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Wyniki wyszukiwania dla: studnie
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Studies on the complex formation between lactams and thiolactams of sparteine with copper(II) cation
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Kinetic and equilibrium studies of the reaction of 2,4-dinitrophenyl-2,4,6-trinitrophenylmethane with cryptands in acetonitrile
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Studies of the complex formation between some proton sponges and Cu(II) cations
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A facile synthesis method and electrochemical studies of a hierarchical structured MoS2/C-nanocomposite
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Synthesis, spectroscopy and computational studies of some biologically important hydroxyhaloquinolines and their novel derivatives
PublikacjaA series crystalline compounds of methyl and phosphinyl derivatives of 2-methylquinolin-8-ol (1a) and related 5,7-dichloro-2-methylquinolin-8-ol (1b) were quantitatively prepared and characterized by microanalysis, IR, UV-vis and multinuclear NMR spectroscopy. Five of them have been characterized by single crystal X-ray diffraction method. The known compounds, 8-methoxy-2-methylquinoline (2a) and 8-methoxyquinoline (2d), were synthesised...
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Threshold photoelectron studies of isoxazole over the energy range 9.9-30 eV
PublikacjaThe threshold photoelectron spectrum of the isoxazole molecule, C3H3NO has been measured over the photon energy range 9.9-30 eV with the use of synchrotron radiation. In the 9.9-10.8 eV range, corresponding to photoionization from the highest occupied molecular orbital 3a"(π3), seven well resolved vibrational series have been observed and their modes are tentatively assigned. A strong adiabatic ionization, with an energy of 11.132...
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Anion recognition by phosphonium calix[4]arens: synthesis and physico-chemical studies
Publikacjap-tert-butylcalix[4]arenes in the cone conformation, di-and tetra substituted at the narrow rim with charged phosphonium groups have been synthesies and characterised.
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Studies on the influence of technological variants of finishing machining on flow of parts in flexible manufacturing
PublikacjaIn the article below the problems of influence of variants of finishing processing on flow of machining parts in flexible manufacturing system were presented. The investigations were carried out the technological processes for piston rods and rams of hydraulic cylinders. There were also presented model variants of technological processes for piston rods finished with the burnishing. In these studies the influence of technological...
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Synthesis, spectroscopy and computational studies of some novelphosphorylated derivatives of quinoline-5,8-diones
PublikacjaThe neutral phosphorus nucleophiles such as R2P(=Y)M allowed the radical addition to 2-methyl-5,8-dioxo-5,8-dihydroquinoline-7-amine and N-(2-methyl-5,8-dioxo-5,8-dihydroquinolin-7-yl)acetamide giving exclusively O-phosphorylated products. All products were quantitatively prepared and characterized by microanalysis, and multinuclear NMR spectroscopy. Seven of them, have been characterized by single crystal X-ray diffraction method....
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Guided wave propagation in structures. Modelling, experimental studies and application to damage detection
PublikacjaCelem niniejszej pracy są eksperymentalne i numeryczne analizy propagacji prowadzonych fal sprężystych w stalowych konstrukcjach prętowych, belkowych, ramowych, tarczowych i płytowych. W szczególności praca poświęcona jest: (a) modelowaniu propagacji fal z uwzględnieniem zjawiska dyspersji; (b) budowie modeli obliczeniowych w formalizmie metody elementów spektralnych; (c) eksperymentalnej weryfikacji zaproponowanych modeli; (d)...
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SEM and TEM Studies on <i>In-Situ</i> Cast Al–TiC Composites
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Nanostructured Lipid Carriers Engineered as Topical Delivery of Etodolac: Optimization and Cytotoxicity Studies
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Identification of yellow luminescence centers in Be-doped GaN through pressure-dependent studies
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X-ray and NMR structural studies of the series of porphyrazines with peripheral pyrrolyl groups
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Selection of reliable reference genes in eutopic and ectopic endometrium for quantitative expression studies
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Femtosecond studies of the excited-state dynamics of ester-alkyloxy substituted zinc phthalocyanines
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Control Theory Education in the Distance Education B.Eng. Studies at Warsaw University of Technology
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Synthesis, biological activity and molecular modelling studies of tricyclic alkylimidazo-, pyrimido- and diazepinopurinediones
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Crystallographic and spectroscopic studies of 5-arylidene-2-amino-imidazol-4-ones
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Studies of human and veterinary drugs' fate in environmental solid samples- analytical problems.
PublikacjaW różnych ośrodkach naukowych na całym świecie trwają prace nad poznaniem losu środowiskowego zanieczyszczeń z grupy farmaceutyków. Obecność pozostałości farmaceutycznych w poszczególnych elementach środowiska stanowi nowe wyzwanie zarówno z punktu widzenia technologii oczyszczania wód i ścieków jak i analityków, których zadaniem jest opracowanie nowych metodyk analitycznych. W publikacji przedstawiono problemy z jakimi stykają...
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Experimental and numerical studies of guided wave damage detection in bars with structural discontinuities
PublikacjaPraca dotyczy analizy propagacji fal podłużnych i poprzecznych w elementach prętowych z nieciągłościami strukturalnymi. Symulacje numeryczne przeprowadzone przy zastosowaniu metody elementów spektralnych zostały porównane z wynikami badań eksperymentalnych dla pręta w stanie nienaruszonym oraz dla prętów z rysą, spawem oraz dodatkową masą.
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Mechanical, Structural and Diffusion Studies of Hydrogel Polyurethane Nanocomposites Containing Modified Montmorillonite
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Performance of Particle Oxidation Catalyst and Particle Formation Studies with Sulphur Containing Fuels
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Experimental and theoretical studies on the Sulfamethazine-Urea and Sulfamethizole-Urea solid-liquid equilibria
PublikacjaThe miscibility of active pharmaceutical ingredients with excipients is an important aspect in pharmaceutical technology protocols. In this study, the differential scanning calorimetry (DSC) was used for Sulfamethazine-Urea (SI–U) and Sulfamethizole-Urea (SO–U) solid-liquid phase diagrams determination. Both sulfonamides form simple binary eutectics with Urea. The lack of new co-crystal phase formation was confirmed by inspection...
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In Search of Panacea—Review of Recent Studies Concerning Nature-Derived Anticancer Agents
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Cooperation areas between universities and industry - case studies in the area of civil engineering
PublikacjaThe paper describes the areas of cooperation between universities and industry in the area of civil engineering. Presented examples are related to didactics, research grants and commissioned works. On the basis of the authors own experiences the mutual benefits of cooperation in different areas are described. As well as the assessment criteria of the areas of cooperation by the scientific community. The first area of cooperation...
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Polyurethane Nanocomposites Containing Reduced Graphene Oxide, FTIR, Raman, and XRD Studies
PublikacjaRecently, graphene and other graphene-based materials have become an essential part of composite science and technology. Their unique properties are not only restricted to graphene but also shared with derivative compounds like graphene oxide, reduced graphene oxide, functionalized graphene, and so forth. One of the most structurally important materials, graphene oxide (GO), is prepared by the oxidation of graphite. Though removal...
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The role of case studies and management experience in the education and personal developement of IT project managers
PublikacjaThe purpose of this article is to indicate the need for project management experience and knowledge in order to improve the competence of IT project managers. In the first part of the article there is shown the impact of experience on the development of project management skills. Also the need for having historical data about the projects - in order to make better project decisions - is shown in the article.In the following parts...
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Application of chemometric approach in studies of dew chemistry (on the basis of samples collected in Poland)
PublikacjaPrzedstawiono wyniki badań wybranych związków chemicznych (aniony, kationy, formaldehyd, nadtlenek wodoru, suma fenoli, TC, TIC, TOC) oznaczonych w próbkach rosy zebranych z różnych obszarów na terenie Polski (Gdynia, Gdańsk, Sopot, Mława, Kraków). Zastosowano analizę funkcji dyskryminacyjnej aby dokonać klasyfikacji poszczególnych próbek w zależności od miejsca pobierania oraz wykryć podstawowe zależności pomiędzy poszczególnymi...
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Spectroscopic studies of sol-gel derived thin film structures for integrated optics
PublikacjaPrzedstawiono wyniki badania struktur cienkowarstwowych wykonywanych dla zastosowań w optyce zintegrowanej z polimerów hybrydowych (np. w postaci ścieżek śwaitłowodów planarnych). Jakość i jednorodność stuktur badano za pomocą mikroskopii ramanowskiej, mikroskopii optycznej i profilometrii światła białego. Wykonano porównanie wyników uzyskanych tymi trzema metodami.
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The crystal and solution studies of glucosamine-6-phosphate synthase from Candida albicans
PublikacjaOkreślono strukturę krystaliczną domeny izomerazowej syntazy glukozamino-6-fosforanu z Candida albicans w stanie natywnym, oraz w kompleksie z inhibitorem allosterycznym UDP-GlcNAc, fruktozo-6-P, glukozo-6-P oraz analogiem stanu przejściowego reakcji enzymatycznej - 2-amino-2-deoksy-D-mannitolo-6-P (ADMP). Na podstawie wyników badań metodą niskokątowego rozpraszania promieni X (SAXS) wydedukowano przypuszczalną strukturę kompletnej...
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Experimental studies on specific cutting resistance while cuttingwith narrow-kerf saws
PublikacjaBadania eksperymentalne właściwego oporu skrawania zostały wymuszone poprzez pojawienie się nowych technologii przecinania za pomocą cienkich pił. W przeprowadzonym eksperymencie wartościami wejściowymi były: rozwarcie całkowite ostrzy (rzaz), posuw na ostrze oraz grubość brzeszczotu piły. W ten sposób, oprócz zmian całkowitego przekroju warstwy skrawanej uwzględniano również wpływ warunków tarcia pomiędzy brzeszczotem piły, ścianami...
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Innovative e-learning approach in teaching based on case studies - Innocase project
PublikacjaThe article presents the application of innovative e-learning approach for the creation of case study content. Case study methodology is becoming more and more widely applied in modern education, especially in business and management field. Although case study methodology is quite well recognized and used in education, there are still few examples of developing e-learning content on the basis of case studies. This task is to be...
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The influence of the substrate temperature on the preparation of DNA films for studies under vacuum conditions
PublikacjaPrzeanalizowano wpływ temperatury na formowanie warstw DNA. Sprawdzono wpływ stabilizatorów na jakość otrzymanych próbek. Stwierdzono, że optymalnymi warunkami przygotowywania filmów do badań w warunkach próżniowych jest - 10 st. C przy minimalnej zawartości NaOH.
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Mechanical, structural and diffusion studies of hydrogel polyurethane nanocomposites containing modified montmorillonite
PublikacjaW pracy zaprezentowano wyniki badań hydrożeli poliuretanowych zawierających poli(tlenek etylenu) oraz montmorylonit. Otrzymane układy scharakteryzowano z użyciem technik XRD, DMA, badań mechanicznych oraz wyznaczono chłonność wody i parametry dyfuzji.
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Edible Flowers Extracts as a Source of Bioactive Compounds with Antioxidant Properties—In Vitro Studies
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New supervised alignment method as a preprocessing tool for chromatographic data in metabolomic studies
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Experimental and theoretical studies of the spectroscopic properties of simple symmetrically substituted diphenylacetylene derivatives
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Conformational studies of cyclic enkephalin analogues withL- orD-proline in position 3
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Spectroscopic and magnetic studies of highly dispersible superparamagnetic silica coated magnetite nanoparticles
PublikacjaSuperparamagnetic behavior in aqueously well dispersible magnetite core-shell Fe3O4@SiO2 nanoparticles is presented. The magnetic properties of core-shell nanoparticles were measured with use of the DC, AC magnetometry and EPR spectroscopy. Particles were characterized by HR-TEM and Raman spectroscopy, showing a crystalline magnetic core of 11.5 ± 0.12 nm and an amorphous silica shell of 22 ± 1.5 nm in thickness. The DC, AC magnetic...
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Local Mesh Deformation for accelerated parametric studies based on the Finite Element Method
PublikacjaThis paper presents an approach for enhancing the efficiency of two-dimensional Finite Element Method analysis in parametric studies or optimisation process of microwave components. The new approach involves local mesh deformation applied near the elements that are modified during computations. Since in the proposed approach the topology of the mesh remains unchanged, a new mesh does not have to be generated from scratch when the...
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Anion binding by p-aminoazobenzene-derived aromatic amides: spectroscopic and electrochemical studies
PublikacjaThe synthesis and complexing properties of p-aminoazobenzene-derived mono-, bis-, and trisamides were described. Ligands 3 and 4 bind anions, including fluorides, chlorides, bromides, acetates, benzoates, dihydrogen phosphates, hydrogen sulfates, and p-toluenesulfonates, in chloroform forming 1 : 1 complexes. The highest value of stability constant was evaluated for the 4-F− complex (log K = 5.63 ± 0.21). On the basis of 1H NMR,...
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Seven Different Lighting Conditions in Photogrammetric Studies of a 3D Urban Mock-Up
PublikacjaOne of the most important elements during photogrammetric studies is the appropriate lighting of the object or area under investigation. Nevertheless, the concept of “adequate lighting” is relative. Therefore, we have attempted, based on experimental proof of concept (technology readiness level—TRL3), to verify the impact of various types of lighting emitted by LED light sources for scene illumination and their direct influence...
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The interaction of the pulsed laser irradiation with titania nanotubes - Theoretical studies on the thermal effect
PublikacjaThis paper reports temperature dispersion simulations of titania nanotubes irradiated by the 355 nm, pulsed, nanosecond laser. The modelling with the use of Finite Elements Method concerns titania nanotubes of the length and the wall thickness in the range of 0.5–2 μm and 5–20 nm, respectively. The uniqueness of the morphology was preserved by ensuring the wall thickness variation along the height of the tube, which was determined...
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Mini-Cave Automatic Virtual Environment Application in Security, Safety, and Defence Studies
PublikacjaThe aim of the article is to analyse the use of mini-Cave Automatic Virtual Reality Environment (mini-CAVE) in academic studies on security, safety, and defence. The literature review based on Web of Science database and the case study of the War Studies University research activities indicated the mini-CAVE can be used in two areas as a research infrastructure and as a didactic tool. It can be concluded that due to the development...
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Ultrastructural analysis of the submandibular sialoliths: Raman spectroscopy and electron back-scatter studies
PublikacjaThe aim of work was the epidemiological analysis of the occurrence of sialolithiasis of the submandibular gland in adults and the evaluation of the ultrastructure of salivary stones. The study sample consisted of 44 sialoliths. Analysis of the structure and chemical composition of sialoliths was performed using a Scanning Electron Microscope and Raman Spectroscopy. Comparing our results with the literature we can say that the epidemiology...
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Recent Applications of 1D GC-MS and 2D GC-MS in Foodomics Studies
PublikacjaGas chromatography coupled with mass spectrometry and food chemistry have been tightly linked since the 1960s. This setup is also an integral part of the omics studies when it comes to low mass metabolites. Therefore, the marriage of GC-MS and foodomics is obvious. Two-dimensional gas chromatography coupled with mass spectrometry fits perfectly within the latest trends in foodomics, since it is tailored for holistic food analysis....
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Effect of Ethanol Extracts of Propolis (EEPs) against Staphylococcal Biofilm—Microscopic Studies
PublikacjaStaphylococci growing in the form of biofilm exhibit high resistance to a plethora of antibiotics. The aim of the study was to assess the influence of ethanolic extract of propolis (EEPs) on S. epidermidis ATCC 35984 biofilm using fluorescent microscopy. Propidium iodide (PI) and SYTO 9 were used for differentiation of live and dead cells, and calcofluor white was used to stain the extracellular matrix, the self-produced extracellular...
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Comparative studies of the Acinetobacter genus and the species identification method based on the recA sequences
PublikacjaZaproponowano metodę genotypowania bakterii rodzaju Acinetobacter, opartą o analizę sekwencji genów recA, amplifikację fragmentów genu recA i analizę profili fragmentów restrykcyjnych po cięciu produktów reakcji PCR enzymami restrykcyjnymi (recA PCR/RFLP). Profile RFLP otrzymane za pomocą enzymu Tsp509I są użyteczne w identyfikacji poszczególnych gatunków bakterii rodzaju Acinetobacter. Na podstawie analizy otrzymanych sekwencji...
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TEM and AFM studies of segmented polyester polyurethanes obtained by quasi-prepolymer method.
PublikacjaPrzedmiotem badań były poliestrouretany o zawartości 50% segmentów sztywnych i zmiennym stosunku NCO/OH. Wykazano, że poliestrouretany otrzymane metodą quasi-prepolimerową wykazują inną morfologię niż otrzymane za pomocą metody prepolimerowej. W poliuretanach quasi- prepolimerowych obserwowano za pomocą mikroskopu AFM agregację segmentów sztywnych o wymiarze poprzecznym rzędu200nm. Segmenty te tworzyły fazę ciągłą. Kruche...