• Electrochemical measurements of FLBP modifications using isocyanates

  Open Research Data

  • P. Jakóbczyk
  • A. Dettlaff
  • S. Makowiec
  • R. Bogdanowicz

  The electrochemical behavior of modified FLBP was investigated using a potentiostat-galvanostat (VMP-300, Bio-Logic, France) with EC-Lab software (v11.50). Measurements were carried out in a three-electrode configuration (Pt wire as the counter electrode, Ag/AgCl wire as a pseudo-reference electrode) under an inert atmosphere. 

• GC electrode functionalization, DEIS studies

  Open Research Data

  • A. Koterwa
  • J. Ryl
  • P. Niedziałkowski
  • M. Pierpaoli
  • R. Bogdanowicz

  This dataset contains experimental results from electrochemical studies of aptamer-based biosensors composed of self-organised AuNC at GC electrode for the rapid detection of E. coli in real human urine samples through polymerase RNA.  The study discusses the electrode in each functionalisation step by attaching a non-coding strand of the oligonucleotide...

• Bioelectrochemical detection of COVID protein (RBD) on boron doped diamond - optimization of functionalziation parameters

  Open Research Data

  • A. Olejnik
  • R. Bogdanowicz

  The following dataset is a comprehensive overview of preparation of biofunctionalizaed BDD (boron-doped diamond) electrodes and their application in electrochemical sensing of COVID protein RBD. The specific receptor against RBD (Receptor Binding Domain) protein ACE-2 (Angiotensin Convertase Enzyme) is attached to the surface of BDD via a series of...

• Bioelectrochemical detection of COVID protein (RBD) on boron doped diamond – supporting measurements

  Open Research Data

  • A. Olejnik
  • R. Bogdanowicz

  This dataset includes a series of supporting electrochemical measurements in the topic of bioelectrochemical detection of COVID proteins (RBD - Receptor Bindign Domain) on boron doped diamond electrodes (BDD). The specific receptor (ACE-2 - angiotensin convertase enzyme) is attached via EDC/NHS linkers according to the previously optimized parameters...

• UV-VIS spectra of transparent thin diamond films on glass substrates

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz

  UV-VIS results for transparent diamond layers on glass. Results obtained with the UV-9000 SPECTROPHOTOMETER (Shanghai Metash Instruments Co., Ltd). They show transmittance and absorbance versus wavelength.

• Thickness profile of thin diamond films on glass substrates

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz

  Thickness profile of thin diamond layers on glass. Results obtained using the Dektak XT device (Bruker). They present a layer thickness profile. allowing to determine the surface roughness and the thickness of the fusion diamond thin layer.

• Electrochemical performance of boron-doped electrodes on quartz substrates in Fe(CN)₆³-/⁴- and ruthenium hexamine (RuHex): Observations from cyclic voltammetry and impedance spectroscopy

  Open Research Data

  • P. Jakóbczyk
  • R. Bogdanowicz

  In this study, we investigated the electrochemical behavior of boron-doped electrodes using two different redox probes: 5 mM ferrocyanide (Fe(CN)₆³⁻/⁴⁻) and ruthenium hexamine (RuHex) in a 0.5 M Na₂SO₄ electrolyte. The electrochemical testing was carried out using cyclic voltammetry (CV) to analyze the redox reactions and kinetics at the electrode interface,...

• XPS data of as-grown BDD, as-implanted Mn-BDD, and annealed Mn-BDD thin films

  Open Research Data

  • R. Bogdanowicz
  • P. Jakóbczyk
  • S. Deshmukh

  XPS survey spectra and detailed spectra O1, C1s and Mn2p of as-grown BDD, as-implanted Mn-BDD, and annealed Mn-BDD thin films. X-ray photoelectron spectroscopy (XPS) studies were conducted on an Escalab 250 Xi from Thermo Fisher Scientific with an Al Kα radiation.  Results were published in the paper ( https://doi.org/10.1002/adfm.202308617)

• Electrochemical Impedance Spectroscopy data of PDA-modified TiO2 nanotubes

  Open Research Data

  • A. Olejnik
  • J. Ryl
  • R. Bogdanowicz

  This dataset contains Electrochemical Impedance Spectroscopy data of the samples from TiO2 nanotubes modified with polydopamine. The studies were presented as a part of the research on "Band Gap Engineering toward Semimetallic Character of Quinone-Rich Polydopamine" (DOI: 10.1021/acs.jpcc.2c08804).

• SEM and Raman studies B:CNWs and BDD electrode used for electrochemical paraquat determination

  Open Research Data

  • M. Ficek
  • A. Olejnik
  • M. Sawczak
  • R. Bogdanowicz

  The dataset contains the scanning electron micrographs (SEM) and Raman  spectra of B:CNWs and BDD samples deposited by MW-PECVD. SEM was used to characterise the morphology of BDD and B:CNW. In contrast, RAMAN was used to reveal the main differences in the crystalline structure of BDD and B:CNWs. 

• Raman data of based on BDD, Mn-BDD, Mn-BDD(AN) electrodes

  Open Research Data

  • R. Bogdanowicz
  • P. Jakóbczyk

  Raman spectra of samples : ion implanted BDD (Mn-BDD) films; prepared by high dose (1015-1017 ions/cm2) Mn ion implantation and post-annealing treatment.

• Electrochemical studies of symmetrical supercapacitors based on BDD, Mn-BDD, Mn-BDD(AN) electrodes

  Open Research Data

  • S. Deshmukh
  • S. Kunuku
  • P. Jakóbczyk
  • A. Olejnik
  • R. Bogdanowicz

  Electrochemical performance of a Supercapacitor device in PVA-H2SO4 gelled electrolyte:  Cyclic voltammograms at varying scan rates ranging from 10 to 1000 mV s−1, galvanostatic charge-discharge curves with varying current density, cyclic stability (88000 charge-discharge cycles).

• XPS data of deuterium and hydrogen grown boron-doped diamond

  Open Research Data

  • R. Bogdanowicz
  • M. Sobaszek
  • M. Ficek

  The high-resolution C1s X-ray absorption spectra of BDD@H and BDD@D samples were measured using the facilities of the HE-SGM beamline (HE-SGM) at the BESSY II synchrotron radiation source of Helmholtz–Zentrum Berlin (HZB).[90] The measurements were carried out under ultra-high vacuum conditions: P ≈ 2×10−9 Torr at T = 300 K. The NEXAFS spectra were...

• Scanning electron microscopy (SEM) images of the boron-dopied carbon nanowalls surfaces

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 1200ppm  in the gas atmosphere during the synthesis.

• Raman data of deuterium and hydrogen grown boron-doped diamond

  Open Research Data

  version 1.0

  • R. Bogdanowicz
  • M. Sobaszek

  Raman spectra were recorded at room temperature using a micro-Raman spectrometer (Invia, Renishaw) equipped with an edge filter with different excitation wavelengths and lasers: UV λ = 325 nm (HeCd), blue λ = 488 nm (Ar+), green λ = 514 nm (Ar+), and IR λ = 785 nm (IR diode) and 50× microscope objective. To avoid sample heating, the radiation power...

• XPS studies of PDA-modified TiO2 nanotubes

  Open Research Data

  • J. Ryl
  • A. Olejnik
  • R. Bogdanowicz

  This dataset contains the XPS results (survey and high-resolution spectra) of the samples from TiO2 nanotubes modified with polydopamine. The studies were presented as a part of the research on "Band Gap Engineering toward Semimetallic Character of Quinone-Rich Polydopamine" (DOI: 10.1021/acs.jpcc.2c08804).

• Electrochemical studies of Boron-Doped Diamond enriched Laser Induced Graphene structures

  Open Research Data

  • S. Deshmukh
  • P. Jakóbczyk
  • M. Ficek
  • J. Ryl
  • d. Geng
  • R. Bogdanowicz

  This dataset contains electrochemical studies aimed to evaluate the capability of the utilization of laser-induced graphene (LIG) with incorporated boron-doped diamond nanowall (BDNW) hybrid nanostructures for microsupercapacitors. Selected results from this dataset were published in Advanced Functional Materials journal: https://doi.org/10.1002/adfm.202206097

• Scanning electron microscopy (SEM) images of boron-doped diamond thin films at poly(lactic acid)

  Open Research Data

  • A. Dettlaff
  • M. Rycewicz
  • M. Ficek
  • A. Wieloszyńska
  • J. Ryl
  • R. Bogdanowicz

  The dataset contains the photos obtained by scanning electron microscope(SEM), revealing the surface morphology and cross-section of boron-doped diamond electrodes on commercially available graphene-doped polylactide acid. The boron doping level expressed as the [B]/[C] ratio in the gas phase for these studies was 500 and 10,000 ppm. The top views of...

• The electrochemical studies of thin boron-doped diamond films deposited at conductive poly(lactic acid) 3D prints

  Open Research Data

  • A. Dettlaff
  • M. Rycewicz
  • M. Ficek
  • A. Wieloszyńska
  • J. Ryl
  • R. Bogdanowicz

  The dataset contains the electrochemical characteristics of the electrodes composed of thin boron-doped diamond films coated on commercially available graphene-doped polylactide acid. The boron doping level expressed as the [B]/[C] ratio in the gas phase for these studies was 500 and 10,000 ppm.

• Determining the optimal filling of the surface with a linker with Universal Force Field and Reax Force Field

  Open Research Data

  • B. Dec
  • R. Bogdanowicz
  • J. Ryl

  The DataSet contains the atomic slabs of diamond surfaces with  ATP molecules in water. The calculated data includes different sized surfaces from 90 Angstrom^2 to 691 Angstrom^2. Structures were relaxed using the Reax Force Field method with the Limited Memory Broyden–Fletcher–Goldfarb–Shanno algorithm. Structures were calculated with a convergence...

• The electrochemical response to Au electrode modification steps towards viral electrochemical immunosensor preparation

  Open Research Data

  • W. Białobrzeska
  • M. Brodowski
  • M. Kowalski
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the electrochemical measurements (CV/EIS) carried out for the consecutive steps of the Au electrode functionalization, in separate subfolders, as described. The cyclic voltammetry (CV) was conducted using a Palmsens 4 potentiostat/galvanostat system (Methrom, Autolab, Netherlands) in the standard three-electrode configuration, with...

• High resolution XPS analysis of BDD electrode functionalization steps towards SARS-CoV-2 detection

  Open Research Data

  • J. Ryl
  • M. Brodowski
  • R. Bogdanowicz

  This dataset contains the results of the high-resolution XPS analyses of a set of boron-doped diamond (BDD) electrodes after consecutive functionalization steps toward anchoring of a receptor capable of SARS-CoV-2 virus detection. The analysis was carried out in the binding energy range of C1s, N1s, O1s, Ni2p3/2. The measurements were carried out on...

• The electrochemical response to BDD electrode functionalization with ACE2 receptor

  Open Research Data

  • M. Brodowski
  • M. Kowalski
  • J. Ryl
  • R. Bogdanowicz

  This dataset contains the results of the electrochemical impedance spectroscopy (EIS) measurements of the boron-doped diamond (BDD) electrode functionalization with ACE2 receptor. The functionalized electrode was then used for the electrochemical detection of the SARS-CoV-2 virus S1 protein. 

• The electrochemical response to BDD electrode functionalization with IgG2B receptor

  Open Research Data

  • M. Brodowski
  • M. Kowalski
  • J. Ryl
  • R. Bogdanowicz

  This dataset contains the results of the electrochemical impedance spectroscopy (EIS) measurements of the boron-doped diamond (BDD) electrode functionalization with IgG2B receptor. The functionalized electrode was then used for the electrochemical detection of the SARS-CoV-2 virus S1 protein. 

• The electrochemical response to BDD electrode functionalization with CD147 receptor

  Open Research Data

  • M. Brodowski
  • M. Kowalski
  • J. Ryl
  • R. Bogdanowicz

  This dataset contains the results of the electrochemical impedance spectroscopy (EIS) measurements of the boron-doped diamond (BDD) electrode functionalization with CD147 receptor. The functionalized electrode was then used for the electrochemical detection of the SARS-CoV-2 virus S1 protein. 

• The electrochemical response to glassy carbon electrode modification steps towards viral electrochemical immunosensor preparation

  Open Research Data

  • W. Białobrzeska
  • M. Brodowski
  • M. Kowalski
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the electrochemical measurements (CV/EIS) carried out for the consecutive steps of the glassy carbon GC electrode functionalization, in separate subfolders, as described. The cyclic voltammetry (CV) was conducted using a Palmsens 4 potentiostat/galvanostat system (Methrom, Autolab, Netherlands) in the standard three-electrode configuration,...

• Scanning electron microscopy (SEM) images of the boron-dopied diamond surfaces

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of diamond electrodes on silicon substrates. The diamond surface is characterized by ultra-crystalline diamonds obtained by CVD synthesis. 

• Scanning electron microscopy (SEM) images of the boron-dopied diamond surfaces

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of diamond electrodes on different substrates. The diamond surface is characterized by an aggregation of crystals that do not form a continuous layer. 

• Scanning electron microscopy (SEM) images of the boron-doped carbon nanowalls surfaces

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 2000ppm  in the gas atmosphere during the synthesis.

• Scanning electron microscopy (SEM) images of the boron-doped carbon nanowalls surfaces

  Open Research Data

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 5000ppm  in the gas atmosphere during the synthesis.

• The BDD electrodes wettability modification by anodic polarization treatment

  Open Research Data

  • J. Ryl
  • M. Sobaszek
  • R. Bogdanowicz
  • Ł. Burczyk

  The dataset contains the raw images, photographs obtained for the contact angle measurement at the surface of the boron-doped diamond (BDD) electrode. The measurements were carried out on after potentiodynamic polarization procedure, at various anodic polarization scan range (no polarization - HTBDD; 1.0 V; 1.4 V; 1.9 V; 2.5 V vs Ag|AgCl, scan rate...

• The scanning electron microscopy (SEM) studies of heavy boron-doped diamond oxidation under high-temperature

  Open Research Data

  • A. Zieliński
  • J. Ryl
  • R. Bogdanowicz
  • M. Ficek
  • M. Cieślik
  • B. Dec

  The dataset contains the results of scanning electron microscopy (SEM) images of heavy boron-doped diamond (BDD) electrodes subjected to high-temperature oxidation in a furnace at 600 Celsius. The micrographs reveal the material decomposition of BDD grains due to high temperature.

• SEM micrographs of boron-doped nanocrystalline diamond-carbon nanospikes

  Open Research Data

  • J. Ryl
  • M. Ficek
  • R. Bogdanowicz

  This dataset contains the Scanning Electron Microscopy (SEM) micrographs taken for rich boron-doped carbon crystalline nanospikes/nanograss structures, at different magnifications, encoded in the labels of the images. The micrographs were made using Hitachi S-3400N SEM microscope in secondary electron mode under 20 kV accelerating voltage. No additional...

• SEM micrographs of diamond-phase (sp3-C) rich boron-doped carbon nanowalls (sp2-C)

  Open Research Data

  • J. Ryl
  • M. Sobaszek
  • R. Bogdanowicz
  • M. Ficek

  This dataset contains the Scanning Electron Microscopy (SEM) micrographs taken for rich boron-doped carbon nanowalls structures, with different boron addition during the synthesis process and different CVD synthesis duration. The [B]/[C] ratios in the plasma were set to 0k, 1.2k, 2k and 5k ppm. The time of growth was ranging between 4 and 9 hours. This...