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Wyniki wyszukiwania dla: 2D TIO2 NANOSHEETS
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Au-RE-TiO2 nanocomposites: Surface characteristics and photoactivity
PublikacjaThe photocatalysts based on TiO2 co-doped with rare earth metal (RE) and gold nanoparticles have been prepared using a sol-gel method and followed by gold reduction. Specific surface areas of the modified photocatalysts were calculated by the Brunauer-Emmett-Teller method (BET). Diffuse reflectance spectra of the obtained photocatalysts were recorded in a UV-Vis spectrophotometer (DRS UV-Vis). The influence of the type of rare...
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Modele 1D i 2D przepływu w pompie diagonalnej
PublikacjaW pracy przedstawiono nowe podejście do rozwiązania zadania konstrukcyjnego pompy w ramach modelu osiowo-symetrycznego typu 2D. Przykład obliczeniowy cytowany w artykule przedstawia wirnik pompy diagonalnej poddanej obliczeniom 3D.Przedstawiono także nowy sposób prezentacji procesu tłoczenia w pompie diagonalnej w ramach modelu 1D w postaci wykresu energia - straty energii.
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Cytocompatibility of stabilized black phosphorus nanosheets tailored by directly conjugated polymeric micelles for human breast cancer therapy
PublikacjaThe novel procedure of few-layer black phosphorus (FLBP) stabilization and functionalisation was here proposed. The cationic polymer PLL and non-ionic PEG have been involved into encapsulation of FLBP to allow sufficient time for further nanofabrication process and overcome environmental degradation. Two different spacer chemistry was designed to bind polymers to tumor-homing peptides. The efficiency of functionalisation was examined...
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Progress, Challenge, and Perspective of Bimetallic TiO2-Based Photocatalysts
PublikacjaBimetallic TiO2-based photocatalysts have attracted considerable attention in recent years as a class of highly active catalysts and photocatalysts under both UV and Vis light irradiation. Bimetallic noble metal structures deposited on TiO2 possess the ability to absorb visible light, in a wide wavelength range (broad LSPR peak), and therefore reveal the highest level of activity as a result of utilization of a large amount of...
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TiO2-TG analyses -OH groups
Dane BadawczeTG analyses of TiO2 were performed under nitrogen flow to monitor desorption of hydroxyl groups. Physisorbed weak-bonded hydroxyl groups were desorbed totally at around 120oC, whereas chemisorbed ones at around 500oC. The mass loss at these temperatures was used as concentration of hydroxyl groups on TiO2 surface. The amount of analysed TiO2 was 10...
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Photocatalytic activity of TiO2 loaded with metal clusters
PublikacjaTiO2 modyfikowano powierzchniowo klasterami metali: srebra, złota i platyny. Zbadano wpływ rodzaju i ilości wprowadzonej domieszki, oraz matrycy TiO2 na aktywność fotokatalityczną otrzymanych próbek. Fotoaktywność próbek badano w reakcji degradacji fenolu (Co = 0,21 mmol/dm3 ) w zakresie światła Vis lub UV. Najwyższą aktywność zaobserwowano dla fotokatalizatorów zawierających 2%Ag, 1%Au oraz 0,5%Pt. Po 60 min naświetlania światłem...
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Measurements of the optical and thermal properties of the 2D black phosphorus coating
PublikacjaBlack phosphorus is a 2D material, which properties are still being discovered. In this paper, the sensitivity to the temperature of a few-layer black phosphorus coating deposited, on the surface of a microsphere-based fiber-optic sensor, by a dip-coating method is presented. The coating was investigated after 2, 3, and 5 deposition cycles and during temperature growth from 50 °C to 300 °C in an interferometric setup. The intensity...
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EFFICIENT LINE DETECTION METHOD BASED ON 2D CONVOLUTION FILTER
PublikacjaThe article proposes an efficient line detection method using a 2D convolution filter. The proposed method was compared with the Hough transform, the most popular method of straight lines detection. The developed method is suitable for local detection of straight lines with a slope from -45˚ to 45˚. Also, it can be used for curve detection which shape is approximated with the short straight sections. The new method is characterized...
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TiO2-zeta potential
Dane BadawczeData contain results from the measurements of zeta potential of TiO2 versus pH. Data are saved as original files and in the format of Excel file. measurements were perfomed in Zetasizer Nano ZS with using Multi-Purpose Titrator MPT-2.
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NOBLE METAL MODIFIED TiO2 FOR PHOTOCATALYTIC AIR PURIFICATION
PublikacjaTiO2 was surface modified with silver, gold, palladium and platinum ion clusters to improve its photocatalytic activity. The effect of metal content, the kind of dopant used during preparation procedure on the photoactivity were investigated. in toluene removal which was used as a model volatile organic compound. Toluene, at the concentration of about 100 ppm, was irradiated over noble metal modified TiO2 using light-emitting diodes...
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Hybrid TiO2–Polyaniline Photocatalysts and their Application in Building Gypsum Plasters
PublikacjaHybrid materials of conjugated polymer and titanium(IV) oxide have attracted considerable attention concerning their potential benefits, including (i) ecient exploitation of visible light, (ii) a high adsorption capacity for organic contaminants, (iii) and eective charge carriers separation. The new class of the photocatalysts is promising for the removal of environmental pollutants in both aqueous and gaseous phases. For the first...
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Pr-doped TiO2: The effect of metal content on photocatalytic activity
PublikacjaThe Pr-TiO2 nanoparticles were prepared by using the sol-gel method. As-prepared samples were characterized by BET measurements, X-ray powder diffraction analysis (XRD) and UV-Vis spectra. Visible and ultraviolet light photocatalytic activity of the sample was studied by photodegradation of phenol while considering the influence of the dopant concentration. TiO2 doped with 0.25 mol% of praseodymium showed the highest photocatalytic...
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Analyses of sulphur in TiO2 by XRFS
Dane BadawczeData contain content of sulphur in TiO2 determined by X-ray fluorescence spectroscopy. The results were obtained by using internal pattern.
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Rational designing of TiO2-X@Cs3Bi2X9 nanocomposite for boosted hydrogen evolution
PublikacjaHalide perovskites are known as compounds possessing interesting properties, including visible light-induced photoactivity, however, they suffer from instability. Herein, a novel technique for reducing the decomposition rate of halide bismuth-based perovskites Cs3Bi2X9 (X=I, Br, Cl) in the aqueous environment by combining with different types of TiO2 (anatase TiO2-I, anatase/rutile TiO2-B, and rutile TiO2-C synthesized using HI,...
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Photocatalytic decomposition of acetaldehyde over TiO2 (titanium dioxide) supported on nickel foam and Ni-doped (nickel-doped) TiO2
Dane BadawczeThis dataset contains chromatograms recorded during the decomposition of acetaldehyde in a high-temperature reaction chamber under UV irradiation using as photocatalytic systems TiO2 (titanium dioxide) supported on nickel foam, TiO2 supported on oxidized nickel foam and TiO2 doped by metallic nickel (Ni) powder. The detailed equipment and measurement...
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Simulation of Residence Time Distribution and Mixing in Reactors with Recirculation Using 2D Approach
PublikacjaIn this paper, we propose a 2D approach in order to create a mathematical model for the determination of the residence time distribution for a flow reactor with recirculation. Apart from characterizing the functional residence time distribution, this model can help improve the operation of the reactor at the design stage. The mathematical model was validated by comparison with experiments carried out in a hydraulic laboratory.
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Methane formation over TiO2–based photocatalysts: reaction pathways
PublikacjaThe effects of organic impurities adsorbed or incorporated into semiconductors structure on the photocatalytic products are noteworthy. For this purpose, the as-prepared Ag, Au and Pdmodified TiO2 samples were exposed to UV-vis irradiation in various gas atmospheres (CO2, N2, 600 ppm CO2 in N2, and 13CO2) in order to clarify the route of CH4 formation in the process of photocatalytic CO2 reduction. In the presented research it...
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TiO2-potential zeta in water
Dane BadawczeData contain results from measurements of zeta potential for powdered TiO2 in a diluted aqueous solution. The measurements were performed in Zetasizer Nano ZS analyser.
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The photoconductivity of sol-gel derived TiO2 films.
PublikacjaPrzygotowano metodą zol-żel warstwy TiO2 na podłożu kwarcowym. Zbadano ich fotoprzewodnictwo w różnych warunkach. Stwierdzono, że fotoprąd w próżni jest o trzy rzędy większy niż w powietrzu. Jako wyjaśnienie zaproponowano absorpcję tlenu na powierzchni warstwy.
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Implementacja zmodyfikowanej metody biliniowej 2D w elektronicznym systemie wbudowanym
PublikacjaPrzedstawiono implementację zmodyfikowanej metody biliniowej 2D diagnostyki sieci analogowych we wbudowanych mikrosystemach mieszanych sygnałowo sterowanych mikrokontrolerami. Metoda cechuje się prostym algorytmem diagnostycznym, który z powodzeniem można zaimplementować w 8-bitowych, powszechnie stosowanych mikrokontrolerach z interfejsem SPI, oraz nie wymaga nadmiernej rozbudowy mikrosystemu o część testującą (BIST). Zaletą metody...
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Photocatalytic decomposition of ethylene on the TiO2-polystyrene spheres
Dane BadawczeData contain results from the measurements of the photocatalytic decomposition of ethylene under UV irradiation with using TiO2 coating on the expanded polystyrene spheres (EPS). EPS-SiO2-TiO2 and EPS-TiO2 were used as the photocatalytic beds in the fluidized bed reactor. Both, stationary and fluidized beds were tested. The comparison of ethylene decomposition...
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A critical review on electrospun membranes containing 2D materials for seawater desalination
PublikacjaElectrospun nanofibers are a cutting-edge class of membranes which have been applied in several molecular separations. These membranes can be well designed and tailored due to the versatility of the electrospinning process. Eminently, electrospun membranes, once implemented in membrane processes, are an alternative in removing salts and some other minerals from water, so-called desalination, for producing drinking water. Such membranes...
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Photo-oxidation of dissolved cyanide using TiO2 catalyst
PublikacjaZbadano utlenianie katalityczne jonów cyjankowych w układzie UV/TiO2. Szybkość utleniania zbadano dla różnego stężenia początkowego CN-, wartość pH, formy katalizatora, temperatury oraz wprowadzanej formy gazowej. Stwierdzono że szybkość degradacji cyjanków w układzie UV/TiO2/O2 wzrasta dwukrotnie, jakkolwiek jest niezależna od ciśnienia cząstkowego tlenu (0,2-1,0 atm.). Wzrost temperatury środowiska reakcji w zakresie od 20 do...
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Enhanced photocatalytic activity of transparent carbon nanowall/TiO2 heterostructures
PublikacjaThe synthesis of novel tunable carbon-based nanostructure represented a pivotal point to enhance the efficiency of existing photocatalysts and to extend their applicability to a wider number of sustainable processes. In this letter, we describe a transparent photocatalytic heterostructure by growing boron-doped carbon nanowalls (B-CNWs) on quartz, followed by a simple TiO2 sol-gel deposition. The effect on the thickness and boron-doping...
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TiO2-based magnetic nanocomposites with core-shell structure
PublikacjaThe main aim of the doctoral dissertation was preparation and characterization of photocatalysts, with particular emphasis on modified titanium (IV) oxide photocatalysts, which can be applied for the degradation of organic pollutants not susceptible to biodegradation. A particularly important aspect of the work was the development of preparation method of nanocomposites with the magnetic core-shell and photocatalyst shell (TiO2)...
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Quenching of bright and dark excitons via deep states in the presence of SRH recombination in 2D monolayer materials
PublikacjaTwo-dimensional (2D) monolayer materials are interesting systems due to an existence of optically non-active dark excitonic states. In this work, we formulate a theoretical model of an excitonic Auger process which can occur together with the trap-assisted recombination in such 2D structures. The interactions of intravalley excitons (bright and spin-dark ones) and intervalley excitons (momentum-dark ones) with deep states located...
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XPS-TiO2 heated in H2
Dane BadawczeThese XPS spectra were recorded for TiO2 heat-treated at 450-600oC in H2. Surface oxygen groups were determined. Deconvolution of Ti 2p peak allowed to determine Ti3+ on the titania surface.
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Enhanced electrochemical capacitance of TiO2 nanotubes/MoSe2 composite obtained by hydrothermal route
PublikacjaThis study presents the hydrothermal synthesis of a novel TiO2 nanotubes/MoSe2 nanocomposite and investigates its enhanced electrochemical capacitance properties. The composite material was fabricated through a hydrothermal method, embedding MoSe2 onto TiO2 nanotubes. The resulting composite, termed Ti/TiO2/MoSe2, exhibited significantly improved electrochemical capacitance compared to TiO2 nanotubes alone. The synthesized composite...
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Chapter 31. Preparation of silver doped titanium dioxide nanoparticles in microemulsion system
PublikacjaNanocząstki TiO2 domieszkowanego srebrem przygotowano w mikroemulsji woda-AOT-cykloheksan. Zbadano wpływ zawartości srebra (od 1,5 do 8,5% mol.) na aktywność fotokatalityczą oraz właściwości bakterio- i grzybobójcze. Stwierdzono, że TiO2 modyfikowany za 6,5% mol. Ag wykazuje najwyższą aktywność w reakcji degradacji fenolu oraz najwyższą aktywność mikrobiologiczną. Aktywność mikrobiologiczną wyznaczano jako minimalne stężenie hamujące...
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Analysis of 2D Feature Spaces for Deep Learning-based Speech Recognition
Publikacjaconvolutional neural network (CNN) which is a class of deep, feed-forward artificial neural network. We decided to analyze audio signal feature maps, namely spectrograms, linear and Mel-scale cepstrograms, and chromagrams. The choice was made upon the fact that CNN performs well in 2D data-oriented processing contexts. Feature maps were employed in the Lithuanian word recognition task. The spectral analysis led to the highest word...
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TG analyses - content of SiO2 and TiO2 in polystyrene
Dane BadawczeTG analyses were performed for polystyrene spheres coating by SiO2 and then coating by SiO2-TiO2. Thermal analyses of polystyrene spheres only were also performed. The content of inorganic remaining was used for calculation the quantity of coating SiO2 and TiO2 in the polystyrene spheres.
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Recent Applications of 1D GC-MS and 2D GC-MS in Foodomics Studies
PublikacjaGas chromatography coupled with mass spectrometry and food chemistry have been tightly linked since the 1960s. This setup is also an integral part of the omics studies when it comes to low mass metabolites. Therefore, the marriage of GC-MS and foodomics is obvious. Two-dimensional gas chromatography coupled with mass spectrometry fits perfectly within the latest trends in foodomics, since it is tailored for holistic food analysis....
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Analiza porównawcza 2D i 3D klasycznego i bezstykowego elektrycznego ogrzewania rozjazdów kolejowych
PublikacjaElektryczne ogrzewanie rozjazdów jest istotnym problemem technicznym i ekonomicznym. Z tych względów istnieje potrzeba prowadzenia badań w celu optymalizacji systemu ogrzewania rozjazdów kolejowych. W niniejszym artykule przedstawiono wyniki analizy numerycznej układów ogrzewania rozjazdów kolejowych metodą klasyczną oraz z zastosowaniem grzejników odizolowanych termicznie od stopki szyny. Przeprowadzono analizę 2D i 3D rozpatrywanych...
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The Effect of Calcination Temperature on Structure and Photocatalytic Properties of WO3/TiO2 Nanocomposites
PublikacjaSeries ofWO3/TiO2 nanocompositeswere obtained by hydrothermal method followed by calcination in the temperature range from 400∘C to 900∘C. The characteristics of photocatalysts by X-ray diffractometry (XRD), scanning electron microscope (SEM), and diffuse reflectance spectroscopy (DRS) showed that increasing the calcination temperature from 400 to 900∘C resulted in change of photocatalytic activity under UV-Vis light.Moreover,...
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Fracture Energy of Bonded Joints with 2D Elastic Adhesive Layer
PublikacjaWhen bonded joint is subjected to mode I fracture loading, the adhesive joints analytical solutions treats the adhesive layer, usually, as not existing or 1D Hooke elastic layer. In the case of 1D elastic layer, represented as Hookes spring element, is acting, only, in direction contrary to the applied load. Basing on the information yielded from sensitive laser profilometry technique, where deflections of bonded part of the joint...
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Physicochemical and photocatalytic data of Cu-TiO2/Ti3C2 composites
Dane BadawczeIn this dataset, we include the data regarding the physicochemical properties (XRD, DR/UV-vis, photoluminescence, electrochemistry) and photocatalytic activity of TiO2/Ti3C2 and Cu-TiO2/Ti3C2 composites in the reaction of carbamazepine degradation. Herein we present the results for pure TiO2/Ti3C2 and composites modified with copper particles (0.25%,...
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Photocatalytic and Antimicrobial Properties of Ag2O/TiO2 Heterojunction
PublikacjaAg2O/TiO2 heterojunctions were prepared by a simple method, i.e., the grinding of argentous oxide with six different titania photocatalysts. The physicochemical properties of the obtained photocatalysts were characterized by diffuse-reflectance spectroscopy (DRS), X-ray powder diffraction (XRD) and scanning transmission electron microscopy (STEM) with an energy dispersive X-ray spectroscopy (EDS). The photocatalytic activity was...
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Preparation and characterisation of visible light responsive iodine doped TiO2 electrodes
PublikacjaPraca przedstawia charakterystykę domieszkowanego jodem ditlenku tytanu (I-TiO2) otrzymanego na drodze hydrotermicznej syntezy, gdzie prekursor stanowiły komplesy tytanu (IV) z ligandami zawierającymi atom jodu. Struktura nowego materiału została opisana za pomocą technik XPS, XRD, UV-vis i FT-IR-ATR. Badania te potwierdziły, że otrzymany proszek I-TiO2 ma zmniejszoną przerwę energetyczną. Praca prezentuje również badania elektrochemiczne...
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Ethylene decomposition on TiO2 under UV
Dane BadawczeData contain chromatograms recorded during decomposition of ethylene over TiO2 in a flow reactor under UV irradiation. Semilac UV lamp with total power of 72 W was used as a source of UV light. Chromatograms were recorded in Trace GC Ultra chromatograph equipped in FID detector. Sampling was realised via the dosing sample loop. TiO2 was coated on the...
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Zastosowanie metod spektroskopowych do charakterystyki nanokompozytów Ag-TiO2
PublikacjaNanocząstki Ag-TiO2 zawierające od 1,5 do 8% mol. srebra otrzymano poprzez hydrolizę tetraizopropylo tytanianu w mikroemulsji woda-AOT-cykloheksan, zawierającej w fazie wewnętrznej prekursor cząstek srebra i następnie redukcję jonów srebra. Charakterystyka otrzymanych fotokatalizatorów Ag-TiO2 obejmowała, wyznaczenie właściwości absorpcyjnych, energii pasma wzbronionego (Eg), powierzchni właściwej BET, badanie aktywności fotokatalitycznej...
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EHD Flow Measured by 2D PIV in a Narrow Electrostatic Precipitator with Longitudinal Wire Electrode
PublikacjaIn this paper, results of the electrohydrodynamic (EHD) flow patterns in two narrow ESPs with longitudinally-to-flow wire electrode arepresented. The influence of the ESP geometry on the EHD flow generated in the ESP was investigated. The results obtained from 2-dimensional(2D) Particle Image Velocimetry (PIV) showed similarities and differences of the particle flow in the wire-plate and wire-cylinder type ESP.
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Optimization of carbamazepine photodegradation on defective TiO2-based magnetic photocatalyst
PublikacjaIn this work, carbamazepine (CBZ) degradation over defective Fe3O4@SiO2/d-TiO2/Pt photocatalyst was studied. Within the titania structure, Ti vacancies and Pt nanoparticles were introduced to enhance the photocatalyst’s light absorption and influence charge carriers’ mobility. For the carbamazepine degradation, process parameters, e.g., temperature, flux intensity, photocatalyst loading, aeration, pH, and addition of H2O2, were optimized...
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Otrzymywanie i charakterystyka TiO2 modyfikowanego metalami ziem rzadkich
PublikacjaW ostatnich latach wzrosło zainteresowanie bardziej wydajnym pozyskiwaniem energii promieniowania słonecznego, dlatego celem badań było opracowanie nowych, funkcjonalnych nanokompozytów na bazie TiO2, charakteryzujących się wysoką aktywnością fotokatalityczną. Metale ziem rzadkich to substancje o właściwościach luminescencyjnych, które mogą absorbować promieniowanie z zakresu widzialnego i emitować promieniowanie z zakresu ultrafioletowego....
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TiO2 and Reducing Gas: Intricate Relationships to Direct Reduction of Iron Oxide Pellets
PublikacjaIn response to the imperative for sustainable iron production with reduced CO2 emissions, this study delves into the intricate role of TiO2 in the direct reduction of iron oxide pellets. The TiO2-dependent reducibility of iron oxide pellets utilizing H2 and CO gas across varied temperatures and gas compositions is thoroughly investigated. Our findings unveil the nuanced nature of the TiO2 effect, underscored by its concentration-dependent...
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Visible light photoactivity and structure of doped TiO2
PublikacjaOmówiono strukturą i właściwości TiO2 domieszkowanego siarką, węglem oraz borem. Aktywność fotokatalityczna zbadano w reakcji degradacji fenolu pod wpływem światła z zakresu widzialnego (l > 400 nm). Aktywność fotokatalizatorów odniesiono do ich właściwości takich jak powierzchnia właściwa, struktura krystaliczna oraz charakter chemiczny domieszki. Stwierdzono, że fotokatalizatory o najwyższej aktywności mają strukturę anatazu...
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SEM of TiO2 heated at 400-600oC in Ar or H2
Dane BadawczeData contain some SEM images of TiO2 taken after its heat treatment in Ar or H2 at 400-600oC. Treated TiO2 was crystalline anatase phase with 3-4 % of rutile nclei.
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ADAPTIVE METHOD FOR THE SOLUTION OF 1D AND 2D ADVECTION-DIFFUSION EQUATIONS USED IN ENVIRONMENTAL ENGINEERING
PublikacjaThe paper concerns the numerical solution of one-dimensional (1D) and two-dimensional (2D) advection-diffusion equations. For the numerical solution of the 1D advection-diffusion equation a method, originally proposed for solution of the 1D pure advection equation, has been developed. A modified equation analysis carried out for the proposed method allowed increasing of the resulting solution accuracy and consequently, to reduce...
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0D, 1D, 2D molybdenum disulfide functionalized by 2D polymeric carbon nitride for photocatalytic water splitting
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Defective TiO2 for CO2 photoreduction: Influence of alkaline agent and reduction temperature modulation
PublikacjaThis study investigates the synthesis and characterization of Black TiO2 photocatalyst (TiO2-x) through the sol-gel method combined with NaBH4 reduction at different temperatures (350 °C, 500 °C, and 650 °C). The photocatalytic performance for CO2 reduction was evaluated, revealing that TiO2-x_500°C sample exhibited the highest efficiency. This enhanced performance is mainly attributed to a higher concentration of oxygen vacancies...
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NOx Photooxidation over Different Noble Metals Modified TiO2
PublikacjaWe compared the activity enhancement effect of noble metal deposited on TiO2 in photocatalytic nitrogen oxides oxidation. Titanium dioxide was decorated with Ag, Au, Pt or Pd in the sol-gel process. Synthesized catalysts were characterized by X-ray diffraction (XRD), Brunauer–Emmett–Teller measurement (BET), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) and energy dispersive X-ray analysis (EDX)....