.15, 303.15, 308.15, 313.15, 318.15 and 328.15) K at experimental pressure p = 0.1 MPa. This data has been used to calculate...
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Interactions of N-alkyl-N-methylmorpholinium based ionic liquids with acetonitrile studied by density and velocity of sound measurements and molecular dynamics simulations
PublicationMorpholinium-based ionic liquids (ILs) and their mixtures with polar co-solvents are an interesting class of emerging electrolytes in electrochemistry that is relatively poorly studied. In this work, densities and sound velocities of four ILs, N-ethyl-N-methylmorpholinium tetrafluoroborate, N-butyl-N-methylmorpholinium tetrafluoroborate, N-octyl-N-methylmorpho-linium tetrafluoroborate and N-decyl-N-methylmorpholinium tetrafluoroborate...
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Satelitowy agregat pompowy
PublicationW artykule opisano najnowszą konstrukcję satelitowego agregatu pompowego charakteryzującego się tym, że pompa satelitowa jest umieszczona wewnątrz silnika elektrycznego i zasysa ciecz poprzez otwór wydrążony osiowo w wale silnika. Zastosowana w agregacie pompa satelitowa jest nowatorską konstrukcją zawierającą mechanizm satelitowy o odwróconej kinematyce znamienny tym, że planeta (wirnik) oraz płyty kompensacyjne (rozrządu) są...
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Mixed ionic-electronic conductivity and structural properties of strontium-borate glass containing nanocrystallites of Bi2 VO5.5
PublicationSamples of strontium borate glass containing bismuth vanadate nanocrystallites were prepared. Nanocomposites containing up to 45mol% of the Bi2VO5.5 phase exhibit electrical properties closer to the strontium-borate glass than to the ferroelectric Bi2VO5.5 ceramic. The glass matrix still may contain some part of bismuth and vanadium ions even after crystallization process and there is too little of crystalline phase to observe...
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Equations of tribological parameters for liquid flow in boundary layer on the tissue surface in bioreactor = Wyznaczanie parametrów tribologicznych dla przepływu cieczy w warstwie granicznej na powierzchni tkanki w bioreaktorze
PublicationW niniejszej pracy przedstawiony został problem tribologiczny wynikający z przepływu nieustalonego odżywczej cieczy lepkiej w cienkiej warstwie przyściennej w bezpośrednim kontakcie z zewnętrzną powierzchnią warstwy wierzchniej wzrastających komórek (chondrocytów) w trakcie procesu ich hodowli w bioreaktorze. Efektem rozważań będą wartości sił tarcia powstające na powierzchni wzrastającej tkanki. Najnowsze badania wykazały lepszą...
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Effect of the working liquid compressibility on the picture of volumetric and mechanical losses in a high pressure displacement pump used in a hydrostatic drive. Part I Energy losses in a drive system, volumetric losses in a pump
PublicationŚciśliwość cieczy roboczej może znacząco zmienić wartości i proporcje współczynników strat objętościowych i mechanicznych w pompie wyporowej zastosowanej w układzie napędu hydrostatycznego. Wpływ ten jest szczególnie widoczny w trakcie pracy pod wysokim ciśnieniem a także wówczas, gdy występuje zapowietrzenie cieczy roboczej. W części I przedstawiono wykres zaproponowany przez autora, wzrostu mocy w układzie napędu hydrostatycznego...
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Effect of the working liquid compressibility on the picture of volumetric and mechanical losses in a high pressure displacement pump used in a hydrostatic drive. Part I Energy losses in a drive system, volumetric losses in a pump
PublicationŚciśliwość cieczy roboczej może znacząco zmienić wartości i proporcje współczynników strat objętościowych i mechanicznych w pompie wyporowej zastosowanej w układzie napędu hydrostatycznego. Wpływ ten jest szczególnie widoczny w trakcie pracy pod wysokim ciśnieniem a także wówczas, gdy występuje zapowietrzenie cieczy roboczej. W części I przedstawiono wykres zaproponowany przez autora, wzrostu mocy w układzie napędu hydrostatycznego...
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublicationVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Convenient identification of desulfoglucosinolates on the basis of mass spectra obtained during liquid chromatography-diode array-electrospray ionisation mass spectrometry analysis: Method verification for sprouts of different Brassicaceae species extracts
PublicationOver the past decade, glucosinolates (GLs) present in different tissues of Brassicaceae and their breakdown products, especially isothiocyanates formed after myrosinase catalyzed hydrolysis, have been regarded as not only environment friendly biopesticides for controlling soilborne pathogens, but most importantly as promising anticarcinogenic compounds. For these reasons, the identification and quantitative determination of the...
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Oscylacje różnicy potencjału elektrochemicznego między fazami oscylatora z membraną ciekłą zawierającego bromek heksadecylotrimetyloamoniowy.Oscyllations of electrochemical potential difference between phases of liquid membrane oscillator containing heksadecyltrimethylammonium bromide.
PublicationBadano zmiany różnicy potencjału elektrochemicznego między fazami wodnymi oscylatora z membraną ciekłą zawierającego bromek heksadecylotrimetyloamoniowy przy zastosowaniu mikroelektrod Ag/AgCl/Cl. Stwierdzono, iż główny udział do różnicy potencjału elektrochemicznego między fazami wodnymi, wnoszą różnice potencjału między odpowiednią faza wodną i membraną ciekłą. Wartości obliczone z poszczególnych składowych są w bardzo dobrej...
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Ring thruster - a preliminary optimisation study of ferrofluid seal and propeller
PublicationThe article reports the course of preliminary examination of a ferrofluid seal applied in liquid environment.A newly built research rig is described, and results of pressure tests performed for different shaft rotationsare discussed. Other studies carried out in the past only referred to the gas environment, while the presentexamination aims at finding an answer to the question whether magnetic liquids can be successfully used...
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An effective method for studying intermolecular interactions in binary liquids with hydrogen bonds: FTIR spectra and ab initio calculations in the N-methylformamide - methanol system
PublicationMolecular complexes in methanol (MeOH)−N-methylformamide (NMF) mixtures were studied based on their FTIR-ATR spectra, to which two methods of analysis were applied: factor analysis and a quantitative version of the difference-spectra method. The mean composition of a complex between NMF and MeOH molecules over the whole range of mixture compositions was determined. Absorbing species differentiated with regard to the interaction...
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Solid Phase Micro-Extraction, a Versatile and Handy Tool in Environmental Trace Organic Analysis, Gets a New Class of Coatings, Polymeric Ionic Liquids
PublicationSolid phase microextraction (SPME) fundamentals, characteristics and application are described. The special stress is put on characteristics of sorbents used as SPME fiber coatings. Description of commercially available fibers and the present-day trends in development of new sorbents for SPME are given. Discussion is focused on possibility of application of ionic liquids (IL) and polymeric ionic liquids (PIL) as SPME fiber coatings....
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Solvation of ionic liquids based on N -methyl- N -alkylmorpholinium cations in N,N -dimethylformamide and N,N -dimethylacetamide – Volumetric and compressibility studies
PublicationDensity and sound velocity of the solutions of ionic liquids based on N-alkyl-N-methyl- morpholinium cations: N-ethyl- -methylmorpholinium bis(trifluoromethanesulfonyl)imide, N-butyl-Nmethylmorpholinium bis(trifluoromethanesulfonyl)imide, N-octyl-N-methyl -morpholinium bis(trifluor omethanesulfonyl)imide and N-decyl-N-methylmorpholinium bis(trifluoromethanesulfonyl)imide in N, N-dimethylformamide and N,N-dimethylacetamide were...