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Search results for: ELECTROCHEMICAL%20SENSOR
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International Journal of Sensor Networks
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Journal of Sensors and Sensor Systems
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ACM Transactions on Sensor Networks
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The influence of precursor selection on electrochemical properties of radiofrequency thermal plasma synthesized graphene
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Electrochemical oxidation of sulphamerazine at boron-doped diamond electrodes: Influence of boron concentration
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Electrochemical investigations of conductive coatings applied as anodes in cathodic protection of reinforced concrete
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Application for novel electrochemical screening of antioxidant potential and phytochemicals in Cornus mas extracts
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Magnesium(ii) 1-(1-adamantylsulfanyl)phthalocyanine – synthesis, photochemical and electrochemical properties
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Bottom up approach of metal assisted electrochemical exfoliation of boron towards borophene
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A facile synthesis method and electrochemical studies of a hierarchical structured MoS2/C-nanocomposite
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Low-Temperature Exfoliated Graphenes: Vacuum-Promoted Exfoliation and Electrochemical Energy Storage
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Deposition of EDOT-Decorated Hollow Nanocapsules into PEDOT Films for Optical and Electrochemical Sensing
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Influence of geometry and annealing temperature in argon atmosphere of TiO2 nanotubes on their electrochemical properties
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Influence of Thermal Modification and Morphology of TiO2 Nanotubes on Their Electrochemical Properties for Biosensors Applications
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Electrochemical stability of TiO2 nanotubes deposited with silver and gold nanoparticles in aqueous environment
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Electrochemical oxidation of sulphamerazine at boron-doped diamond electrodes: Influence of boron concentration
PublicationThe boron-doped diamond (BDD) electrodes with different boron concentrations have been tested as electrode material for sulphamerazine (SRM) oxidation in water solution. An investigation of the electrode morphology and molecular structure was carried out using high resolution scanning electron microscopy (SEM) and Raman spectroscopy. Electrochemical results showed clearly that the kinetics and efficiency of SRM oxidation were dependent...
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Nanocrystalline diamond microelectrode on fused silica optical fibers for electrochemical and optical sensing
PublicationFabrication process of thin boron-doped nanocrystalline diamond (B-NCD) microelectrode on fused silica single mode optical fiber has been investigated. The B-NCD films were deposited on the fibers using Microwave Plasma Assisted Chemical Vapor Deposition (MW PA CVD) at glass substrate temperature of 475 ºC. We have obtained homogenous, continuous and polycrystalline surface morphology with the mean grain size in the range of 100-250...
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Electrochemical activity of composite material poly(3,4-ethylenedioxythiophene) modified by silver hexacyanoferrate
PublicationW pracy przedstawiono sposób slektrochemicznj syntezy materiału składającego się z polimeru przewodzącego poli(3,4-etylenodioksytiofen) (pEDOT) i nieorganicznej sieci typu redox heksacyjanożelazianu srebra (Aghcf). Materiał otrzymano na drodze dwuetapowej. Etap pierwszy polega na galwanostatycznej redukcji srebra na elektrodzie z węgla szklistego. Etap drugi to roztwarzanie srebra z jednoczesną polimeryzacją monomeru. Otrzymany...
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Experimental study of corrosion in reinforced concrete by acoustic emission and electrochemical noise techniques
PublicationTechnika emisji akustycznej jest znaną metodą badań korozji zbrojenia żelbetu. Źródłem aktywności akustycznej są zawsze zjawiska o naturze mechanicznej. Przedstawiono wynik badań akustycznych zbrojonego betonu w warunkach polaryzacji anodowej, przyspieszającej procesy korozyjne. Symultanicznie prowadzona była rejestracja szumu elektrochemicznego. Dla umożliwienia korelacji wyników, uzyskanych obiema technikami, wykonana została...
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Electrochemical investigations of conductive coatings applied as anodes in cathodic protection of reinforced concrete.
PublicationW pracy przedstawiono rezultaty badań elektrochemicznych polimerów przewodzących z pigmentem grafitowym. Wyznaczono parametry elektrochemiczne badanych powłok w trakcie długotrwałej polaryzacji zbrojonego betonu. W oparciu o pomiary impedancyjne wyznaczono parametry elektrochemiczne powłok przewodzących. Wykazano, że badane powłoki mogą być stosowane w ochronie katodowej żelbetu. Badania wykazały, że optymalne stężenie grafitu...
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Production and Properties of the Porous Layer Obtained by the Electrochemical Method on the Surface of Austenitic Steel
Publication: The growing demand for implants has seen increasing interest in the introduction of new technologies and surface modification methods of metal biomaterials. This research aimed to produce and characterize a porous layer grown on austenitic stainless steel 316L, obtained via the anodization process near the micro-arc oxidation, i.e., low voltage micro-arc oxidation (LVMAO). The discussed layer significantly influences the properties...
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Electrochemical performance of thin free-standing boron-doped diamond nanosheet electrodes
PublicationIn the following work we describe preparation and the electrochemical performance of thin and free-standing heavy boron-doped diamond (BDD) nanosheets. The investigated foils were deposited on Ta substrate using microwave plasma-enhanced chemical vapor deposition technique (MPECVD). Foils of two B-dopant densities were investigated, obtained on the base of 10 k and 20 k ppm [B]/[C] ratio in the gas admixture. The obtained foils...
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Synergistic effects of nitrogen-doped carbon and praseodymium oxide in electrochemical water splitting
PublicationHybrid materials featuring perovskite-type metal oxide in conjunction with heteroatom-doped graphene hold immense promise as alternatives to costly noble metal catalysts for electrochemical water splitting, facilitating the generation of environmentally friendly hydrogen. In this study, perovskite-type oxide containing praseodymium, barium, strontium, cobalt, and iron atoms dispersed in a carbon matrix as a catalyst is synthesized...
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Structural, optical and electrochemical performance of black phosphorus and black arsenic-phosphorus nanostructures
PublicationBlack phosphorus (BP)-based nanostructures have drawn a lot of attention due to their tunable bandgap and extraordinary properties such as: high surface-to-volume ratio, large number of active sites, and prominent edges. However, low dimensional structures of black phosphorus oxidize easily, which hamper their application on a broader scale. One way to overcome these difficulties is to modify the black phosphorus structure by substituting...
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Comparison of corrosion resistance of al-alloys by means of dynamic electrochemical impedance spectroscopy
PublicationPrzeprowadzono badania metodą dynamicznej elektrochemicznej spektroskopii impedancyjne stopów 1100 i 5162. Zaproponowano zastępcze modele elektryczne opisujące zachowanie się stopów w warunkach ekspozycji w roztworach zawierających wysokie stężenie jonów chlorkowych. Wyznaczono zmiany podstawowych parametrów elektrycznych układów zastępczych od potencjału. Stwierdzono wyższą podatność na korozję stopu 5162 w porównaniu ze stopem...
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Investigating BiMeVOx compounds as potential photoelectrochemical and electrochemical materials for renewable hydrogen production
PublicationIn this study, BiMeVOx compounds (where Me: Co, Mo, Ce, Zr) were synthesized and characterized as potential photoelectrochemical materials for solar water splitting, the hydrogen evolution reaction (HER), and oxygen evolution reaction (OER). The analysis confirmed the successful formation of phase BiMeVOx compounds with the desired crystal structure. Among the tested materials, BiCoVOx(800) showed the highest photocurrent density...
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Nitrogen-incorporated boron-doped diamond films for enhanced electrochemical supercapacitor performance
PublicationThe electrochemical (EC) supercapacitor, known for its rapid charging, reliability, and versatile applications, demands optimized electrode characteristics and an understanding of their electrochemical behaviour. Although boron-doped diamond (BDD) holds promise as a supercapacitor electrode, a crucial gap exists in comprehending its material behaviour under specific growth conditions. Here, nitrogen-incorporated BDD (N-BDD) films...
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An electrochemical biosensor for the determination of hormone Human Chorionic Gonadotropin (hCG) in human serum
PublicationThis work describes the modification of a gold electrode to create an electrochemical biosensor capable of detecting human chorionic gonadotropin (hCG). The biosensor was obtained by modifying the gold electrode with cysteamine and oligopeptide (PPLRINRHILTR). The modification steps of the gold electrode were confirmed by cyclic voltammetry (CV) and impedance electrochemical spectroscopy (EIS) measurements. The conducted EIS experiments...
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Enhanced Electrochemical Performance of MnCo1.5Fe0.5O4Spinel for Oxygen Evolution Reaction through Heat Treatment
PublicationMnCo1.5Fe0.5O4 spinel oxide was synthesized using the sol−gel technique, followed by heat treatment at various temperatures (400, 600, 800, and 1000 °C). The prepared materials were examined as anode electrocatalysts for watersplitting systems in alkaline environments. Solid-state characterization methods, such as powder X-ray diffraction and X-ray absorption spectroscopy (XAS), were used to analyze the materials’ crystallographic...
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Application of BDD thin film electrode for electrochemical decomposition of heterogeneous aromatic compounds
PublicationThe aim of the presented study is to investigate the applicability of electrochemical oxidation of aromatic compounds containing heteroatoms, e.g. waste from production of pesticides or pharmaceutics, at a borondoped diamond (BDD) electrode. The BDD electrodes were synthesized by microwave plasma enhanced chemical vapour deposition (MW PE CVD). Investigation of the electrode surface by optical microscopy and scanning electron microscopy...
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Simultaneous opto-electrochemical monitoring of carbamazepine and its electro-oxidation by-products in wastewater
PublicationThe growing human impact on aquatic environments, due to the extensive use of pharmaceuticals and the release of persistent pollutants, makes it necessary to implement new widespread methods for the characterisation and quantification of such contaminants and relative degradation products. Carbamazepine, 5H-dibenzo[b,f]azepine-5-carboxamide, (CBZ) is a widely used anti-epileptic drug, characterised by its limited removal by conventional...
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Application of Electrochemical Impedance Spectroscopy to evaluate cathodically protected coated steel in seawater
PublicationTwo types of organic coated carbon steel (S235JR2 grade) electrodes were exposed to artificial seawater environment. One prepared type was defect free while the other one had an intentionally introduced φ0,5 cm coating defect. Both kinds of samples were polarized during the exposure to four potentials corresponding to four different cathodic protection levels. Evolution of their EIS spectra is presented in this paper. Results obtained...
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Anion binding by p-aminoazobenzene-derived aromatic amides: spectroscopic and electrochemical studies
PublicationThe synthesis and complexing properties of p-aminoazobenzene-derived mono-, bis-, and trisamides were described. Ligands 3 and 4 bind anions, including fluorides, chlorides, bromides, acetates, benzoates, dihydrogen phosphates, hydrogen sulfates, and p-toluenesulfonates, in chloroform forming 1 : 1 complexes. The highest value of stability constant was evaluated for the 4-F− complex (log K = 5.63 ± 0.21). On the basis of 1H NMR,...
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Time evolution of Electrochemical Impedance spectra of cathodically protected steel in artificial seawater
PublicationUsability of Electrochemical Impedance Spectroscopy data for better cathodic protection control was investigated. Carbon steel – S235JR2 grade specimen were exposed in artificial seawater environment. Samples were polarized and their potentials corresponded to four different cathodic protection degrees. Time evolution of Electrochemical Impedance spectra was investigated. Goodness of fit function (X2) was analysed in terms of proper...
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Biosilica from sea water diatoms algae—electrochemical impedance spectroscopy study
PublicationHere, we report on an electrochemical impedance study of silica of organic origin as an active electrode material. The electrode material obtained from carbonized marine biomass containing nanoporous diatoms has been characterised by means of XRD, IR, SEM and EIS. Dif- ferent kinds of crystallographic phases of silica as a result of thermal treatment have been found. The electrode is electrochemically stable during subsequent cyclic...
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Study of the electrochemical stability of polypyrrole coating on iron in sodium salicylate aqueous solution
PublicationIn this work electrochemical stability of optimized PPy film on iron in aqueous solution of sodium salicylate is studied. The main drawback of conducting polymers is their possibility to undergo an irreversible degradation (overoxidation). The overoxidized polymers lose their properties, for example, conductivity and redox activity, what excludes them from some practical applications. This study demonstrates that lowering the concentration...
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Tailoring the electrochemical degradation of iron protected with polypyrrole films for biodegradable cardiovascular stents
PublicationThe degradation of polypyrrole (PPy) coated iron is studied in phosphate buffer saline solution at 37 °C by odd random phase multisine electrochemical impedance spectroscopy (ORP-EIS). PPy is electropolymerized with anti-inflammatory salicylates incorporated in the film, as a drug release system. The modelling of EIS over time provides the quantitative description of the corrosion behaviour of the material. Thus, the reliable...
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Developing electrochemical measurements in order to assess anti-corrosive coatings more effectively
PublicationCelem pracy było sprawdzenie powtarzalności wyników uzyskanych metodą pomiaru szumu (Electrochemical Noise method - ENM) elektrochemicznego wykonanych na powłokach organicznych w konfiguracji bez połączenia z podłożem metalowym (NOCS - No Connection to the Substrate). NOCS polega na wykonaniu pomiarów na trzech teoretycznie takich samych obszarach badanego układu. W takim układzie nie jest wymagane połączenie elektryczne z metalowym...
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Sensor Letters
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Corrosion resistance evaluation of Al‐based alloys by means of dynamic electrochemical impedance spectroscopy
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Application of electrochemical impedance spectroscopy to monitoring discharging process of nickel/metal hydride battery
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Electrochemical properties of metallated porphyrazines possessing isophthaloxybutylsulfanyl substituents: Application in the electrocatalytic oxidation of hydrazine
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Influence of Filler Metal on Electrochemical Characteristics of a Laser-Welded CoCrMoW Alloy Used in Prosthodontics
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Structure and electrochemical reactivity of new sulphur–silicon podands adsorbed on silver or gold surfaces
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Carbon nanotube based dielectric spectroscopy of tumor secretion; electrochemical lipidomics for cancer diagnosis
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Synthesis, Growth Mechanism, and Electrochemical Properties of Hollow Mesoporous Carbon Spheres with Controlled Diameter
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Ultrathin NiO confined within hollow carbon sphere for efficient electrochemical energy storage
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Poly(amidoamine) dendrimer immunosensor for ultrasensitive gravimetric and electrochemical detection of matrix metalloproteinase-9
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Polymer membranes loaded with lipids for taste sensing: electrochemical impedance spedance spectroscopy studies
PublicationZcharakteryzowano metodą impedancyjnej spektroskopii elektrochemicznej membrany polichlorku winilu z lipidami zanurzone w roztworze kwasu cytrynowego. Badano membrany elektrod dodatnio naładowanych (heksadecyloamina, chlorek, benzyloheksadecylodimetyloamoniowy) i ujemne naładowanych (kwas elaidynowy, cholesterol, l-dodekonol). Badania impedacyjne pozwoliły na rozróznienie czterech stałych czasowych: rezystancja wysokiej częstotliwości,...
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Application of electrochemical impedance spectroscopy to monitoring discharging process of nickel/metal hydride battery.
PublicationThis paper presents the possibility of applying impedance analysis to cell diagnostics. In order to obtain characteristic curves of both electrodes of a NiMH battery simultaneously, a reference electrode was added into the circuit. The authors analysed the cell under three cases, i.e. when its properties are determined only by the state of the positive electrode, only by the state of the negative electrode, or when both electrodes...