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Search results for: MICRO-ARC OXIDATION
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Investigations of shear localization in granular bodies within an anisotropic micro-polar hypoplasticity
PublicationArtykuł omawia wyniki MES dotyczące stref lokalizacji w materiałach granulowanych podczas ściskania w płaskim stanie odkształcenia. Obliczenia wykonano na bazie mikro-polarnego prawa hipoplastycznego. W obliczeniach uwzględniono anizotrpowość ośrodka w skutek sedymentacji. Analizę wykonano dla różnych kątów napełnienia materiału w stosunku do płaszczyzny obciążenia.
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Effect of MAO coatings on cavitation erosion and tribological properties of 5056 and 7075 aluminum alloys
PublicationTwo ceramic coatings have been applied on 5056 and 7075 aluminum alloy by microarc oxidation (MAO) technology. The mass losses, surface morphologies and the phase constituents of the MAO coatings before and after cavitation tests were examined by means of digital scales, scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. In order to assess the impact of the mechanical properties of the surface layer on...
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublicationGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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Effect of native air-formed oxidation on the corrosion behavior of AA 7075 aluminum alloys
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Aqueous Mechanical Oxidation of Zn Dust: An Inventive Technique for Bulk Production of ZnO Nanorods
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Electrochemical properties of metallated porphyrazines possessing isophthaloxybutylsulfanyl substituents: Application in the electrocatalytic oxidation of hydrazine
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Phosphate and Nitrate Removal from Coffee Processing Wastewater Using a Photoelectrochemical Oxidation Process
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The plasma concentration of advanced oxidation protein products and arterial stiffness in apparently healthy adults
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The products of electro- and photochemical oxidation of 2-hydroxyacridinone, the reference compound of antitumor imidazoacridinone derivatives
PublicationBadano reakcje elektrochemicznego utleniania 2-hydroksyakrydonu, związku modelowego aktywnych przeciwnowotworowo pochodnych imidazoakrydonu. Do badań zastosowano metody woltamperometrii cyklicznej, metodę spektroelektrochemiczną oraz elektrolizę przy kontrolowanym potencjale. Badano też reakcje fotochemicznego utleniania. Badania prowadzono w ramach szerszego problemu poznania przemian aktywacji metabolicznej pochodnych hydroksyakrydonu...
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A Closed Bipolar Electrochemical Cell for the Interrogation of BDD Single Particles: Electrochemical Advanced Oxidation
PublicationA closed bipolar electrochemical cell containing two conductive boron-doped diamond (BDD) particles of size 250 – 350 m, produced by high-pressure high-temperature (HPHT) synthesis, has been used to demonstrate the applicability of single BDD particles for electrochemical oxidative degradation of the dye, methylene blue (MB). The cell is fabricated using stereolithography 3D printing and the BDD particles are located at either...
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Method for prediction of the frost resistance ability of air‐entrained concrete based on the 3D air void characteristics by x‐ray micro‐CT
PublicationIn modern construction, one of the most important factors in the execution of contracts is time. Standard procedures for assessing the frost resistance or concrete are usually very time-consuming and can take up to 40 days. The current paper is experimentally and practically oriented. It presents an alternative testing method, based on air void network, that allows to assess the frost resistance of concrete within just a few days...
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Activated sodium percarbonate-ozone (SPC/O3) hybrid hydrodynamic cavitation system for advanced oxidation processes (AOPs) of 1,4-dioxane in water
PublicationHydrodynamic cavitation (HC) was employed to activate sodium percarbonate (SPC) and ozone (O3) to degrade recalcitrant 1,4-dioxane. The degradation efficiency > 99 % with a rate constant of 4.04 × 10−2 min−1 was achieved in 120 min under the optimal conditions of cavitation number (Cv) 0.27, pH 5, molar ratio of oxidant to pollutant (rox) 8, ozone dose of 0.86 g h−1 under 25 ± 2 °C with initial concentration of 1,4-dioxane 100...
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Characterization and properties of low-friction, multilayered Cr-doped diamond-like carbon coatings prepared by pulse biased filtered cathodic arc deposition
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Obliczanie czasów chłodzenia spawanych łukowo złączy stali odpornych na korozję = Cooling times calculation for stainless steels arc welded joints.
PublicationPrzedstawiono wpływ właściwości cieplnych i parametrów spawania stali odpornych na korozję na czas chłodzenia złącza w zakresie temperatur 800-500oC. Przedstawiono analityczne obliczenia tego czasu. W oparciu o wyniki badań rzeczywistych cykli cieplnych spawania stali typu duplex 2205 opracowano wzór do obliczania czasów chłodzenia złącza 800-500 C.
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Natural deep eutectic solvent based ultrasound assisted liquid-liquid micro-extraction method for methyl violet dye determination in contaminated river water
PublicationSimple and green natural deep eutectic solvent (NADES) based ultrasound assisted liquid-liquid micro-extraction (UA-LLME) method was developed for extraction and determination of methyl violet dye in contaminated river water samples using UV/Vis spectrophotometry. Choline chloride - decanoic acid based natural deep eutectic solvent was used for extraction. Important analytical parameters like pH, deep eutectic solvent volume/phase...
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Chromium‑based metal organic framework for pipette tip micro‑solid phase extraction: an effective approach for determination of methyl and propyl parabens in wastewater and shampoo samples
PublicationAbstract Background A chromium-based metal organic framework was synthesized and employed as an efficient sorbent for pipette tip micro-solid phase extraction and preconcentration of parabens from wastewater and shampoo samples up to sub-ppb level before their spectrophotometric analysis. Results Factors affecting preconcentration including volume and type of solvent, amount of sorbent, number of extraction, and volume and pH of...
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Cascaded doubly fed induction generator for mini and micro power plants connected to grid
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Thermal decomposition of [Cd{SSi(OBut)3}(S2CNC4H8)]2 to CdS “micro-noodles”
PublicationThis work presents studies on thermal degradation of novel heteroleptic complex possessing mixed S-donor ligands, [Cd{SSi(OBut)3}(S2CNC4H8)]2 using TGA, DSC, TGA-IR, SEM and XRD methods.
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Thermoluminescence and optically stimulated luminescence studies on LiMgPO4 crystallized by micro pulling down technique
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Micro-cloud point extraction for preconcentration of Aspirin in commercial tablets prior to spectrophotometric determination
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Application of a Novel Micro-Cloud Point Extraction for Preconcentration and Spectrophotometric Determination of Azo Dyes
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Applications of metal organic framework adsorbents for pipette-tip micro solid-phase extraction
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4,4′-Isopropylidenebis(2,6-dibromophenol) Photocatalytic Debromination on Nano- and Micro-Particles Fe3O4 Surface
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Prediction of cutting forces during micro end milling considering chip thickness accumulation
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Micro-Cloud Point Extraction for Preconcentration of Aspirin in Commercial Tablets Prior to Spectrophotometric Determination
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Novel materials and approaches for solid-phase (micro) extraction in LC-MS-based metabolomics
PublicationMetabolomics offers a unique approach to study biological systems. Liquid chromatography coupled to mass spectrometry serves as a powerful analytical tool to analyze complex mixtures of metabolites. However, successful metabolomic analysis relies on sample preparation. While untargeted analysis traditionally favors nonselective procedures like liquid-liquid extraction (LLE), these methods can compromise analytical performance due...
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FE-investigations of micro-polar boundary conditions along interface between soil and structure
PublicationW artykule zaproponowano mikropolarne warunki brzegowe w strefie kontaktu materiału granulowanego ze ścianą konstrukcji. Warunki te umożliwiają wyznaczenie grubości strefy kontaktu w zależności od szorstkości ściany. Obliczenia wykonano przy zastosowaniu metody elementów skończonych i mikropolarnego modelu hipoplastycznego.
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Effect of grain crushing on shear localization in granular bodies within micro-polar hypoplasticity
PublicationW artykule przedstawiono efekt miażdżenia ziaren na zachowanie się materiału granulowanego podczas ścinania nieskończenie długiej warstwy piasku. Obliczenia wykonano przy pomocy mikropolarnego prawa hipoplastycznego rozszerzonego o efekt miażdżenia ziaren w oparciu o teorię mechaniki zniszczenia. Zbadano wpływ wstępnego zagęszczenia i poziomu naprężeń na strefy lokalizacji.
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Experimental investigations of fracture process in concrete by means of x-ray micro-computed tomography
PublicationW artykule pokazano doświadczalne wyniki badań procesu pękania w betonie stosując mikro-tomografię. Doświadczenia wykonano dla zginanych belek betonowych. Wyniki doświadczalne modelowano stosując MES na bazie modelu z degradacją sztywności sprężystej z nielokalnym osłabieniem. Beton symulowano jako materiał 4-fazowy. Uzyskano dobra zgodność wyników MES z doświadczeniami.
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Experimental investigations on water sorptivity in mortars with the use of X-ray micro-CT system.
PublicationW pracy doswiadczalnej zbadano zjawisko sorpcji wody w pryzmatycznych próbkach zapraw, które jest ściśle powiązane z trwałością materiału. Sorpcyjność oceniana na etapie ustalonym w połączeniu z warunkami zewnętrznymi może być wykorzystana do przewidywania okresu użytkowania. Sorpcyjność początkową i wtórną wody w próbkach zapraw nienasyconych zmierzono w badaniach laboratoryjnych zgodnie z normą amerykańską ASTM C 1585–04. Wpływ...
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Dispersive Micro‐Solid Phase Extraction of Selected Metals in Water and Food Samples Followed by ICP‐OES Analysis: Method Development, Analysis of Real Samples and Greenness Evaluation
PublicationMultiwalled carbon nanotubes (MWCNTs) are well-known adsorbents because of their high surface area, layered and hollow architecture, hydrophobicity, and multiple and easily accessible adsorption sites. In this study, MWCNTs were used for dispersive micro-solid-phase extraction of various metal chelates in environmental and food samples. Different parameters such as concentration of the chelating reagent, the sorbent dosage, the...
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A comparative study on the decolorization of Tartrazine, Ponceau 4R, and Coomassie Brilliant Blue using persulfate and hydrogen peroxide based Advanced Oxidation Processes combined with Hydrodynamic Cavitation
PublicationDecolorization of Ponceau 4R, Tartrazine, and Coomassie Brilliant Blue (CBB) was studied using hybrid processes of hydrodynamic cavitation (HC) with potassium persulfate (KPS) and hydrogen peroxide (H2O2). The different properties of these dyes such as hydrophobicity, molecular structures, and molecular weights provided this opportunity to investigate the effects of these factors by comparing the decolorization values of the dyes....
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SU-FF-T-192: Complete 3D QA for Rapid Arc Using BANG Polymer Gel and OCTOPUS-IQ Fast Laser CT Scanner
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Ce-modified zeolite BEA catalysts for the trichloroethylene oxidation. The role of the different and necessary active sites
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Biofiltration using C. fluminea for E.coli removal from water: Comparison with ozonation and photocatalytic oxidation
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Toxicity of aqueous mixture of phenol and chlorophenols upon photosensitized oxidation initiated by sunlight or vis-lamp
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Establishing the background level of base oxidation in human lymphocyte DNA: results of an interlaboratory validation study
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FeCl3-Modified Carbonaceous Catalysts from Orange Peel for Solvent-Free Alpha-Pinene Oxidation
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Silver nanoparticles induce premutagenic DNA oxidation that can be prevented by phytochemicals from Gentiana asclepiadea
PublicationAmong nanomaterials, silver nanoparticles (AgNPs) have the broadest and most commercial applications due to their antibacterial properties, highlighting the need for exploring their potential toxicity and underlying mechanisms of action. Our main aim was to investigate whether AgNPs exert toxicity by inducing oxidative damage to DNA in human kidney HEK 293 cells. In addition, we tested whether this damage could be counteracted...
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High temperature oxidation behavior of SUS430 SOFC interconnects with Mn-Co spinel coating in air
PublicationIn this study, SUS430 alloy is evaluated for its high temperature corrosion properties as a possible material for interconnects of solid oxide fuel cells (SOFCs). Samples are coated with Mn-Co by commercial physical vapor deposition (PVD) process and oxidized in air for 1250 h at 800 °C. A dense cubic Mn-Co-Fe spinel layer is formed on the surface, showing great effect on corrosion reduction compared with the samples without coating....
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Similarity between enzymatic and electrochemical oxidation of 2-hydroxyac ridinone, the reference compound of antitumor imidazoacridinones.
PublicationPraca jest częścią szerszych badań zmierzających do poznania molekularnego mechanizmu metabolicznej aktywacji przeciwnowotworowej pochodnej imidazoakrydonu, związku C-1311. Celem prezentowanych badań jest (i) zbadanie reakcji enzymatycznego utleniania związku modelowego, 2-hydroksyakrydonu oraz (ii) zbadanie czy zachodzi podobieństwo między przebiegiem reakcji elektrochemicznego i enzymatycznego utleniania tego związku. Podobieństwo...
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Recent advances on magnetic carbon-related materials in advanced oxidation processes of emerging pollutants degradation
PublicationRecently, carbon-related materials have been proposed to improve the charge separation of the photogenerated carriers in the semiconductor matrices’ and surface properties. Carbon-related materials may act as co-catalysts, enhancing the pollutants adsorption on the surface, improving the charge carriers separation and photocatalyst stability and providing more active centres for photocatalytic reactions. This review summarizes...
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The effect of high pressure and sub-zero temperature on total antioxidant capacity and the content of vitamin C, fatty acids and secondary products of lipid oxidation in human milk
PublicationThe objective of this study was to compare of the effects of high pressure of 193 MPa at - 20°C and Low Temperature Long Time pasteurization (LTLT or holder pasteurization, 62,5°C; 30 min) on the content and composition of fatty acids (FAs), concentrations of secondary products of lipid oxidation (TBARS), the total antioxidant capacity (TAC), total vitamin C and ascorbic acid (AsA) content in human milk. It was shown that no significant...
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Porous carbon derived from rice husks as sustainable bioresources: insights into the role of micro-/mesoporous hierarchy in hosting active species for lithium–sulphur batteries
PublicationThe exploration of natural resources as sustainable precursors affords a family of green materials. Exploring highly abundant and available biowaste precursors remaining from food processing throughout a scalable and cost-effective material synthesis path is highly important especially for new materials discovery in emerging energy storage technologies such as lithium–sulphur (Li–S) batteries. Herein, we have produced a series...
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Effect of Mo Content on the Structural, Mechanical, and Tribological Properties of New Zr-Nb-Mo Alloys Obtained by Combining Powder Metallurgy and Vacuum Arc Melting Methods
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Custom FBGs inscription using modified phase mask method with precise micro- and nano-positioning
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Linking Macro- and Micro-structural Analysis with Luminescence Control in Oxynitride Phosphors for Light-Emitting Diodes
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The influence of street conditions on sea buckthorn fruit quality and content of micro- and macronutrients in berries and in soil
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Micro-Abrasive Wear Testing of Surface Engineered Surgical Grade CoCrMo Alloy for Biotribological Applications
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublicationA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...