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Wyniki wyszukiwania dla: ATOMIC LAYER DEPOSITION
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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MnCo2O4 deposited by spray pyrolysis as a protective layer for stainless steel interconects
PublikacjaStainless steel interconnects working in Solid Oxide Fuel Cells stacks are exposed to high temperature resulting in their corrosion. Protective layers for the hydrogen and oxygen sides are necessary to protect the interconnect material, prolongate the stack lifetime and maintain the output power. In this paper MnCo2O4 protective layer for the oxygen side of the interconnect is deposited by spray pyrolysis and is examined.
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Influence of laser melting on surface layer properties of titanium alloy Ti6Al4V
PublikacjaIn time of rapid technology and medicine progress, implants are becoming more widely used in the human body, ranging from dental implants, stabilizing plates, screws, orthopaedic prostheses. For example, there are many types of hip prostheses used for hip replacement as well as various types of materials used for these orthopaedic prostheses. Properties of titanium alloys used in hip prostheses combined with good strength properties,...
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Fabrication and Characterization of Flexible Medical-Grade TPU Filament for Fused Deposition Modeling 3DP Technology
PublikacjaThe possibility of using additive manufacturing (AM) in the medicine area has created new opportunities in health care. This has contributed to a sharp increase in demand for 3D printers, their systems and materials that are adapted to strict medical requirements. We described herein a medical-grade thermoplastic polyurethane (S-TPU) which was developed and then formed into a filament for Fused Deposition Modeling (FDM) 3D printers...
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Journal of Atomic and Molecular Sciences
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Exploration and Research for Atomic Minerals
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Nuclear Physics and Atomic Energy
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Sensing the onset of epoxy coating degradation with combined Raman spectroscopy/atomic force microscopy/electrochemical impedance spectroscopy
PublikacjaThe paper presents the results of investigation on epoxy resin durability upon 12-week exposure to UV radiation. The aim was early determination of the onset of epoxy degradation and for this purpose an epoxy film on steel substrate systems were periodically inspected using Raman spectroscopy, atomic force microscopy and electrochemical impedance spectroscopy. The behaviour of examined polymer could be divided into three periods: immunity,...
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Recent advances on spinel-based protective coatings for solid oxide cell metallic interconnects produced by electrophoretic deposition
PublikacjaThe application of ceramic protective coatings to the metallic interconnects in solid oxide cells (SOCs) is a viable and effective method to limit interconnect degradation issues. This featured letter provides a critical overview of the main outcomes of current research on the use of the electrophoretic deposition (EPD) technique to produce protective coatings for SOC metallic interconnects, specifically focusing on different approaches...
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Polyurethanes as a Potential Medical-Grade Filament for Use in Fused Deposition Modeling 3D Printers – a Brief Review
PublikacjaThe possibility of using 3D printing technology (3DP) in medical field is a kind of revolution in health care. This has contributed to a rapid growth in demand for 3D printers, whose systems and materials are adapted to strict medical requirements. In this paper, we report a brief review of polyurethanes as a potential medical-grade filament for use in Fused Deposition Modeling (FDM) 3D printer technology. The advantages of polyurethanes...
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Nanotubular Oxide Layer Formed on Helix Surfaces of Dental Screw Implants
PublikacjaSurface modification is used to extend the life of implants. To increase the corrosion resistance and improve the biocompatibility of metal implant materials, oxidation of the Ti-13Nb- 13Zr titanium alloy was used. The samples used for the research had the shape of a helix with a metric thread, with their geometry imitating a dental implant. The oxide layer was produced by a standard electrochemical method in an environment of...
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Influence of Gd deposition on the oxidation behavior and electrical properties of a layered system consisting of Crofer 22 APU and MnCo2O4 spinel
PublikacjaIn the study, the surface of the Crofer 22APU ferritic steel was modified with gadolinium oxide nanoparticles and a protective-conducting layer consisting of the MnCo2O4 spinel. This system was studied in the context of application in IT-SOFC interconnects. Four types of samples were studied: unmodified steel, steel coated with a manganese-cobalt spinel layer, steel modified with gadolinium oxide nanoparticles, and a system consisting...
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Estimation of Stresses in a Dry Sand Layer Tested on Shaking Table
PublikacjaTheoretical analysis of shaking table experiments, simulating earthquake response of a dry sand layer, is presented. The aim of such experiments is to study seismic-induced compaction of soil and resulting settlements. In order to determine the soil compaction, the cyclic stresses and strains should be calculated first. These stresses are caused by the cyclic horizontal acceleration at the base of soil layer, so it is important...
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The Impact of Homogeneity of High Modulus Asphalt Concrete Layer on Low-Temperature Cracking
PublikacjaDuring winter season of 2012 numerous transverse cracks developed in high-modulus asphalt concrete (HMAC) base of newly constructed motorway. Pavement cracked both in transverse joint locations and in the area between them. Research which was conducted during investigation of the causes and mechanisms of cracking consisted of: field examination, laboratory testing of specimens cored out of the existing pavement, computational analyses...
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41st European Group for Atomic Systems Conference Book of Abstracts
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Building federation of digital libraries basing on concept of atomic services
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Optimal reshaping and stress controlling of double-layer spherical structures under vertical loadings
PublikacjaOptimal reshaping and stress controlling of double-layer spherical structures under vertical loadings
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Corrosion Study of Ceria Protective Layer Deposited by Spray Pyrolysis on Steel Interconnects
PublikacjaSingle fuel cells and electrolysis cells are assembled into stacks using interconnects in order to increase power and gas production capacity. The most common choice for the interconnect material is stainless steel. It has good electrical and mechanical properties and is also cost effective. One of the problems when using steel is the formation of a thermally grown oxide scale during use which has a lower electrical conductivity...
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Changes of emissions and atmospheric deposition of mercury, lead and cadmium
PublikacjaPrzedstawiono informacje o zmianach emisji rtęci, ołowiu i kadmu w przeszłości, jak również przedyskutowano poziom aktualnych emisji tych zanieczyszczeń oraz ich scenariusze zmian w przyszłości. Przeanalizowano wpływ różnych parametrów na zmiany emisji w tym stopień implementacji różnych strategii kontroli emisji w Europie. Scenariusze zmian emisji w przyszłości oparte są na scenariuszach rozwoju gospodarczego w poszczególnych...
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Pressure field in a plane layer
PublikacjaPraca prezentuje wyniki badań teoretycznych i numerycznych zagadnienia przejścia fal płaskich przez warstwę. Omówiono zagadnienie tworzenia i rozchodzenia się fal w poszczególnych warstwach. Zaproponowano model matematyczny opisujący zmiany ciśnienia wewnątrz warstwy. Analizowano ciśnienie wewnątrz warstwy, fale bieżące i odbite wewnątrz warstwy oraz w ośrodku otaczającym. Przedstawiono wyniki badań numerycznych.
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The Influence of the Depth of Cut in Single-Pass Grinding on the Microstructure and Properties of the C45 Steel Surface Layer
PublikacjaThe paper contains the results of a metallographic examination and nanoindentation test conducted for the medium carbon structural steel with low content of Mn, Si, Cu, Cr, and Ni after its grinding to a depth ranging from 2 μm to 20 μm, at constant cutting speed (peripheral speed) of vs = 25 ms−1 and constant feed rate of vft = 1 m/min. Applied grinding parameters did not cause the surface layer hardening, which could generate...
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Investigation of poly(3,4-ethylenedioxythiophene) deposition method influence on properties of ion-selective electrodes based on bis(benzo-15-crown-5) derivatives
PublikacjaGlassy carbon electrodes modified by conductive polymers and membrane with derivatives of bis(benzo-15-crown-5) were tested as solid contact ion selective electrodes for K+ ions concentration determination. PEDOT with PSS, Cl- and ClO4- counter ions was electrochemically deposited onto glassy carbon substrates using four different electrochemical approaches (potentiostatic, galvanostatic, potentiodynamic and potentiostatic pulses)....
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JOURNAL OF AEROSOL MEDICINE-DEPOSITION CLEARANCE AND EFFECTS IN THE LUNG
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CMGNet: Context-aware middle-layer guidance network for salient object detection
PublikacjaSalient object detection (SOD) is a critical task in computer vision that involves accurately identifying and segmenting visually significant objects in an image. To address the challenges of gridding issues and feature...
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Performance of a single layer fuel cell based on a mixed proton-electron conducting composite
PublikacjaMany of the challenges in solid oxide fuel cell technology stem from chemical and mechanical incompatibilities between the anode, cathode and electrolyte materials. Numerous attempts have been made to identify compatible materials. Here, these challenges are circumvented by the introduction of a working single layer fuel cell, fabricated from a composite of proton conducting BaCe0.6Zr0.2Y0.2O3-δ and a mixture of semiconducting...
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Hydrogen Embrittlement and Oxide Layer E ect in the Cathodically Charged Zircaloy-2
PublikacjaThe present paper is aimed at determining the less investigated effects of hydrogen uptake on the microstructure and the mechanical behavior of the oxidized Zircaloy-2 alloy. The specimens were oxidized and charged with hydrogen. The different oxidation temperatures and cathodic current densities were applied. The scanning electron microscopy, X-ray electron diffraction spectroscopy, hydrogen absorption assessment, tensile, and...
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Investigation of the Few‐Layer Black Phosphorus Degradation by the Photonic Measurements
PublikacjaFew-layer black phosphorus (FLBP) is a 2D material that gains worldwide interest for its possible applications, mainly in electronics and optoelec-tronics. However, as FLBP is prone to a degradation process under envi-ronmental conditions, there is a need for a monitoring method allowing investigation of its surface quality. Among many techniques, optoelectronic ones have unique advantages of fast response, non-contact, and non-invasive...
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Equivalent single-layer models in deformation analysis of laminated multilayered plates
PublikacjaThe performance of selected Equivalent Single-Layer (ESL) models is evaluated within several classical benchmark tests for linear static analysis of multi-layered plates. The authors elaborated their own Finite Element software based on the first-order shear deformation theory (FOSD) with some modifications incorporated including a correction of the transverse shear stiffness and an application of zig-zag type functions. Seven...
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Modelling of elastic wave propagation in a bolted joint using a thin layer of shell elements
PublikacjaThere are many mathematical models describing the propagation of elastic waves through the imperfect boundary of two media. They were successfully applied to modelling of high frequency bulk waves and their interaction with local defects. On the other hand, the existing literature models of bolted connections ignore the aspect of imperfect connection between elements. Therefore, this paper presents the concept of application of...
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The effect of metal cluster deposition route on structure and photocatalytic activity of mono- and bimetallic nanoparticles supported on TiO2 by radiolytic method
PublikacjaTiO2 (P25) was modified with small and relatively monodisperse mono- and bimetallic clusters (Ag, Pd, Pt, Ag/Pd, Ag/Pt and Pd/Pt) induced by radiolysis to improve its photocatalytic activity. The as-prepared samples were characterized by X-ray fluorescence spectrometry (XRF), photoluminescence spectrometry (PL), diffuse reflectance spectroscopy (DRS), X-ray powder diffractometry (XRD), scanning transition electron microscopy (STEM)...
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Determination of the refractive index and wavelength‐dependent optical properties of few‐layer CrCl3 within the Fresnel formalism
PublikacjaBased on previous reports on the optical microscopy contrast of mechanically exfoliated few layer CrCl3 transferred on 285 nmand 270 nmSiO2 on Si(100), we focus on the experimental determination of an effective mean complex refractive index via a fitting analysis based on the Fresnel equations formalism. Accordingly, the layer and wavelength-dependent absorbance and reflectance are calculated. Layer and wavelength-dependent optical...
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Advances in assessing the elemental composition of distilled spirits using atomic spectrometry
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Dynamic Nanoimpedance Characterization of the Atomic Force Microscope Tip-Surface Contact
PublikacjaNanoimpedance measurements, using the dynamic impedance spectroscopy technique, were carried out during loading and unloading force of a probe on three kinds of materials of different resistivity. These materials were: gold, boron-doped diamond, and AISI 304 stainless steel. Changes of impedance spectra versus applied force were registered and differences in the tip-to-sample contact character on each material were revealed. To...
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Determinants of Directionality and Efficiency of the ATP Synthase Fo Motor at Atomic Resolution
PublikacjaFo subcomplex of ATP synthase is a membrane-embedded rotary motor that converts proton motive force into mechanical energy. Despite a rapid increase in the number of high-resolution structures, the mechanism of tight coupling between proton transport and motion of the rotary c-ring remains elusive. Here, using extensive all-atom free energy simulations, we show how the motor’s directionality naturally arises from the interplay...
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Chemistry of non-precipitation components of wet deposition with Poland as an example
PublikacjaW pracy przedstawiono badania dotyczące chemizmu osadów atmosferycznych pobieranych na terenie Polski w okresie od 2004 do 2007 roku. Średni skład jonowy (TIC) dla rosy, szronu i mgły (w stanie ciekłym i stałym) wynosił odpowiednio 2147, 1929 i 1014 µeq/l, gdzie typowy skład jonowy TIC dla opadów atmosferycznych wynosi 318 µeq/l. Dla wszystkich typów osadów atmosferycznych różne jony pełnią ważną rolę: Ca2+ i SO42-...
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The electrochemical deposition of nickel from electrolytes containing malonic acid
PublikacjaZbadano proces elektrolitycznego osadzania niklu z roztworów siarczanowych zawierających kwas malonowy lub winowy jako bufor zamiast kwasu borowego. Badano wpływ gęstości prądu katodowego, pH roztworu i temperaturę. Określono pojemność buforową i wgłębność kąpieli. Wyznaczono wydajności prądowe, twardość oraz połysk powłok niklowych otrzymanych z badanych kąpieli. Określono optymalne warunki pracy kąpieli i wykazano jej zalety...
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Energy deposition on the inner surface of a Hall Effect thruster for satellite
PublikacjaHET - Hall Effect Thruster, to silnik powszechnie wykorzystywany w kosmonautyce do pozycjonowania satelitów. Medium dostarczającym ciąg silnikowi jest zjonizowany gaz. Praca przedstawia wyniki trzech symulacji komputerowych: 1. Modelowanie sondy Langmuira zanurzonej w plazmie ksenonowej o warunkach zbliżonych do tych panujących w silniku HET. Symulacje wykonano metodą metodą Particle-in-Cell Monte Carlo. Celem była analiza oddziaływania...
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POM/EVA Blends with Future Utility in Fused Deposition Modeling
PublikacjaPolyoxymethylene (POM) is one of the most popular thermoplastic polymers used in the industry. Therefore, the interest in its potential applications in rapid prototyping is understandable. Nevertheless, its low dimensional stability causes the warping of 3D prints, limiting its applications. This research aimed to evaluate the effects of POM modification with ethylene-vinyl acetate (EVA) (2.5, 5.0, and 7.5 wt.%) on its processing...
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The accretion of the new ice layer on the surface of hexagonal ice crystal and the influence of the local electric field on this process
PublikacjaThe process of creation of a new layer of ice on the basal plane and on the prism plane of a hexagonal ice crystal is analyzed. It is demonstrated that the ordering of water molecules in the already existing crystal affects the freezing. On the basal plane, when the orientations of water molecules in the ice block are random, the arrangement of the new layer in a cubic manner is observed more frequently — approximately 1.7 times...
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Thermal and hydraulic phenomena in boundary layer of minijets impingement on curved surfaces
PublikacjaPresented work considers flow and thermal phenomena occurring during the single minijet impingement on curved surfaces, heated with a constant heat flux, as well as the array of minijets. Numerical analyses, based on the mass, momentum and energy conservation laws, were conducted, regarding single phase and two-phase simulations. Focus was placed on the proper model construction, in which turbulence and boundary layer modeling...
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Microporous Polyurethane Thin Layer as a Promising Scaffold for Tissue Engineering
PublikacjaThe literature describes that the most efficient cell penetration takes place at 200–500 µm depth of the scaffold. Many different scaffold fabrication techniques were described to reach these guidelines. One such technique is solvent casting particulate leaching (SC/PL). The main advantage of this technique is its simplicity and cost efficiency, while its main disadvantage is the scaffold thickness, which is usually not less than...
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Tuning Electrochemical Performance by Microstructural Optimization of the Nanocrystalline Functional Oxygen Electrode Layer for Solid Oxide Cells
PublikacjaFurther development of solid oxide fuel cell (SOFC) oxygen electrodes can be achieved through improvements in oxygen electrode design by microstructure miniaturisation alongside nanomaterials implementation. In this work, improved electrochemical performance of an La0.6Sr0.4Co0.2Fe0.8O3-d (LSCF) cathode was achieved by the controlled modification of the La0.6Sr0.4CoO3-d (LSC) nanocrystalline interlayer introduced between a porous...
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Wear Resistance Enhancement of Al6061 Alloy Surface Layer by Laser Dispersed Carbide Powders
PublikacjaIn this paper, results of the experimental study on improving wear resistance in sliding friction of Al-based alloy are presented. The technique used involves the formation of a metal matrix composite (MMC) in the alloy surface layer by laser dispersion of carbide powders such as WC, TiC and SiC. For WC and TiC MMC surface coatings fabricated under conditions typical for most of the technologically relevant solid-state lasers (wavelength...
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Modeling of nonlinear generation in a bubble layer
PublikacjaPraca prezentuje numeryczne podejście do zagadnienia liniowego i nieliniowego rozpraszania w warstwie z pęcherzykami. Badania numeryczne niekoherentnego rozpraszania wykonano stosując metodę Monte Carlo. Propagację i wsteczne rozpraszanie sygnałów badano w oparciu o równanie Rayleigha-Plesseta.
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Electrochemical analysis of aluminium passive layer
PublikacjaZbadano proces pękania warstwy pasywnej na aluminium dla liniowo narastających naprężeń rozciągających oraz różnych warunków elektrochemicznych. Badania prowadzono w 0.1M NaCl metodą dynamicznej elektrochemicznej spektroskopii impedancyjnej przy różnych poziomach polaryzacji anodowej. Określono progową wartość naprężeń, przy której następowało zniszczenie warstwy pasywnej wskutek działania sił rozciągających.
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Superconductivity in three-layer Na0.3CoO2*1.3H2O
PublikacjaOdkryto nadprzewodnictwo w trójwarstwowym związku uwodnionego sodowo -kobaltowego tlenku Na0.3CoO2 * 1.3H2O. Opisany został sposób syntezy, badania strukturalne (XRD i TGA) a także badania podatności magnetycznej.
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High - voltage thin - layer fuses
PublikacjaZaprezentowano nową technologię i konstrukcję bezpieczników wysokonapięciowych wykorzystując technologie stosowane w mikroelektronice. Cienką warstwę topika naniesiono na quasiceramiczne podłoże. Wykonane modele bezpieczników charakteryzują się wysoką pewnością działania oraz małymi stratami I2t.
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Superconductivity in three-layer Na0.3CoO2·1.3H2O
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Analysis of nonlinear generation in bubble layer
PublikacjaRozważano zagadnienie liniowego i nieliniowego rozpraszania w warstwie z pęcherzykami. Badania numeryczne dotyczyły rozpraszania koherentnego i różnych własności rozchodzenia się fal wewnątrz warstwy z pęcherzykami jak odbicie od brzegu, dyspersja, tłumienie. Badania dla różnych rozkładów pęcherzyków przeprowadzono w oparciu o równanie Rayleigha-Plesseta.
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Structural and dynamic properties of water within the solvation layer around various conformations of the glycine-based polypeptide
PublikacjaSeveral conformations of the solvated glycine-based polypeptides were investigated using molecular dynamics simulations. Some properties of water in the neighbouring space around these molecules were investigated. It was found, that water forms a well-defined layer - the first solvation shell - around the peptide molecule, and thickness of this layer is independent of the peptide structure, and it equals to approximately 0.28 nm....