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Search results for: materials science
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In-depth characterization of icosahedral ordering in liquid copper
PublicationThe presence of icosahedral ordering in liquid copper at temperatures close to the melting point is now well-established both experimentally and through computer simulation. However, a more elaborate analysis of local icosahedral and icosahedron-like structures, together with a system for classifying such structures based on some measure of "icosahedrity", has so far been conspicuously absent in the literature. Similarly, the dynamics...
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THE PROPERTIES OF NANOSILVER – DOPED NANOHYDROXYAPATITE COATING ON THE Ti13Zr13Nb ALLOY
PublicationThe aim of this research was to study the properties of nanohydroxyapatite (nanoHAp) and nanohydroxyapatite, doped with nanosilver (nanoHAp/nanoAg), coatings obtained by an electrophoretic deposition process. The suspensions was prepared by dispersing 0.1 g of HAp nanopowder for nanoHAp coatings and 0.1 g of nanoHAp and 0.025 g nanoAg for nanoHAp/nanoAg coatings. The deposition was carried out for 1 min at 50 V voltage followed...
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Determination of ionic conductivity in the Bi-Si-O and Pb-Si-O glasses
PublicationImpedance spectroscopy measurements in various gas atmospheres were carried out in order to explain the doubts about the type of carriers and the mechanism of electrical conductivity in Bi-Si-O and Pb-Si-O glasses. In bismuth silicate glass, a typical ionic conductivity with oxygen ions as charge carriers was observed. The level of electrical conductivity of the glass at 400 °C was 5 × 10−8 S·cm−1 , with the activation energy of...
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Bacterial nanocellulose as a microbiological derived nanomaterial
PublicationBacterial nanocellulose (BNC) is a nanofibrilar polymer produced by strains such as Gluconacetobacter xylinus, one of the best bacterial species which given the highest efficiency in cellulose production. Bacterial cellulose is a biomaterial having unique properties such as: chemical purity, good mechanical strength, high flexibility, high absorbency, possibility of forming any shape and size and many others. Such a large number...
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Cavitation erosion of X5CrNi18-10 austenitic stainless steel alloyed with TiC
PublicationPraca prezentuje zmianę odporności kawitacyjnej stali X5CrNi18-10 po laserowym stopowaniu jej warstwy wierzchniej węglikiem TiC. Laserowe stopowanie przeprowadzono dla 2 wariantów. W pierwszym przypadku stal stopowano do zawartości 1,55 TiC a w drugim do zawartości 3,97% TiC. Uzyskane rezultaty wskazują że przy zawartości 3,97 TiC nastopiło znaczące zwiększenie odporności na plastyczne odkszyałcenie warstwy wierzchniej pod wpływem...
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Wpływ utleniania w wysokich temperaturach na struktury napawanych warstw na bazie kobaltu
PublicationPrzedmiotem badań są napawane plazmowo warstwy wykonane ze stopu kobaltu zawierające ok. 29% chromu, ok. 5% wolframu i ok. 2% niklu, nałożone powierzchnie przylgni grzybków zaworów wylotowych silnika dieslowskiego. Powierzchnia podlega zarówno oddziaływaniom temperatury i środowiska, jak i oddziaływaniom mechanicznym. Podczas badań warstwy poddano oddziaływaniu środowiska utleniającego i wysokich temperatur: 750°C- górna w normalnej...
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Microstructure and corrosion properties of the (Mn-N-O-P) type layers created on aluminium alloys
PublicationPrzedstawiono mikrostrukturę i właściwości korozyjne warstw powierzchniowych typu (Mn-N-O-P) wytworzonych na stopach aluminium. Wykazano, iż warstwy (Mn-N-O-P) podwyższają wielokrotnie odporność korozyjną stopów aluminium i mogą być stosowane jako warstwy ochronne na tych materiałach.
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The degradation of metal implants
PublicationThe presence of metal implants in the human body causes some dangers, which result from introducing another object into organism. There may occur a biocorrosion, which causes different modifications of implant surface.
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Analisys of the failure of fixator used in bone surgery
PublicationThe Gamma nail (fixator) made of stainless steel, which has broken in the body, was subjected to examination. The fixator was removed from the patient femur. The fracture occurred in the area of the nail hole after two months' stay in the organism. The research included chemical composition, hardness of the Gamma nail material and the observation and analysis of the type of fracture. The research showed the fatigue failure of the...
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Stabilization of the titanium vibration damping wires in the steam turbine blades system
PublicationPrzedstawiono metody stabilizacji drutów tłumiących w systemie łopatkowym turbin parowych. Na podstawie badań eksperymentalnych mikrostruktury i własności mechanicznych wykazano przydatność metody stabilizacji na gorąco drutów tłumiących wykonywanych ze stopu tytanu WT3-1.
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Frequency bands selection of the Portevin-LeChatelier
PublicationEfekt Portevina-LeChateliera ujawnia się w postaci skokowych zmian naprężenia w trakcie procesu odkształcenia próbek pewnych stopów. Zjawisko PLC występuje w kilku odmianach charakteryzujących się istotnymi różnicami zarówno w przestrzennym rozkładzie pasm odkształcenia jak też przebiegu krzywej naprężeniowej. Przebiegi odpowiadające różnym odmianom serration charakteryzują się odmiennymi właściwościami rozkładu energetycznego...
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Surface cracking of laser melted Ti-6Al-4V alloy
PublicationOpisano charakterystyczne cechy pękania powierzchniowego obserwowanego po nadtapianiu laserem CO2 i Nd:YAG stopu Ti-6Al-4V. Obserwowano pęknięcia niezależnie od sposobu nadtapiania, penetrujące głęboko strefę przetopioną i w niewielkim stopniu zależne od sposobu nadtapiania. Przypisano obserwowane zjawisko przemianie martenzytycznej i (lub) naprężeniom cieplnym powstającym podczas gwałtownego chłodzenia.
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Underwater welding - a review
PublicationW artykule przedstawiono stan obecny oraz perspektywy rozwoju technik spawania pod wodą. Przeanalizowano najważniejsze problemy spawania w środowisku wodnym. Przedstawiono najważniejsze kierunki badań spawania podwodnego podejmowane w Katedrze Technologii Materiałów Maszynowych i Spawalnictwa Politechniki Gdańskiej
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Microbiological corossion of metallic products as a result of biofilm
PublicationWarunkiem do pojawienia się korozji mikrobiologicznej jest utworzenie na powierzchni metalu biofilmu. Zawiera on biologicznie czynne mikroorganizmy wraz z produktami ich przemian metabolicznych. Biofilm ogranicza dyfuzję produktów metabolizmu wytwarzanych przez poszczególne komórki mikrokolonii. Powoduje to, że produkty uboczne tych przemian gromadzą się w bezpośrednim sąsiedztwie metalu. Gdy powierzchnia metalu nie jest odporna...
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Assessment of evaporator tubes corrosion in low-emission steam boilers
PublicationW artykule przedstawiono wyniki badań rur ekranowych(16Mo3) kotła niskoemisyjnego po jednym roku i dwóch latach eksploatacji. Powierzchnie rur pokryte zostały warstwami natryskiwanymi cieplne - pojedynczą ze stopu 70%Ni 30%Cr i podwójną Ni-30Cr /Al2O3. Rury bez powłok natryskiwanych wykazywały pocienienie ze względu na działanie korozji siarkowej oraz korozyjnego oddziaływania warstwy stopionych soli. Pojedyncza warstwa 70%Ni 30%Cr...
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Pure silicon recovering from photovoltaic modules
PublicationOdzyskiwanie krzemu ze zużytych lub uszkodzonych modułów fotowoltaicznych może mieć znaczenie nie tylko ekonomiczne, ale również ekologiczne. Etap obejmujący procesy chemiczne wymaga optymalizacji z punktu widzenia wymaganej czystości odzyskiwanego krzemu. W pracy przedstawiono wyniki przeprowadzonych prób trawienia poszczególnych warstw ogniw PV: warstwy antyodblaskowej, metalizacji (kontaktów), złącza p-n. Skład roztworów trawiących...
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Effects of the time and temperature on the oxide scale formed on the cobalt alloys
PublicationWarstwy wykonane za pomocą techniki PTA ze stopu kobaltu poddano utlenianiu w różnych temperaturach i w różnym czasie. Mikrostruktury otrzymane po utlenianiu wskazują na proces degradacji materiału. Proces ten prowadził do degradacji obszarów międzydendrytycznych napoiny. Skład chemiczny powstającej zgorzeliny byłzależny od temperatury utleniania, składu chemicznego stopu, ze szczegfólnym uwzględnieniem obecności małych ilości...
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FEM approach to estimate the behaviour of biocomposite metal-surface coating system
PublicationA three dimensional (3D) model of biocomposite metal-surface coating system, which is influenced byknown external forces, is proposed. This model consists of the metallic substrate (Ti6Al4V) and thehydroxyapatite (HA) coating. Using FEM (finite element method), strain-stress maps of model weregenerated for investigating relations between the extreme stress of HA coating and the magnitude ofexternal force and the thickness of the...
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Assessment of cavitation erosion damage of laser remelted the SUPERSTON alloy
PublicationW artykule przedstawiono wpływ obróbki laserowej w warunkach kriogenicznych na mikrostrukturę stopu SUPERSTON po badaniach kawitacyjnych. Badania odporności kawitacyjnej przeprowadzono na stanowisku z wirującą tarczą w IMP PAN Gdańsk. Określono kinetykę ubytku masy próbek podczas testu kawitacyjnego dla stopu odlanego i nadtopionego laserowo.
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Fracture of aluminium joints bonded with epoxy adhesive reinforced by mmt nanoparticles
PublicationCrack propagation behavior was studied for aluminium/aluminum adhesive joints bonded with two epoxy adhesives: pure and reinforced with clay nanoparticles. The focus was also on the novel use of the constant displacement rate test to study adhesion/adhesives efficiency. The epoxy systems studied were: Epidian E6 produced from bisphenol A and epichlorohydrin, (''Organika -Sarzyna'' Poland); pure or strengthened with montmorillonit...
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Coatings in arthroplasty [online]
PublicationThe modern coatings used in arthroplasty for long term implants are reviewed. The phosphate coatingsare the most popular technique to improve the bone-implant interfacial strength and promote theosseointegration. The plasma spraying, electrophoretic precipitation, powder metallurgy, ion beamsputtering, high velocity oxy-fuel (HVOF) combustion spraying, sol-gel technique, biomimeticdeposition are mostly used to obtain the phosphate,...
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Self-Organized Nanotubular Oxide Layers on Ti and Ti Alloys
PublicationTo improve bioactivity of titanium and titanium, the implant surface modification by formation of self-organized TiO2 nanotube arrays with electrochemical techniques is presented. The influence of electrolyte composition and deposition parameters during anodization is characterized. The enhancement of phosphates deposition by titanium nanotubular structure is discussed. The calcium phosphate ceramics is shown to be uniformly deposited...
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Allergy to implant components: chromium, nickiel, cobalt and titanium
PublicationImplant jest kompozycja roznych pierwiastkow: niklu, chromu, kobaltu, tytanu, molibdenu i wanadu. Pierwiastki te moga doprowadzic do alergii, egzemy i obluzowania implantu.
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Electrical properties of hybrid planar diode based on palladium phthalocyanine and titanium dioxide
PublicationThis work details experimental studies of a planar diode made of indium tin oxide/titanium dioxide/palladium phthalocyanine/gold. The rectification ratio of current was 105 at 1.5 V. The analysis of the electrical properties of the system was based on small signal complex capacitance spectra measured in the frequency range of 25 Hz-1 MHz at different values of bias. No depletion region at the TiO2/PdPc interface was observed. Forward...
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Cold Cracking Of Underwater Wet Welded S355G10+N High Strength Steel
PublicationWater as the welding environment determines some essential problems influencing steel weldability. Underwater welding of high strength steel joints causes increase susceptibility to cold cracking, which is an effect of much faster heat transfer from the weld area and presence of diffusible hydrogen causing increased metal fragility. The paper evaluates the susceptibility to cold cracking of the high strength S355G10+N steel used,...
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ESTIMATION OF YOUNG`S MODULUS OF THE POROUS TITANIUM ALLOY WITH THE USE OF FEM PACKAGE
PublicationPorous structures made of metal or biopolymers with a structure similar in shape and mechanical properties to human bone can easily be produced by stereolithographic techniques, e.g. selective laser melting (SLM). Numerical methods, like Finite Element Method (FEM) have great potential in testing new scaffold designs, according to their mechanical properties before manufacturing, i.e. strength or stiffness. An example of such designs...
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Reliable method of assessing fracture properties of asymmetric bonded joints
PublicationTwo methods of assessing fracture properties of adhesive joints were studied. Two wedge tests: with continuous deflection and with force measurements were compared. Asymmetric geometry of the bonded joint was considered, i.e. two different plates of aluminium alloys: Al-Cu and Al-Mg, were bonded with epoxy DGEBA adhesive. The analytical model is shown to estimate the values of fracture properties: crack position and critical fracture...
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Surface modifications of ti and its alloys
PublicationThis article reviews the various surface modification techniques pertaining to titanium and titanium alloys including physical treatment, mechanical treatment, and chemical and electrochemical treatment. The proper surface modification expands the use of titanium and its alloys in the biomedical field for long-term implants retaining the excellent properties of substrate material and improving the specific surface properties required...
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Hydroxyapatite coatings on porous ti and ti alloys
PublicationDeposition of hydroxyapatite coating on porous Ti and Ti alloys with electrochemical and biomimetic deposition approach is presented. The enhancement of phosphates deposition by well oriented and uniform titanium oxide nanotube array on the surface of titanium substrate is discussed.
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Influence of laser remelting at cryogenic conditions on corrosion resistance of non-ferrous alloys
PublicationCelem nadtapiania laserowego elementów wytwarzanych z stopów aluminium, miedzi i tytanu jest uzyskanie wysokiej twadrości i odporności na korozję dla wydłużenia okresu ich eksploatacji w rezultacie ich szybkiej krystalizacji. Końcowa mikrostruktura, skład fazowy i właściwości wymienionych stopów zależą od parametrów obróbki laserowej oraz budowy wykresów równowagi fazowej. W artykule przedstawiono wpływ laserowego nadtapiania...
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Optimal Features of Porosity of Ti Alloys Considering their Bioactivity and Mechanical Properties
PublicationW artykule przedstawiono wpływ porowatości i rozmiaru porów tytanu i jego stopów, użytych, jako materiały ortopedyczne, na bioaktywność i własności mechaniczne struktur porowatych. Optymalne cechy porowatych rusztowań tytanowych umożliwiają rekonstrukcję i regenerację tkanki kostnej w zastosowaniach przenoszących obciażenie.
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Properties of surface layers of titanium alloy Ti6Al4V after laser melting processes
PublicationThe article presents the investigation results of titanium alloy Ti6Al4V surface layer after laser melting process. The process of laser melting was performed using Nd-YAG laser. The evaluation of structure of the alloy as well as hardness and chemical composition was performed. It was shown that laser melting changes the structure and properties of titanium alloy Ti6Al4V and process parameters as scanning speed affects the thickness...
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DYNAMIC MECHANICAL BEHAVIOUR OF GFRP COMPOSITES WITH SiO2 NANO PARTICLES REINFORCED EPOXY MATRIX
PublicationDynamic mechanic (DMA) tests were performed to compare the mechanical behaviour of glass fibre reinforced epoxy laminate composites with SiO2 nanoparticle reinforced matrix. The selection of the most promising nanoparticle concentrations was considered in terms of elastic modulus and glass transition temperature. The reference specimens (0% nanoparticles) did not contain diluent accordingly the results do not allow the exact comparison...
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Weldability of S500MC Steel in Underwater Conditions
PublicationWet welding with the use of covered electrodes is one of the methods of underwater welding. This method is the oldest, the most economic and the most versatile. The main difficulties during underwater wet welding are: high cooling rates of the joint, the presence of hydrogen in the arc area and formation of hard martensitic structure in the weld. These phenomena are often accompanied by porosity of welds and large number of spatters,...
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The Effect of Welding Conditions on Mechanical Properties of Superduplex Stainless Steel Welded Joints
PublicationThe tests results of superduplex stainless steel welded joints made with a different heat input, using automatic submerged arc welding (SAW) and semi-automatic flux-cored arc welding (FCAW) have been presented. Metallographic examinations, the measurements of the ferrite content, the width of the heat affected zone (HAZ) and the hardness of the welds in characteristic areas have been performed. Significant differences in the amount of...
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Impact Behaviour of Glass Fribre /Epoxy Composites with Nano-Enhanced Resin after Water Exposure
PublicationImpact behaviour of glass fibre /epoxy composites with nano- SiO2 modified resin was studied in terms of low velocity impact after water exposure. Nanocomposites with 1%, 2%, 3% 5% 7% nano-SiO2 (Nanopox- Evonic) were investigated. Peak impact load and impact damage area as a function of nanoparticle contents were compared for dry specimens and for samples exposed to water (0.7 %wt. 1.7% water absorbed) at 1J, 2J 3J impact energies....
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Structure and thermal expansion of liquid bismuth
PublicationExperimental structural data for liquid Bi were used for estimation of the main structure parameters as well as the thermal expansion coefficient both in supercooled and superheated temperature ranges. It was shown that the equilibrium melt had a positive thermal expansion coefficient within a temperature range upon melting and a negative one at higher temperatures. The former was related to structure changes upon melting, whereas...
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Structure and properties of liquid Al–Cu alloys: Empirical potentials compared
PublicationWe report on the structure and mass transport properties of liquid Al–Cu alloys predicted by two recently-developed empirical many-body potentials: MEAM (Jelinek et al., 2012) and EAM-ADP (Apostol and Mishin, 2011), and by the well-known Gupta potential. Total and partial pair correlation functions, angular distribution functions, densities, coordination numbers and self-diffusion coefficients are compared with published experimental...
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Water sorption and blistering of GFRP laminates with varying structures
PublicationThe microstructures, water absorption as well as blistering was studied for bi- and tri- axial glass fibre vinyl ester and polyester -matrix laminates coated with gel coat layer and uncoated. The effect of manufacturing technique on water sorption characteristics was considered. It was found that water sorption characteristics of GFRP depend on manufacturing methods. The least water intake was found for specimens having perfect...
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Environmental degradation of titanium alloy in artificial saliva
PublicationThe titanium and its alloys are potentially prone to hydrogen embrittlement, including those proposed for dental implants. The research has been aimed to assess a susceptibility to environment-enhanced degradation of the Ti-13Zr-13Nb alloy in artificial saliva with or without hydrofluoric acid, subject or not to cathodic polarisation. The results have shown that even if artificial saliva is safe environment, both cathodic polarization...
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Novel Polyurethanes as Antifouling Paint Matrices
PublicationThe new poly(ester-ether urethane)s (PEEUR) were prepared in two stage synthesis from formerly obtained oligo(alkylene ester-ether)diols (OAEE) and 4,4‘-diphenylmethane diisocyanate (MDI). PEEUR samples were subjected to crosslinking with styrene in the presence of radical polymerization initiators: methyl ethyl ketone peroxide (MEKPO) or cobalt 2-ethyl cyclohexanoate (EtHCo). Crosslinked PEEUR were characterized by their physicochemical...
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DEGRADATION OF GFRP MARINE LAMINATES WITH NANO PARTICLE MODIFIED COATINGS
PublicationWater absorption and surface blistering behaviour was studied for polyester-matrix laminates with SiO2 nanoparticle reinforced gel coats. Accelerated water immersion tests at 37°C showed that addition of 10% nanoparticles increases blisters incubation time by ca. 50% compared to 5% and 0% nanoparticles composites.
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Structural properties of hypothetical CeBa2Cu3O7 compound from LSDA+DMFT calculations
PublicationThe hypothetical stoichiometric CeBa2Cu3O7 (Ce123) compound, which has not been synthesized as a single phase yet, was studied by the density functional theory (DFT). We utilized a method which merges the local spin density approximation (LSDA) with the dynamical mean-field theory (DMFT) to account for the electronic correlations. The LSDA+DMFT calculations were performed in the high-temperature range. The particular emphasis was...
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Influence of Nitriding and Laser Remelting on Properties of Austenitic Stainless Steel Type X10CrNi18-8 and Cavitation Erosion Resistance
PublicationThe paper presents properties of surface layers. Surface layers were obtained by using low temperature glow–discharge nitriding process and laser remelting carried out on austenitic stainless steel type X10CrNi18-8. Investigations were done by using an Ultra Nanoindentation Tester (UNHT) in the Warsaw Institute of Fundamental Technological Research. The influence of the above mentioned...
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Temper bead welding of S420G2+M steel in water environment
PublicationThe article presents the idea of the use of Temper Bead Welding (TBW) technique to improve the weldability of high strength steel at underwater wet welding conditions. Wet welding method with the use of covered electrodes is described. This work shows results of metallographic examinations and hardness measurements of samples of S420G2+M steel with weld beads performed under water. It has been shown that Temper Bead Welding technique...
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Quadratic Cohen representations in spectral analysis of serration process in Al–Mg alloys
PublicationImportant from mechanical point of view the Portevin–Le Chatelier serration phenomenon is being characterized by a complicated spectral profile. As a typical example of nonstationary processes it demands a special treatment allowing to follow the evolution of energy of stress fluctuations as a function of strain. The authors suggest the utilization of a compact system of quadratic transformations, known as Cohen class, as a technique...
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THE DETERMINATION OF ABRASION RESISTANCE OF SELECTED BIOMATERIALS FOR THE FRICTION PAIRS IN THE HIP JOINT ENDOPROSTHESIS
PublicationThe key requirement for the modern endoprosthesis is high durability of the friction components, which results in long and trouble-free operation in the human body. The durability of currently used endoprosthesis is often limited by tribological wear processes of friction components (e.g. between the head and the acetabular component in a hip joint endoprosthesis) [8, 19, 23, 24]. In order to compare the tribological wear, tribological...
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Comparative in vitro research of the Human Aortic Bioprosthesis
PublicationE valuate of the usefulness and reliability of structures based on the analysis of recorded parameters determining the flow through the Human Aortic Bioprosthesis (HAB) have been dealt with. By flow parameters changes determining the performance environment of prosthesis analyzed change of the motion dynamics of the valve leaflets as a function of pressure, thereby determining the degree of alignment of the prosthesis to the performance...
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Correlation between structural and electrical properties in highly porous (Y,Sr)(Ti,Nb)O3-delta SOFC anodes
PublicationIn order to find a relationship between structural and electrical properties, niobium and yttrium doped SrTiO3 ceramics were prepared via solid-state reaction. The samples were sintered in hydrogen and air conditions. The samples were also fabricated with a pore-former to obtain highly porous specimens. The electrical properties of Nb-doped SrTiO3 samples and yttrium and niobium co-doped SrTiO3 were compared. The comparable electrical...
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CLAY MINERALS – MINERALOGY AND PHENOMENON OF CLAY SWELLING IN OIL & GAS INDUSTRY
PublicationAmong the minerals found in the earth's crust, clay minerals are of the widest interest. Due to the specific properties such as plasticity, absorbing and catalytic properties clay minerals are used in many industries (oil & gas, chemistry, pharmacy, refractory technology, ceramics etc.). In drilling, a phenomenon of swelling clays is frequently observed. It has an important impact on the cementing quality. During the last few decades...