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Performance tuning of chitosan-based membranes by protonated 2-Pyrrolidone-5-carboxylic acid-sulfolane DES for effective water/ethanol separation by pervaporation
PublikacjaToday, the applicability of deep eutectic solvents (DES) in various fields, including membrane science and technology, is extensively investigated. In pioneering works, we have implemented different DES as a component of chitosan (CS)-based flat membranes for pervaporation (PV) separation. Herein, we present a new protonated (by sulphuric acid) 2-Pyrrolidone-5-carboxylic acid: sulfolane DES, as a green additive for its chemical...
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Method development and validation for optimized separation of quercetin derivatives in selected Potentilla species using high-performance thin-layer chromatography photodensitometry method
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Nowe metodyki oznaczania dodatków do paliw z zastosowaniem rozdzielenia wielopomiarowego = New procedures for fuel additives determination by multidimensional separation systems
PublikacjaW pracy przedstawiono wyniki badań nad opracowaniem metodyki oznaczania wybranych dodatków "myjących" w paliwie diesla. Porównano metodyki jednoetapowe z wykorzystaniem chromatografii gazowej z detektorem płomieniowo-jonizacyjnym (GC-FID) lub spektrometrem mas (GC-MS) oraz wysokosprawnej chromatografii cieczowej z detektorem UV z matrycą fotodiodową (HPLC-UV-DAD), z metodykami dwuetapowymi, w których do wstępnej izolacji składników...
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Distinction of clenbuterol intake from drug or contaminated food of animal origin in a controlled administration trial – the potential of enantiomeric separation for doping control analysis
PublikacjaThe differentiation of clenbuterol abuse and unintentional ingestion by contaminated meat is crucial with respect to the valuation of an adverse analytical finding in human sports doping control. The proportion of the two enantiomers of clenbuterol may serve as potential discriminating parameter. For the determination of the individual enantiomers, specific methods were developed and validated for the different matrices under investigation...
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Optimal conditions of ramentaceone and plumbagin separation and isolation from carnivorous plants extracts using reverse phase-high performance liquid chromatography (RP-HPLC)
PublikacjaPreparatywna chromatografia cieczowa jest szczególnie przydatną techniką do rozdzielania i izolacji użytecznych ilości substancji z różnych skomplikowanych mieszanin. Praca prezentuje optymalne warunki rozdzielania i izolacji ramentaceonu i plumbaginy uwzględniając maksymalną selektywność rozdzielania naftochinonów od substancji balastowych z chloroformowych ekstraktów roślinnych D. aliciae i D. capensis z zastosowaniem techniki...
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Optimal conditions of ramentaceone and plumbagin separation and isolation from carnivorous plants extracts using normal phase-high performance liquid chromatography (NP-HPLC)
PublikacjaPraca prezentuje optymalne warunki rozdzielania i izolacji plumbaginy i ramentacenu z matrycy analitycznej, którą stanowią chloroformowe ekstrakty z roślin D.aliciae i D.capensis z wykorzystaiem techniki NP-HPLC. Skład eluentu dla żelu krzemionkowego jako fazy stacjonarnej był optymalizowany. Zostały przedstawione optymalne warunki powiększania skali procesu izolacji badanych metabolitów z ekstrakrów roślinnych. Określono również...
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Automatic music genre classification based on musical instrument track separation / Automatyczna klasyfikacja gatunku muzycznego wykorzystująca algorytm separacji dźwięku instrumentó muzycznych
PublikacjaThe aim of this article is to investigate whether separating music tracks at the pre-processing phase and extending feature vector by parameters related to the specific musical instruments that are characteristic for the given musical genre allow for efficient automatic musical genre classification in case of database containing thousands of music excerpts and a dozen of genres. Results of extensive experiments show that the approach...
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Rapid and Green Separation of Mono- and Diesters of Monochloropropanediols by Ultrahigh Performance Supercritical Fluid Chromatography–Mass Spectrometry Using Neat Carbon Dioxide as a Mobile Phase
PublikacjaThis study demonstrates the effect of column selectivity and density of supercritical carbon dioxide (SC-CO2) on the separation of monochloropropanediol (MCPD) esters, known as food toxicants, using SC-CO2 without addition of cosolvent in ultrahigh performance supercritical fluid chromatography–mass spectrometry (UHPSFC-MS). This study shows that over 20 2-monochloropropanediol (2-MCPD) and 3-monochloropropanediol (3-MCPD) mono-...
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NUMERICAL SIMULATIONS OF GAP FLOW ABOVE ROTATING DISK
PublikacjaA rotating disk can be considered a basic configuration for the investigati ons of the impact of various conditions on the flow through the clearance between the s hrouded turbine blade and the casing. Numerical calculations using Fine/Turbo Numeca were conducted to examine the influence of the rotational velocity and the pressure differ ence across the disk on the flow conditions, especially the mass flow through the clearance....
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Viral infection-oxidative stress/DNA damage-aberrant DNA methylation: separate or interrelated events responsible for genetic instability and childhood ALL development?
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Ruch wirowy wywoływany przez ultradźwięk w płynach z relaksacją
PublikacjaRozprawa doktorska poświęcona jest badaniu ruchu wirowego wywoływanego przez ultradźwięk w różnych modelach płynów z relaksacją. Ma ona charakter teoretyczny, jednak wykorzystanie uzyskanych dzięki niej wyników może przynieść lepsze zrozumienie ruchu wirowego wywoływanego przez siłę akustyczną. W I rozdziale rozprawy przedstawione zostały ogólne rozważania dotyczące akustyki nieliniowej. Rozdział II dotyczy ruchu wirowego wywoływanego...
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Evaluation of the suitability of low hazard surfactants for the separation of phenols and carotenoids from red-flesh orange juice and olive mill wastewater using cloud point extraction
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Problems of collisions between adjacent steel structures under earthquake excitation
PublikacjaNowadays, the high level of urbanization forces the designers to design closely-separated structures and to take into account many factors influencing the response of these structures, which may collide due to insufficient separation distance during moderate to strong ground motions. Recent observations as well as numerical and experimental investigations have confirmed that the interactions between structures may lead to significant...
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Application of additional factors supporting the microextraction process
PublikacjaDue to the fact that green analytical chemistry is of high importance, the past two decades have witnessed a rapid growth in the sample preparation area with special emphasis on simplification, miniaturization and automation of extraction procedures. In addition, to accelerate the extraction processes and to improve the separation of analytes, several enhanced parameters are applied. These factors include, ultrasounds, microwaves,...
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Can unequal distributions of wealth influence vote choice? A comparative study of Germany, Sweden and the United States.
PublikacjaIt is widely accepted that income influences voting behavior. Does wealth? Is the effect similar across countries? Studies of wealth and voting behavior have not existed until recently, in part because of the absence of data on wealth holdings. The findings in this chapter indicate that wealth is related to voting behavior in some countries but not in others. The chapter models the effects of wealth on one form of voting behavior,...
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Fast collaborative graph exploration
PublikacjaWe study the following scenario of online graph exploration. A team of k agents is initially located at a distinguished vertex r of an undirected graph. At every time step, each agent can traverse an edge of the graph. All vertices have unique identifiers, and upon entering a vertex, an agent obtains the list of identifiers of all its neighbors. We ask how many time steps are required to complete exploration, i.e., to make sure...
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Fast Collaborative Graph Exploration
PublikacjaWe study the following scenario of online graph exploration. A team of k agents is initially located at a distinguished vertex r of an undirected graph. At every time step, each agent can traverse an edge of the graph. All vertices have unique identifiers, and upon entering a vertex, an agent obtains the list of identifiers of all its neighbors. We ask how many time steps are required to complete exploration, i.e., to make sure...
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The role of solvent solubility parameters in the formation of intermittent low and high molecular weight polystyrene rich structures in a thin film resulting from water vapor induced phase separation
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Food Bioactive Ingredients Processing Using Membrane Distillation
PublikacjaSeparation processes are an important part of today’s food industries, especially in the case of specific bioactive components due to their health benefits. In general, processing of bioactive food ingredients assumes the introduction of integrated system directed to their separation, fractionation, and recovery. Recently, membrane distillation (MD) has been considered as an alternative membrane-based separation and concentration...
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In uence of Low-Level Features Extracted from Rhythmic and Harmonic Sections on Music Genre Classi cation
PublikacjaWe present a comprehensive evaluation of the infuence of 'harmonic' and rhythmic sections contained in an audio file on automatic music genre classi cation. The study is performed using the ISMIS database composed of music files, which are represented by vectors of acoustic parameters describing low-level music features. Non-negative Matrix Factorization serves for blind separation of instrument components. Rhythmic components...
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PROBLEMS OF COLLISIONS BETWEEN ADJACENT STEEL STRUCTURES UNDER EARTHQUAKE EXCITATION
PublikacjaNowadays, the high level of urbanization forces the engineers to design closely-separated structures and to take into account many factors influencing their response, including collisions between them due to insufficient separation distance during moderate to strong ground motions. Recent observations as well as experimental and numerical investigations have confirmed that interactions...
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A note on polynomial algorithm for cost coloring of bipartite graphs with Δ ≤ 4
PublikacjaIn the note we consider vertex coloring of a graph in which each color has an associated cost which is incurred each time the color is assigned to a vertex. The cost of coloring is the sum of costs incurred at each vertex. We show that the minimum cost coloring problem for n-vertex bipartite graph of degree ∆≤4 can be solved in O(n^2) time. This extends Jansen’s result [K.Jansen,The optimum cost chromatic partition problem, in:...
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Ion Chromatography in Environmental Analysis of Selected Organic Acids
PublikacjaLow molecular mass carboxylic acids (LCAs) occur in many environmental compartments dueto natural processes and human activity. When volatile and nonvolatile acids are to be monitored then liquidchromatography, including ion chromatography seems a method of choice. At high pH the acids are inionized form and can be separated as carboxylats by means of anion exchange chromatography. LCAs canalso be separated at low pH by ion exclusion...
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Separation and determination of ciprofloxacin in seawater, human blood plasma and tablet samples using molecularly imprinted polymer pipette‐tip solid phase extraction and its optimization by response surface methodology
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Distributed graph searching with a sense of direction
PublikacjaIn this work we consider the edge searching problem for vertex-weighted graphs with arbitrarily fast and invisible fugitive. The weight function w provides for each vertex v the minimum number of searchers required to guard v, i.e., the fugitive may not pass through v without being detected only if at least w(v) searchers are present at v. This problem is a generalization of the classical edge searching problem, in which one has...
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Membrane distillation assisting food production processes of thermally sensitive food liquid items: a review
PublikacjaPhysical separation technologies have become important tool for processing in the current food manufacturing industries, especially for the products containing bioactive compounds thanks to their health benefits in costumers. As for the processing of bioactive food ingredients implies the implementation of integrated systems oriented to their separation, fractionation, and recovery. In this field, membrane distillation (MD), which...
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The Application of 2,6-Bis(4-Methoxybenzoyl)-Diaminopyridine in Solvent Extraction and Polymer Membrane Separation for the Recovery of Au(III), Ag(I), Pd(II) and Pt(II) Ions from Aqueous Solutions
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Efficient, fast, simple, and eco-friendly methods for separation of toxic chromium(VI) ions based on ion exchangers and polymer materials impregnated with Cyphos IL 101, Cyphos IL 104, or D2EHPA
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MINERAL MATTER IN MUNICIPAL SOLID WASTE
PublikacjaMunicipal solid waste (MSW) contains mineral materials which are seldom considered as a potential resource. Currently, the waste management sector pays attention to recyclable parts, biodegradable material, waste-to-energy fraction, and residues after waste reuse and recycle. In contrast, this study focus as on the mineral matter in MSW. The aim was to analyze and discuss the sources of mineral matter in MSW, the impact which the...
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Design of Inner Gate for CRIST Shipyard Dry Dock
PublikacjaThe paper deals with a removable steel inner gate which was designed to separate two parts of a dry dock of about 70 m in width and 380 m in length. The gate allows for independent assembly of ship structures in two separated parts of the dock. The fore part of the dock can be flooded while the after part is dry. Tthe gate was designed by IDEK Company Ltd in 2011 and it was soon constructed and used by CRIST Shipyard in Gdynia.
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On-line ranking of split graphs
PublikacjaA vertex ranking of a graph G is an assignment of positive integers (colors) to the vertices of G such that each path connecting two vertices of the same color contains a vertex of a higher color. Our main goal is to find a vertex ranking using as few colors as possible. Considering on-line algorithms for vertex ranking of split graphs, we prove that the worst case ratio of the number of colors used by any on-line ranking algorithm...
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New Molecular Markers Involved in Regulation of Ovarian Granulosa Cell Morphogenesis, Development and Differentiation during Short-Term Primary In Vitro Culture—Transcriptomic and Histochemical Study Based on Ovaries and Individual Separated Follicles
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Zastosowanie trendów przełącznikowych w analizie płac realnych w Polsce
PublikacjaStreszczenie W początkowej części artykułu zostały przedstawione i omówione informacje o poziomie miesięcznych nominalnych płac (WN) oraz indeksie cen dóbr konsumpcyjnych (ICK) w gospodarce polskiej w latach 1995-2015. Następnie opisano poziomy realnych płac (W) wyrażone w cenach roku 2015. Na bazie tych informacji przedstawiono i przedyskutowano zagadnienia dotyczące rocznych przyrostów płac realnych oraz ich rocznych stóp wzrostu....
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On trees with double domination number equal to 2-domination number plus one
PublikacjaA vertex of a graph is said to dominate itself and all of its neighbors. A subset D subseteq V(G) is a 2-dominating set of G if every vertex of V(G)D is dominated by at least two vertices of D, while it is a double dominating set of G if every vertex of G is dominated by at least two vertices of D. The 2-domination (double domination, respectively) number of a graph G is the minimum cardinality of a 2-dominating (double dominating,...
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On trees with double domination number equal to total domination number plus one
PublikacjaA total dominating set of a graph G is a set D of vertices of G such that every vertex of G has a neighbor in D. A vertex of a graph is said to dominate itself and all of its neighbors. A double dominating set of a graph G is a set D of vertices of G such that every vertex of G is dominated by at least two vertices of D. The total (double, respectively) domination number of a graph G is the minimum cardinality of a total (double,...
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Chemical, thermal and laser processes in recycling of photovoltaic silicon solar cells and modules
PublikacjaIn recent years, photovoltaic power generation systems have been gaining unprecedented attention as an environmentally beneficial method to solve the energy problem. From the economic point of view the pure silicon, which can be recapture from the used cells, is the most important material due to its cost and shortage. In the paper selected methods of used or damaged module and cells recycling and experimental results are presented....
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Solid-State Modification of Poly(butylene terephthalate) with a Bio-Based Fatty Acid Dimer Diol Furnishing Copolyesters with Unique Morphologies
PublikacjaCopolyesters based on poly(butylene terephthalate) (PBT) and a bio-based fatty acid dimer diol (FADD) were prepared by solid-state modification (SSM). The chemical incorporation of the FADD into the backbone of the PBT was proven using various techniques. It was clear that the incorporation rate was diffusion-limited rather than reaction-limited. From quantitative 13C NMR a nonrandom chemical microstructure was obtained at all...
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Domination-Related Parameters in Rooted Product Graphs
PublikacjaAbstract A set S of vertices of a graph G is a dominating set in G if every vertex outside of S is adjacent to at least one vertex belonging to S. A domination parameter of G is related to those sets of vertices of a graph satisfying some domination property together with other conditions on the vertices of G. Here, we investigate several domination-related parameters in rooted product graphs.
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On extremal sizes of locally k-tree graphs
PublikacjaA graph G is a locally k-tree graph if for any vertex v the subgraph induced by the neighbours of v is a k-tree, k>=0, where 0-tree is an edgeless graph, 1-tree is a tree. We characterize the minimum-size locally k-trees with n vertices. The minimum-size connected locally k-trees are simply (k + 1)-trees. For k >= 1, we construct locally k-trees which are maximal with respect to the spanning subgraph relation. Consequently, the...
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Some Progress on Total Bondage in Graphs
PublikacjaThe total bondage number b_t(G) of a graph G with no isolated vertex is the cardinality of a smallest set of edges E'⊆E(G) for which (1) G−E' has no isolated vertex, and (2) γ_t(G−E')>γ_t(G). We improve some results on the total bondage number of a graph and give a constructive characterization of a certain class of trees achieving the upper bound on the total bondage number.
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On the partition dimension of trees
PublikacjaGiven an ordered partition Π={P1,P2,…,Pt} of the vertex set V of a connected graph G=(V,E), the partition representation of a vertex v∈V with respect to the partition Π is the vector r(v|Π)=(d(v,P1),d(v,P2),…,d(v,Pt)), where d(v,Pi) represents the distance between the vertex vv and the set Pi. A partition Π of V is a resolving partition of G if different vertices of G have different partition representations, i.e., for every...
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Analysis of unsteady flow forces on the thermowell of steam temperature sensor
PublikacjaIn this paper, 3D numerical analysis of unsteady flow forces acting on the measuring sheath of steam temperature is presented. According to that purpose, the CFD (Computation Fluid Dynamic [1]) approach has been used. The nonstationary of fluid acting on the measuring sheath such as: Strouhal frequency, amplitude of pressure, structure of vortex, peak of pressure, field of pressure, field of velocity etc. are studied analytically...
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Zastosowanie addytywów w separacji pianowej białek serwatkowych i białek mlecznych
PublikacjaZaproponowano proces separacji pianowej do wydzielania białek ze strumieni poprodukcyjnych przemysłu mleczarskiego Ponadto zaproponowano zastosowanie w separacji pianowej białek serwatkowych i mlecznych addytywów dopuszczonych ustawą do stosowania w żywności. Jako cel pracy przyjęto uzyskanie wyników uzasadniających wybór takich addytywów, które intensyfikują przebieg i polepszają wynik procesu separacji pianowej białek. W części...
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Możliwości zamiany elektrycznych przepływomierzy powietrza stosowanych w silnikach spalinowych samochodów
PublikacjaW artykule przedstawiono podstawowe typy przepływomierzy powietrza, stosowane w silnikach spalinowych samochodów: z klapąspiętrzającą, HLM, HFM, Vortex i MAP. Przedstawiono wyniki badania tych przepływomierzy na specjalnie przygotowanym stanowisku pomiarowym. Przeanalizowano możliwość ich zamiany i zweryfikowano taką możliwość w praktyce.
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Syntactic modular decomposition of large ontologies with relational database
PublikacjaSupport for modularity allows complex ontologies to be separated into smaller pieces (modules) that are easier to maintain and compute. Instead of considering the entire complex ontology, users may benefit more by starting from a problem-specific set of concepts (signature of problem) from the ontology and exploring its surrounding logical modules. Additionally, an ontology modularization mechanism allows for the splitting up of...
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On trees with double domination number equal to 2-outer-independent domination number plus one
PublikacjaA vertex of a graph is said to dominate itself and all of its neighbors. A double dominating set of a graph G is a set D of vertices of G such that every vertex of G is dominated by at least two vertices of D. The double domination number of a graph G is the minimum cardinality of a double dominating set of G. For a graph G=(V,E), a subset D subseteq V(G) is a 2-dominating set if every vertex of V(G)D has at least two neighbors...
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Derecho Evolving from a Mesocyclone—A Study of 11 August 2017 Severe Weather Outbreak in Poland: Event Analysis and High-Resolution Simulation
PublikacjaThis study documents atmospheric conditions, development, and evolution of a severe weather outbreak that occurred on 11 August 2017 in Poland. The emphasis is on analyzing system morphology and highlighting the importance of a mesovortex in producing the most significant wind damages. A derecho-producing mesoscale convective system (MCS) had a remarkable intensity and was one of the most impactful convective storms in the history...
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The nonlinear effects of sound in a liquid with relaxation losses
PublikacjaThe nonlinear effects of sound in electrolyte with a chemical reaction are examined. The dynamic equations that govern non-wave modes in the field of intense sound are derived, and acoustic forces of vortex, entropy, and relaxation modes are determined in the cases of low-frequency sound and high-frequency sound. The difference in the nonlinear effects of sound in electrolyte and in a gas with excited vibrational degrees of molecules,...
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Electronic Voting: 8th International Joint Conference, E-Vote-ID 2023, Luxembourg City, Luxembourg, October 3–6, 2023, Proceedings
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Electronic Voting: 8th International Joint Conference, E-Vote-ID 2023, Luxembourg City, Luxembourg, October 3–6, 2023, Proceedings
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