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Wyniki wyszukiwania dla: POLIMER CIEKŁOKRYSTALICZNY
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Evaluation of structural change during fast transformation process of cross-linked NR into liquid NR by light pyrolysis
PublikacjaThe presence of cross-linked networks in rubber creates a tremendous problem for recycling and reusing of waste rubber. Fast transformation of cross-linked natural rubber (NR) into liquid natural rubber was carried out by light pyrolysis in temperature range from 240 to 300 °C in variable time (in range: 1–30 min). The transformation efficiency was evaluated by measuring the sol fraction and the cross-link density of the gel fraction....
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Mechanical and thermal analysis of injection molded poly(methyl methacrylate) modified with 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) fire retarder
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Development of stabilized protonconducting membrane based on poly(ethylene-co-vinyl alcohol)
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Sulfonated poly(benzoyl paraphenylene) as a membrane for PEMFC: Ex situ and in situ experiments of thermal and chemical stability
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Comparison of the effect of montmorillonite, magnesium hydroxide and a mixture of both on the flammability properties and mechanism of char formation of HDPE composites
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Synergistic effect of activated carbon and Ni2O3 in promoting the thermal stability and flame retardancy of polypropylene
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Synergistic effect of fumed silica with Ni2O3 on improving flame retardancy of poly(lactic acid)
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Identification and localization of organic coating degradation onset by impedance imaging
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Effect of ground tire rubber on structural, mechanical and thermal properties of flexible polyurethane foams
PublikacjaFlexible polyurethane foams were modified with two kinds of ground tire rubber, untreated and thermo-mechanically reclaimed. A reclamation process was performed in auto-thermal conditions, which reduced the cost of the process and decreased the environmental impact of devulcanization (e.g., emission of gases). The reclamation process was carried out in a continuous manner using a co-rotating twin screw extruder. The foams were...
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Investigation of volatile low molecular weight compounds formed during continuous reclaiming of ground tire rubber
PublikacjaGround tire rubber was thermo-mechanically reclaimed at different temperature conditions (80, 120, 160 °C) using a co-rotating twin screw extruder. The progress of ground tire rubber reclaiming was evaluated with specific mechanical energy, sol fraction and thermogravimetric analysis. Volatile organic compounds (VOCs) including volatile sulfur compounds (VCSs) released from ground tire rubber and ground tire rubber after reclaiming...
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Mechanical properties of PVDF-coated fabric under tensile tests
PublikacjaThis article describes the laboratory tests necessary to identify the mechanical properties of the polyvinylidene fluoride (PVDF)-coated fabrics named Precontraint 1202S and Precontraint 1302S. First, a short survey of the literature concerning the description of coated woven fabrics is presented. Second, the material parameters for PVDF-coated fabrics are specified on the basis of biaxial tensile tests. A comparison of the 1:1...
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Curing characteristics, mechanical and thermal properties of reclaimed ground tire rubber cured with various vulcanizing systems
PublikacjaGround tire rubber was thermo-mechanical reclaimed at 120 °C using a co-rotating twin screw extruder. The effect of vulcanizing system type on curing characteristics, static mechanical properties (tensile strength, elongation-at-break, hardness and resilience), dynamic mechanical properties and thermal properties of reclaimed ground tire rubber was investigated. Reclaimed rubber was cured using different types of vulcanization...
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Degradation of polyurethanes in sea water
PublikacjaOceniono degradowalność różnych poliuretanów w wodzie morskiej Bałtyku. Porównano te dane z wynikami stopnia degradacji poliuretanów w wodzie morskiej z dodatkiem azydku sosowego. Ocenę stopnia degradacji przeprowadzano na podstawie pomiarów zmian masy, właściwości mechanicznych i morfologii przed i po procesie degradacji. Wykazano, że różna podatność na degradację poliuretanów w wodzie morskiej związana jest z ich odmiennym stopniem...
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Preparation and characterization of rigid polyurethane-polyglycerolnanocomposite foams
PublikacjaThis work reports on the preparation of polyurethane-polyisocyanurate (PUR-PIR) foams containing different polyglycerols and layered silicate nanoclays. The rigid polyurethane foams were obtained in a laboratory scale, in a single step method, from a two-component system with a NCO to OH groups ratio equal to two. The reaction mixture consisted of the proper amounts of a commercial oligoetherpolyol, polyglycerol, catalysts, water,...
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Influence of modified attapulgite on silicone pressure-sensitive adhesives properties
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Solubility of dapsone in deep eutectic solvents: Experimental analysis, molecular insights and machine learning predictions
PublikacjaBackground. Dapsone (DAP) is an anti-inflammatory and antimicrobial active pharmaceutical ingredient used to treat, e.g., AIDS-related diseases. However, low solubility is a feature hampering its efficient use. Objectives. First, deep eutectic solvents...
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Incorporation of magnetite particles in 3D matrices made from the blends of collagen, chitosan, and hyaluronic acid
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Predicting sulfanilamide solubility in the binary mixtures using a reference solvent approach
PublikacjaBackground. Solubility is a fundamental physicochemical property of active pharmaceutical ingredients. The optimization of a dissolution medium aims not only to increase solubility and other aspects are to be included such as environmental impact, toxicity degree, availability, and costs. Obtaining comprehensive...
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Influence of nitrogen plasma treatment on the wettability of polyetheretherketone and deposited chitosan layers
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The impact of lignin addition on the properties of hybrid microspheres based on trimethoxyvinylsilane and divinylbenzene
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Nonlinear viscoelasticity in Three Dimensional filler reinforced rubber composites and nanocomposites
PublikacjaThis chapter describes the influence of three-dimensional nanofillers used in elastomers on the nonlinear viscoelastic properties. In particular, this part focuses and investigates the most important three-dimensional nanoparticles, which are used to produce rubber nanocomposites. The rheological and the dynamic mechanical properties of elastomeric polymers, reinforced with spherical nanoparticles, like POSS, titanium dioxide and...
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Kinetics and Mechanism of Potassium Persulphate/L-Serine Initiated Polymerization of Methylmethacrylate
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Saturation ESR spectroscopy of PA12 polyamide
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Preparation and characterization of rigid polyurethane -polyglycerol nanocomposite foams
PublikacjaThis work reports on the preparation of polyurethane–polyisocyanurate (PUR–PIR) foams containing different polyglycerols and layered silicate nanoclays. The rigid polyurethane foams were obtained in a laboratory scale, in a single step method, from a two-component system with a NCO to OH groups ratio equal to two. The reaction mixture consisted of the proper amounts of a commercial oligoetherpolyol, polyglycerol, catalysts, water,...
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Clickable polysaccharides for biomedical applications: A comprehensive review
PublikacjaRecent advances in materials science and engineering highlight the importance of designing sophisticated biomaterials with well-defined architectures and tunable properties for emerging biomedical applications. Click chemistry, a powerful method allowing specific and controllable bioorthogonal reactions, has revolutionized our ability to make complex molecular structures with a high level of specificity, selectivity, and yield...
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Thermal degradation of polylactic acid (PLA)/polyhydroxybutyrate (PHB) blends: A systematic review
PublikacjaPolylactic acid (PLA) and polyhydroxybutyrate (PHB) are two biopolyesters obtained from renewable resources like corn or sugar under bacterial fermentation. PLA is the most widely used biopolymer in diverse applications. Addition of PHB to PLA can improves the crystallinity of PLA, and thereby its mechanical strength. However, both PLA and PHB suffer from poor thermal stability, which limits their potential industrial application....
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Weldability of pipe grade polyethylenes as realized from thermal and mechanical properties assessments
PublikacjaSince polyethylene (PE) has been widely accepted for the production of high-pressure fluid conveying pipelines, studies devoted to weldability of PE connections were always of major importance. In this study, two industrial PE grades designed for pipe production, namely PE80 and PE100, were injection molded, cut, and then welded as PE100-PE100, PE100-PE80, and PE80-PE80. The heat-welded joints were assessed by differential scanning...
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Investigating the combined impact of plasticizer and shear force on the efficiency of low temperature reclaiming of ground tire rubber (GTR)
PublikacjaIn the present work, ground tire rubber (GTR) was mechano-chemically reclaimed at ambient temperature using two-roll mills. Road bitumen and styrene-butadiene-styrene (SBS)-modified bitumen at variable content (in range: 2.5–20 phr) were applied as reactive plasticizers to enhance reclaiming of GTR. For better understanding the plasticizing effect of bitumen on the quality of obtained reclaimed rubber, mechano-chemically reclaimed...
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Effect of high loading of titanium dioxide particles on the morphology and selected properties of natural rubber-based composites
PublikacjaThe aim of this work was to prepare and characterize the natural rubber vulcanizates contained different amounts of titanium dioxide particles. At first rubber mixture was prepared using a laboratory two-roll mill and then samples were vulcanized in a hydraulic press. The formulation of rubber mixture and rubber-processing technique is based on our earlier investigations. Materials were obtained at the different titanium dioxide...
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Characterization of volatile compounds, structural, thermal and physico-mechanical properties of cross-linked polyethylene foams degraded thermo-mechanically at variable times
PublikacjaWaste cross-linked polyethylene foam (wXLPE) was thermo-mechanically degraded at variable time using internal batch mixer. The progress of wXLPE degradation has been investigated by using a simultaneous thermogravimetric/differential scanning calorimetry analyzer coupled with Fourier transform infrared spectroscopy, swelling measurements, tensile tests and scanning electron microscopy. Volatile organic compounds generated during...
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Rheological characteristics of oligomeric semiproducts gained via chemical degradation of polyurethane foam using crude glycerin in the presence of different catalysts
PublikacjaPolyurethane (PU) recycling is a topic of growing interest due to the increasing amount of polyurethane waste. The main purpose of polyurethane chemical recycling is to recover the starting polyol. In this study, a method of polyurethane thermochemical recycling, glycerolysis by means of crude glycerin, is proposed. This work presents a comparative study of commercial catalysts used in order to accelerate the decomposition process,...
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Microwave radiation in the synthesis of urethane prepolymers
PublikacjaThis paper describes the use of microwave radiation in the synthesis of urethane prepolymers in bulk (without solvent). The prepolymers were synthesized using 1,6-hexamethylene diisocyanate (HDI) and poly (ε-caprolactone) diol (PCL) at a molar ratio of 4:1. The reaction was carried out without a catalyst in the reactor with a conventional heating system (oil bath) or in the microwave reactor (MW Reactor NOVA 09) at temperatures...
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Thermoplastic polyurethanes derived from petrochemical or renewable resources: A comprehensive review
PublikacjaThermoplastic polyurethanes (TPUs) materials are obtained by the reaction of polyol (ether-, ester-, and carbonate-based diols with average molecular weight in the range from 1,000 to 3,000 g/mol) with aliphatic or aromatic diisocyanates. Synthesized materials consist of the hard and soft segments which are separated in different level. All mechanical and thermal properties of TPUs depend on the chemical structure of used monomers,...
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Processing, physico-mechanical and thermal properties of reclaimed GTR and NBR/reclaimed GTR blends as function of various additives
PublikacjaIn this work, ground tire rubber (GTR) was mechano-chemically reclaimed in the presence of bitumen and various additives. During studies three types of processing and curing additives: (i) peptizer P300; (ii) vulcanization accelerator tetramethylthiuram disulfide (TMTD) and (iii) organic peroxide di(2-tert-butyl-peroxyisopropyl)benzene (BIB1) were applied to enhance reclaiming of GTR. Reclaiming process was evaluated by oscillating...
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A comparative study on selective properties of Kraft lignin–natural rubber composites containing different plasticizers
PublikacjaEffect of plasticizer type on the kraft lignin–nat- ural rubber composite microstructure and selected proper- ties was determined. The composites were prepared with addition of a commonly used naphthenic oil plasticizer to study the decomposition product of polyurethane (glyc- erolysate) and its characteristics. Kraft lignin powder was incorporated into the natural rubber matrix in amounts of 10 and 40 parts per 100 parts of natural...
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Elastic polyurethane foams containing graphene nanoplatelets
PublikacjaElastic polyurethane foams were produced from two-component polyurethane systems (SPECFLEX NE 113 izocyjanian/NR 816 poliol system—SPC and Elastic MBMarket company system POLYOL ET MB 500/ISO ET MB 800—ET) by using a one-step method. The foams were a graphene nanoplatelets (GNP) in the amount ranging from 1 to 2 wt.%. The effect of the nanofiller on polyurethane matrix was determined by analyzing the chemical structure, static...
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Structure and properties comparison of poly(ether-urethane)s based on nonpetrochemical and petrochemical polyols obtained by solvent free two-step method
PublikacjaThe application of thermoplastic polyurethanes (TPU) is becoming more and more extensive, and the decreasing of used petrochemical monomers and reduction of energy for the polymerization and processing processes is getting increasingly important. In this paper, we confirmed the positive influence of high bio-based monomers contents (by replacing petrochemical polyol and glycol by bio-based counterparts) on processing and properties...
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High-density polyethylene/EPDM rubber blend composites of boron compounds for neutron shielding application
PublikacjaNovel materials with neutron shielding property were fabricated by incorporating boron compounds into highdensity polyethylene (HDPE)/Ethylene propylene diene monomer rubber (EPDM) blends. A detailed investigation on the morphological, thermal, mechanical, and neutron attenuation properties of suitable proportion of HDPE/EPDM blend with boric acid (BA), boron carbide (BC), and nano boron carbide (NBC) were performed. Morphology...
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A comprehensive evaluation of flexible FDM/FFF 3D printing filament as a potential material in medical application
PublikacjaThe use of FDM/FFF in 3D printing for medical sciences is becoming common. This is due to the high availability and decent price of both 3D printers and filaments useful for FDM/FFF. Currently, researchers' attention is focused mainly on the study of medical filaments based on PLA, PCL or their modifications. This contributes to insufficient diversity of medical-grade filaments on the market. Moreover, due to the lack of specified...
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Assessment of the devulcanization process of EPDM waste from roofing systems by combined thermomechanical/microwave procedures
PublikacjaEthylene-propylene-diene rubber (EPDM) is a elastomer widely used in common industrial applications. EPDM can be shaped into sheets and employed as isolating material for roofing systems. In this study, scraps of EPDM from commercial, industrial and residential roofing systems were treated by combined thermo-mechanical and microwave devulcanization processes including peroxide of benzoyl (BPO). The devulcanized EPDM (Dev-EPDM)...
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Enhancement of PUR/PIR foam thermal stability after addition of Zostera marina biomass component investigated via thermal analysis and isoconversional kinetics
PublikacjaIn the present work, a thorough thermogravimetric (TG) analysis of bio-based polyurethane–polyisocyanurate (PUR–PIR) foams in both nitrogen and oxygen atmosphere is performed. A sustainable element of the foam is a biopolyol obtained via acid-catalyzed liquefaction of Zostera marina and Enteromorpha Algae biomass. Based on isoconversional analysis and apparent activation energies, several conclusions are obtained. In contradiction...
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Impedance spectroscopy studies on hybrid materials consisting of poly(3,4-ethylenedioxythiophene) and iron, cobalt and nickel hexacyanoferrate
PublikacjaBadania warstw polimeru pEDOT modyfikowanego heksacyjanożelazianami żelaza, kobaltu i niklu przeprowadzono za pomocą spektroskopii impedancyjnej (SI). Wykazano, że materiały hybrydowe charakteryzują się dobrą stabilnością. Warstwy testowano w zakresie temperatur od 283 do 313K. w kontakcie z wodnym roztworem KCl. Wysokie współczynniki dyfuzji wskazują na możliwości wykorzystania układów jako przewodników jonowych.
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Quantum dots in gas sensing a review
PublikacjaAir pollution becomes an increasing problem in the recent years. There is a need to develop more sensitive gas sensors. Much effort has been performed to develop different types of gas sensors, such as electrochemical sensors or polymer sensors. One of the most promising approaches to improve sensors performance is the application of the nanostructures as sensing materials. State of the art of quantum...
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Hydroliza enzymatyczna wybranych prób tłuszczów smażalniczych w obecności lipazy
PublikacjaWybrane próbki tłuszczów stosowanych do głębokiego smażenia w punktach gastronomicznych poddawano lipolizie in vitro w obecności lipazy trzustkowej. Tłuszcze te charakteryzowały się zróżnicowaną zawartością frakcji polarnej i spolimeryzowanych triacylogliceroli (TAG). Przebieg lipolizy kontrolowano metodą HPSEC. Stwierdzono, że tłuszcze ogrzewane ulegają lipolizie znacznie trudniej niż olej świeży. Najtrudniej ulegają lipolizie...
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Numerical model of human head phantom to ensure dosimetry of dose components for boron neutron capture therapy
PublikacjaExtremely important aspects of the boron neutron capture therapy are, first of all, administering to the patient a boron compound that selectively reaches the neoplastic cells, and in the second step, the verification of the irradiation process. This paper focuses on the latter aspect, which is the detailed dosimetry of the processes occurring after the reaction of thermal neutrons with the boron-10 isotope. The results of computer...
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Wytrzymałość połączeń poliuretanowo-stalowych otrzymanych z użyciem kleju cilbond
PublikacjaPrzedstawiono wyniki badań wytrzymałości na oddzieranie elementów warstwowych poliuretanowo-stalowych połączonych przy użyciu klejuCilbond 45SF. Stalowe płaskowniki o różnej chropowatości pokrywanoklejem Cilbond 45SF i wygrzewano w kilku przyjętych czasach i określonej temperaturze. Na płaskowniki ułożone w stalowej formie wylewano ciekły system poliuretanowy. Po zżelowwaniu polimeru, próbki warstwowe poddawano utwardzeniu w różnych...
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Fuzyjne polimerazy DNA – otrzymywanie, charakterystyka i zastosowanie
PublikacjaObecnie reakcje PCR (ang. Polymerase Chain Reaction) wykazują bardzo szerokie zastosowanie w diagnostyce medycznej, biologii molekularnej czy inżynierii genetycznej. Efektywność tych reakcji rozumiana jako wydajność i wierność przeprowadzonej amplifikacji jest nieodłącznie związana ze stosowaną polimerazą DNA i warunkami prowadzenia reakcji PCR. Aby sprostać wymaganiom stawianym przez nowoczesne metody diagnostyczne oraz współczesną...
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Badania spektroskopowe wybranych silanotiolanów metali o budowie polimerycznej
PublikacjaPodjęto próby otrzymania tri-tert-butoksysilanotiolanowych kompleksów niklu(II), kobaltu(II), cynku(II) i kadmu(II) o budowie polimerycznej mogących pełnić rolę prekursorów w syntezie materiałów funkcjonalnych. W tym celu przeprowadzono syntezy odpowiednich silanotiolanowych metali z grupą diamin alifatycznych. Otrzymano szereg nowych obojętnych polimerów koordynacyjnych o budowie przestrzennej typu 1D. Dla siedmiu z nich zostały...
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Influence of selected submicron inorganic particles on mechanical and thermo-mechanical properties of unsaturated polyester/glass composites
PublikacjaIn this paper, the influence of different submicron-scaled particles (zinc oxide, titanium dioxide, or silica) on mechanical and thermo-mechanical properties of unsaturated polyester matrix composites reinforced with glass fabric was investigated. Surface morphology of obtained composites was also examined. At first inorganic particles were mechanically dispersed into unsaturated polyester resin system as per the calculated weight...
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Experimental comparison of hydrodynamic thrust bearings with different pad surface materials
PublikacjaBabbitt is the material most frequently used as the pad surface material for hydrodynamic bearings operating at usual operating conditions. It shows many advantages important for safe bearing operation, as for example: low friction coefficient, corrosion resistance, fair mechanical properties and outstanding conformability. On the other hand, it is not free from disadvantages, such as limited fatigue strength or limited resistance...