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Search results for: SOLID ELECTROLYTE INTERPHASE
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Phase investigations of copper based CuZn38Al2MnFe alloy
PublicationW pracy przedstawiono analizę fazową mosiądzu CuZn38Al2MnFe. Wykazano, że obecność fazy Fe4Mn77Si19 powoduje kruchość stopu w teście zginania próbek.
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Comparison of Single and Multi-Population Evolutionary Algorithm for Path Planning in Navigation Situation
PublicationIn this paper a comparison of single and multi-population evolutionary algorithm is presented. Tested algorithms are used to determine close to optimal ship paths in collision avoidance situation. For this purpose a path planning problem is defined. A specific structure of the individual path and fitness function is presented. Principle of operation of single-population and multi-population evolutionary algorithm is described....
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Wear of Electroplated Tools Used for Flat Grinding of Ceramics
PublicationTwo methods for the abrasive properties evaluation, based on the image processing, are presented in the paper. Image processing analysis was developed to evaluate quickly the abrasive properties as the tool wears down. The coefficient based on the image brightness was calculated and additional analysis was based on the number of grains located on the active surface of the tool before and after machining. The active surfaces of...
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Surface Structure of Components Created by Stereolitography
PublicationStereolithography is an additive rapid prototyping method. This method is based on the principle of solidifying a liquid photopolymer (resin) by laser radiation. Models obtained with this method are characterized by a specific surface structure called “stairstep effect”. It causes that, the surface should be processed by additional finishing (postprocessing). To minimize the additional machining process, the model should be set...
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Research on Tool Temperature Dependence on Lapping Grains Size
PublicationCommonly used as a finishing operation, lapping has been used for achieving ultra-high finishes and close tolerances between mating pieces. Its carried out by applying loose abrasive grains between work and lap surfaces, and causing a relative motion between them resulting in a finish of multi-directional lay. The grains activity (sliding and rolling) in the working gap causes not only the material removal but also the temperature...
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The Influence of Workpiece Hardness on Plate Temperature during One Side Lapping
PublicationLapping leads to a surface with low roughness and high precision. Because of required parts accuracy tool flatness is the key to the successful machining. To avoid its excessive thermal expansion, plate temperature research was taken. The goal was to determine the correlation between the basic lapping conditions and wheel temperature. In work Bulsara et al. authors developed model to estimate the maximum and average temperature...
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A simplified model of 3-D pipe system conveying flowing liquid
PublicationThe paper presents a model reduction technique of a 3-D pipe system with flowing liquid. In the analysis and design of control (mechatronic) systems it is useful to work with simple, low order models. A hybrid reduced order model is proposed. The system model consists of two parts, the modal model and the finite element model.
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Influence of Flat Lapping Kinematics on Machinability of Ceramics
PublicationNew tools for flat grinding of ceramics are presented in the paper. Electroplated CBN tools (B64 and B107) were used in a modified single-disc lapping machine configuration. The results from experiments, such as the material removal rate and surface roughness parameters are presented and analyzed. Numerical simulations, based on the model for the shape error and tool wear estimation in machining with flat lapping kinematics, are...
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Technological Problems in Lapping on Flat Surfaces of Ceramic Parts
PublicationThis paper will present the results of research on single-disc lapping of flat surfaces of small ceramic elements. Machining with the use of different tools such as metallic, two-metallic and abrasive-metallic will be analyzed. The basics and techniques of reinforcement of laps will be discussed. The results of the influence of parameters on the surface quality of ceramic conponents (sealing) for three treatments on lapping machines...
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SmallAngle Neutron Scattering Study of the Structure of Mixed Micellar Solutions Based on Nonionic and Two Cationic Surfactants
PublicationThe aggregation in mixed water systems based on nonionic surfactant, i.e., heptaethylene glycol monotetradecyl ether (C14E7), and cationic surfactants, i.e., cetyltrimethylammonium bromide (CTAB), and cetyltrimethylammonium chloride (CTAC) has been investigated using the smallangle neutron scattering method. The preliminary results of the study of the behavior of C14E7 aqueous solutions (for a concentration of 0.17%) when adding...
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Influence of pyrolysis atmosphere on the lithium storage properties of carbon-rich polymer derived SiOC ceramic anodes
PublicationPolymer derived carbon-rich SiOC ceramics are prepared from polysiloxane precursors through a pyrolysis process at 1000 °C using pure argon and argon/hydrogen mixture as pyrolysis atmosphere. The precursor is synthesized from a linear (Si–H)-containing polysiloxane cross-linked with divinylbenzene using hydrosilylation reaction in the presence of a platinum catalyst. Pyrolysis in Ar/H2 mixtures, compared to the treatment under...
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HILS for the Design of Three-Wheeled Mobile Platform Motion Surveillance System with a Use of Energy Performance Index
PublicationCurrent tendency in mechatronic design requires the use of comprehensive development of an environment, which gives the possibility to prototype, design, simulate and integrate with dedicated hardware. The paper discusses the Hardware-In-the-Loop Simulations (HILS) mechatronic technique, used during the design of the surveillance system based on energy performance index. The presented test configuration (physical controller – emulated...
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New ceramic materials derived from pyrolyzed poly(1,2-dimethylsilazane) and starch as a potential anode for Li-ion batteries
PublicationNewmaterialswere obtained by pyrolysis of starch (S) and poly(1,2-dimethylsilazane) (PSN) (weight ratio: PSN/S 30/70) at temperature a) 500 °C, b) 700 °C and c) 900 °C. Ceramic materials were characterized by infrared spectroscopy, TGA, Raman spectroscopy and SEM. New Si\O and shifted Si\C stretching vibration modes emerged confirming direct interaction between silicon originating fromsilazane and oxygen coming fromstarch. The...
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Modelling of Geared Multi-Rotor System
PublicationIn the paper the method of modelling a speed-varying geared rotor system is presented. The proposed approach enables us to obtain an accurate low-order lumped parameter representation of the investigated system. The final model consists of reduced modal models of an undamped beam/torsional shaft system as well as a spatially lumped model of other linear and nonlinear phenomena including gear mesh interaction.
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Copper and cobalt co-doped ceria as an anode catalyst for DIR-SOFCs fueled by biogas
PublicationThe nanocrystalline compounds of Co and Cu co-doped ceria (with up to 20 mol.% of dopants) were fabricated by the reverse microemulsion synthesis method. They were deposited in a form of layers on the surface of SOFC anode in an aim to act as electrochemically active materials for biogas reforming process. Fourier Transformed Infrared Spectroscopy was used to analyze a composition of outlet gases simultaneously with the tests of...
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Ion conduction in beryllium-alumino-silicate glasses doped with sodium or sodium and lithium ions
PublicationElectrical properties of beryllium-alumino-silicate glasses containing sodium ions or sodium and lithium ions were studied with impedance spectroscopy technique over a frequency range from 10 mHz to 1 MHz and at temperature range from 213 to 473 K. The frequency- and temperature-dependent conductivity spectra of individual single alkali glasses were superimposed by means of the Summerfield scaling. Mixed-alkali glasses do not overlap...
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Structure and optical parameters of Eu doped tellurium oxide thin films prepared by reactive magnetron sputtering method
PublicationIn this work the structural properties and photoluminescence of tellurium dioxide thin films doped by europium were described. Thin films were deposited by magnetron sputtering method and simultaneously heated at 200 °C. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the...
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Electronic conductivity in the SiO2-PbO-Fe2O3 glass containing magnetic nanostructures
PublicationThe linear impedance spectra of iron–silicate–lead glass samples were measured in the frequency range from 1 MHz to 1 MHz and in the temperature range from 153 K to 423 K. The structure was investigated by means of XRD and atomic force microscopy. Local electrical and magnetic properties of the samples were tested with the aid of electrostatic force microscopy (EFM) and magnetic force microscopy (MFM). The obtained results show...
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Electrical properties and structure of lead-borate glass containing iron ions.
PublicationThe ac and dc conductivity in iron–lead-borate glass samples was investigated in the frequency range from 1 mHz to 1 MHz and in the temperature range from 153 K to 423 K. The structure was investigated by the means of atomic force microscopy (AFM) and the crystalline phases (if present) were identified by the means of X-ray diffractometry. Two types of ac electrical behaviour were observed. The first group of glass samples which...
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Tailoring of SiOC composition as a way to better performing anodes for Li-ion batteries
PublicationPolymer derived silicon oxycarbide (SiOC) ceramics are investigated as potential anodes for lithiumion batteries. Different SiOC ceramics are prepared by pyrolysis (1000 °C and 1400 °C under controlled argon atmosphere) of polysiloxanes ceramic precursors. Preceramic polymers are synthesized using the sol–gel method. Phenyltriethoxysilane (PhTES) and methyltriethoxysilane (MTES) have been used as starting precursors and mixed with...
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The Influence of Modelling Material Zones on Strains and Stresses at Weld Toe Notch
PublicationThe latest development in the field of welding technology enabled prefabrication of thin-walled sandwich structures in an industrial scale. Sandwich structures fabricated of steel, or aluminium alloy plates and stiffeners are welded with the use of hi-power CO2 lasers. Strength analysis of such structures with the use of finite element method needs proper material modelling.In this paper the material model of steel sandwich panel...
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Multi Parameter Sliding Test Result Evaluation for The Selection of Material Pair for Wear Resistant Components of a Hydraulic motor Dedicated for Use With Environmentally Friendly Working Fluids
PublicationIn the paper the method and results are presented of the testing of tribological performance of a number of hard materials available commercially. The tests consisted in unidirectional sliding with liquid lubrication. The load and velocity regime chosen were similar to a standard four-ball lubricity test with constant velocity and load increasing over time. The regime was modified in such a way that over the initial part of the...
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Influence of Spatial Structures of 316L Stainless Steel on Its Cavitation Erosion Resistance
PublicationCavitation erosion performance of modified macroscopic internal structure 316L stainless steel was investigated. The samples processed by means of SLM method were subjected to cavitation erosion test. The scanning electron microscope Philips 30/ESEM was used to examine morphology of eroded surface.
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Effect of Some Sulphur Additives on The Degradation of 9Cr-1Mo Steel After Its 10 Years Service in The CCR Platforming Unit
PublicationThe work shows the results of the tests of 9Cr-1Mo steel, which was for 10 years operated in the CCR platforming unit in Group Lotos SA in Gdańsk, and then in the laboratory was sulphidised during 166 h at a temperature of 600 °C. Sulphidation was performed in a mixture of H2-H2S gases at the vapour pressure of sulphur 4.1·10-14 atm, so the order of magnitude of vapour pressure was less than that of the dissociation pressure of...
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Nonlinear electrical properties of glass-ceramics nanocomposites containing ferroelectric nanocrystallites of Bi2VO5.5
PublicationNonlinear A.C. impedance measurements were conducted in the 50BiV-50SrBAlO nanocomposite as a function of frequency, temperature and A.C. voltage. This material is ferroelectric below temperature of 730 K, and above 730 K is a good ion-conductor. For this nanocomposite a low A.C. voltage of 1 V rms is enough to observe high nonlinearities. The origin of these nonlinear effects depends on the temperature and frequency. In the high...
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Electrical properties of Na2O-CaO-P2O5 glasses doped with SiO2 and Si3N4
PublicationSodium-calcium-phosphate glasses doped with SiO2 or Si3N4 having similar sodium ion concentrations were prepared by melt quenching. The conductivity was measured by impedance spectroscopy under nitrogen atmosphere in a wide frequency range (10 mHz–1 MHz) and wide temperature range (153–473 K). At 36.6 °C, DC conductivities of all glasses vary between 1.1 ∗ 10−12 and 8.9 ∗ 10−12 S cm−1 and have similar activation energies (between...
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Multicomponent layers for aluminium alloys surface consolidation
PublicationThe main reason of the surface modification of the components such as pistons and cylinder blocks made of cast aluminium alloys is to obtain high hardness, wear and corrosion resistance of the working surface for larger lifetime of the motor-car and aircraft engines. In that aspect, the new conception of development - by hybrid method - of surface layers containing manganese, nitrogen, sulphur (Mn-N-S) and manganese, nitrogen,...
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Determination of ability of hydrotronic systems to start in low ambient temperatures
PublicationPrzedstawiono wyniki badań symulacji komputerowej zespołów układów hydrotronicznych w warunkach szoku termicznego. Pokazano metodę określania zdatności hydrotronicznych zespołów i układów podczas rozruchu w warunkach szoku termicznego.
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High temperature corrosion of evaporator tubes with thermal sprayed coatings
PublicationDegradation examinations of outer surface of low-emission steam boiler evaporator tubes are presented in the paper. Metallographic evaluation of scale morphology, its micro sites chemical composition analysis and distribution of elements on cross sections have been performed. Water-wall tubes were exposed in steam boiler for up to two years period. Common tubes made of 16Mo3 steel suffered sulphide and molten salts corrosions....
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Monitoring of Velocity of Manufacturing Machines Subassamblieas by Means of a DAQ System
PublicationArtykuł dotyczy dokładnych cyfrowych pomiarów prędkości ruchu podzespołów maszyn, realizowanych za pomocą enkoderów kwadraturowych, kart licznikowych DAQ oraz dedykowanych aplikacji pomiarowych DAQ. Przedstawiono koncepcje trzech różnych sposobów takiego pomiaru. W pierwszym sposobie, nazywanym ''częstotliwościowym'', pomiar odbywa się poprzez bramkowane zliczanie impulsów enkodera. Drugi sposób nazywany ''czasowym'' polega na...
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Properties of surface layers of duplex stainless steel after burnishing processes
PublicationStress corrosion cracking resistance of cold worked layers of 25 Cr duplex stainless steel grade UR52N+ has been investigated. The surface layers were performed through burnishing treatment. The residual stresses at surface layers were determined using grazing angle incidence X-ray diffraction method (g-sin2 Ψ). Corrosion tests were performed with the use of Slow Strain Rate Test technique in boiling 35% MgCl2 solution. It has...
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Finishing of Ceramics in a Single-Disk Lapping Machine Configuration
PublicationPrzedstawiono metodę obróbki ceramiki technicznej na zmodifikowanej docierarce jednotarczowej z niezależnym napędem pierścienia prowadzącego. Omówiono przebieg obróbki z wykorzystaniem nowych narzędzi i zastosowaniem ziarna wiązanego.
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Rigid Finite Element Modeling for Identification of Vibrations in Elastic in Elastic Rod Driven by a DC-motor Suplied from a Thyristor Rectifier
PublicationRozdział dotyczy analizy numerycznej układu elektromechanicznego. Układ składa się z silnika zasilanego z jednopołówkowego prostownika tysystorowego i napędzanego tym silnikiem wirującego pręta. Celem obliczeń jest określenie postaci i wielkości drgań pręta, jeśli uwzględniamy jego elastyczność. Dyskretna struktura modelu to łańcuch wielomasowy ciał - sztywnych ciał połączonych bezmasowymi węzłami. Autorzy obliczyli zachowanie...
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Cavitation wearing of the SUPERSTON alloy after laser treatment at cryogenic conditions
PublicationThe purpose of this paper is to demonstrate the method of laser remelting at cryogenic conditions of the SUPERSTON alloy and its influence on microstructure and cavitation wearing. The cavitation test was performed using the rotating disc facility in IPM PAN Gdansk. During the cavitation test, the mass loss of the material with different parameters of laser remelting was determined. Surface and cross-section microstructure of the...
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Research of hydrotronic variable displacement radial piston pump with electro -pneumatic control
PublicationThe paper presents the developed new electro-pneumatic control (pneumotronic) system for hydraulic fixed-displacement radial piston pump. Hydraulic fixed-displacement radial piston pump equipped with the proposed control system changes into hydrotronic variable-displacement radial piston pump. Pump flow rate control is realized by means of programmable logic controller, electro-pneumatic valves, pneumatic cylinders and a sensor.
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Port-Based Modelling of Distributed-Lumped Parameter Systems
PublicationThere in the paper is presented an uniform, port-based approach to modelling of both lumped and distributed parameter systems. Port-based model of the distributed system has been defined by application of bond graph methodology and distributed transfer function method (DTFM). The approach proposed combines versatility of port-based modelling and accuracy of distributed transfer function method. The concise representation of lumped-distributed...
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Effect of the Unit Pressure on the Selection Parameters of Intermetallic Coastings NiAl and Ni3Al after Platic Working
PublicationW artykule omówiono wpływ zgniotu na wybrane parametry warstwy międzymetalicznej NiAl i Ni3Al napawanej na stali C45 podanej obróbce plastycznej poprzez prasowanie na zimno.
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Modal Reduction and Analysis of Gyroscopic Systems
PublicationThe paper introduces the method of the modal reduction of systems that experience the Coriolis acceleration or gyroscopic effect component. In such cases corresponding system equations are non-self-adjoined. To solve the problem modal reduced model is built up for the system without Coriolis acceleration or gyroscopic effect terms. These phenomena are included by application of any lumping technique. Hence, the final reduced model...
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Analysis of Asymmetrical Rolling Process of Multilayer Plates
PublicationW niniejszej pracy przedstawiono wyniki badań numerycznych asymetrycznego procesu walcowania blach wielowarstwowych M1E-Al99,8-AlMg5. Modelowanie numeryczne procesu walcowania blach wielowarstwowych przeprowadzono w programie Forge 2D, którego obliczenia bazują na metodzie elementów skończonych. Przedstawione w pracy wyniki umożliwiły przeprowadzenie analizy procesu walcowania blach wielowarstwowych.
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Surface Roughness Model Components Created by Stereolithography Method
PublicationW pracy przedstawiono charakterystykę powierzchni elementów wykonywanych metodą stereolitografii. Opisano modele chropowatosci stosowane do opisywania powierzcni wraz z prezentacją formuł matematycznych. W oparciu o wyniki badań eksperymentalnych przeprowadzono częściową weryfikację modeli.
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On small signal capacitance spectra of organic diode formed by ITO-palladium phthalocyanine-Al sandwich system
PublicationPraca poświęcona jest widmom małosygnalowej pojemności w zakresie 25 Hz-1 MHz i charakterystyce prądowo-napięciowej planarnego układu utworzonego przez ITO/ftalocyanina palladu/Al.
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Modeling and simulation of tool cycle in manufacturing cell
PublicationThe paper addresses issues concerning modeling and analysis of tool flow within a three-machine manufacturing cell used for small batch manufacturing of a definite spectrum of prismatic parts. The approach utilizes a method for job and tool allocation to work centers with limited number of machines and capacity of tool resources, based on the analysis of formalized relations: job - tool sets required. Selected tool flow control...
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Optimum Control of Gyroscopic Systems
PublicationThe problem of optimum control of transverse rotor vibrations with gyroscopic interactions has been described and solved in the paper. An integral performance index has been defined for such system in order to minimize vibration level of a chosen rotor point. For this reason, an efficient way of finding the weight coefficients of integral performance index for multi-degrees-of-freedom system with gyroscopic interactions has been...
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The effect of pre-hydrogen charging on corrosion behaviour of superduplex stainless steel welded joints
PublicationThe paper presents results of research undertaken to determine the influence of hydrogen on passivity and corrosion resistance of 2507 super duplex stainless steel welded joints. Butt welded joints were made with low heat input using flux corded arc welding (FCAW) method. Coupons of 5.0 x 5.0 mm were cut from the welded joints containing weld metal (WM), heat affected zone (HAZ) and parent metal (PM). Hydrogen was introduced...
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Electronic and ionic relaxations in strontium-borate glass and glass-ceramics containing bismuth and vanadium oxides
PublicationThe topography, microstructure and electrical properties of strontium-borate glass and SBO glass containing bismuth and vanadium oxides, were studied. The structure was measured using X-ray diffraction (XRD), Energy Dispersive X-ray Spectrometer (EDS) and Scanning electron microscope (SEM) methods. The A.C. complex conductivity was investigated as a function of temperature and frequency. The influence of the quantity of bismuth...
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Fabrication and characterization of composite TiO2 nanotubes/ boron-doped diamond electrodes towards enhanced supercapacitors
PublicationThe composite TiO2 nanotubes / boron-doped diamond electrodes were deposited using Microwave Plasma Enhanced Chemical Vapor Deposition resulting in the improved electrochemical performance. This composite electrode can deliver high specific capacitance of 7.46 mF cm‐− 2 comparing to boron-doped diamond (BDD) deposited onto flat Ti plate (0.11 mF cm‐− 2).The morphology and composition of composite electrode were characterized...
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Deformation of the Structural Details of the Components Created by the Rapid Prototyping Method
PublicationThe paper present the results of preliminary research and describes the deformation of construction details within the process of producing small element employing a stereography system. The article discuses a scheme for changes in data conversion. Variation in construction details have been described on the basis of analysing photographs.
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Hardened Steel Surface Waviness Created by Rolling Burnishing Process
PublicationThe surface of the finishing machined parts is defined mainly by roughness parameters. Growing demands on the part, especially mating sliding or rolling, require the specification of additional parameters, such as waviness parameters, particularly when there is significant resistance to seizing or noise reduction. This paper presents surface waviness characteristics of hardened burnished steel.
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The Roughness of the Hardened Steel Surface Created by the Rolling-Burnishing Process
PublicationBurnishing hard materials can be used as an alternative finishing process. this paper presents the results of burnishing hardened steel. The article discusses surface deformation that occurs during this process and depends on the selected parameters of the geometric structure of the force applied for surface burnishing.
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Two kinds of oxygen vacancies in lithium titaniate doped with copper as detected by EPR
PublicationLithium titanate (Li1+xTi2-xO4) doped with Cu2+ ions was synthesized by sol-gel processing method. The structure and morphology are characterized by X-ray Diffraction (XRD), X-ray Photoemission Spectroscopy (XPS), Scanning Electron Microscopy (SEM) and Electron Paramagnetic Resonance (EPR). Spin Hamiltonian parameters describing Zeeman and hyperfine interaction for 63Cu2+ ions were obtained from EPR spectra simulations. The spectra...