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Search results for: GPC/SEC
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A novel methodology for the enantiomeric resolution of methamphetamine, its precursors and intermediates by GC-MS
PublicationImpurity profiling and classification of abused drugs using chiral analytical techniques is of particular interest and importance because of the additional information obtained from this approach. When these methods are applied to the synthesis of illicitly used substances, they can supply valuable information about the conditions/chemicals used in the synthesis. In this study, simultaneous chiral separation of methylamphetamine,...
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The application of TD-GC-FID technique for production of matrix-free reference materials
PublicationIn the last few years particular pressure is exerted on finding new analytical methods which would provide real possibilities of monitoring and control of the state of the environment. Intensive development of analytical techniques for measurements of gaseous media and the negative effects of BTX compounds make it necessary to produce new gaseous reference materials. To prepare the appropriate non- matrix reference material thermal...
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Problems of PAH quantification by GC-MS method using isotope-labelled standards.
PublicationChromatografia gazowa w połączeniu ze spektromerią mas (GC-MS) jest obecnie rutynowo stosowaną metodą w analityce środowiskowej do oznaczania śladowych ilości zanieczyszczeń organicznych. Stosowanie detektora mas sprawia, że wygodnym wzorcem wewnętrznym są stabilne izotopowo analogi oznaczanych związków. Związki te są wykorzystywane do śledzenia i kompensacji strat analitów podczas wykonywania określonych operacji związanych z...
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Molecular Characterization of Growth Hormone-producing Tumors in the GC Rat Model of Acromegaly
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PTR-MS and GC-MS as complementary techniques for analysis of volatiles: A tutorial review
PublicationThis tutorial review is a critical commentary on the combined use of two instrumental analytical techniques, namely GC-MS and PTR-MS. The first mention of such an analytical approach likely appeared after the year 2000 and despite many advantages, it has not been applied very often. Therefore, the aim of this article is to elaborate on the concept of their combined use and to provide a curse tutorial for those considering taking...
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The Analysis of the distribution of available mesopores in cellulosic pulp, using Inverse Size Exclusion Chromatography-ISEC
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Mass spectrometry reveals the presence of specific set of epigenetic DNA modifications in the Norway spruce genome
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Bioindicative potential of shell abnormalities occurring in the clam Macoma balthica (L.) from the Baltic Sea
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A phylogenetic and morphological study of Polystachya sect. Superpositae (Orchidaceae) with description of a new species from Cameroon
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Probability measures of likelihood of diagnosis of the technical state of main combustion engines of sea-going ships
PublicationW artykule uzasadniono potrzebę rozróżniania pojęć wiarygodności diagnozy i trafności diagnozy przy podejmowaniu decyzji eksploatacyjnych. Wyprowadzono wzór na prawdopodobieństwo sformułowania prawidłowej diagnozy jako miary wiarygodności diagnozy. Do wyprowadzenia tego wzoru zastosowano teorię procesów semimarkowskich oraz wzór Bayesa na prawdopodobieństwo warunkowe. Podano także inne probabilistyczne miary wiarygodności diagnozy....
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The bioactivity studies of drug-loaded mesoporous silica-polydimethylsiloxane xerogels using FTIR and SEM/XEDS
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Watershed characteristics and climate factors effect on the temporal variability of mercury in the southern Baltic Sea rivers
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Wind-wave variability in a shallow tidal sea—Spectral modelling combined with neural network methods
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SPATIAL-TEMPORAL DETECTION OF CHANGES ON THE SOUTHERN COAST OF THE BALTIC SEA BASED ON MULTITEMPORAL AERIAL PHOTOGRAPHS
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Elemental and organic carbon in aerosols over urbanized coastal region (southern Baltic Sea, Gdynia)
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Temporal changes in the content of labile and stabile mercury forms in soil and their inflow to the southern Baltic Sea
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High-Resolution Ecosystem Model of the Puck Bay (Southern Baltic Sea)—Hydrodynamic Component Evaluation
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Selective inhibition of cancer cells' proliferation by compounds included in extracts from Baltic Sea cyanobacteria
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Wave‐Induced Surge Motion and Collisions of Sea Ice Floes: Finite‐Floe‐Size Effects
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Distribution of mercury in different environmental compartments in the aquatic ecosystem of the coastal zone of the Southern Baltic Sea
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AN EXPERIMENTAL STUDY OF THE PHOTOCATALYTIC HYDROGEN PRODUCTION IN THE LABORATORY-SCALE SET-UP DEPENDING ON THE PROCESS CONDITIONS
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SELECTING A REPRESENTATIVE DATA SET OF THE REQUIRED SIZE USING THE AGENT-BASED POPULATION LEARNING ALGORITHM
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Set membership estimation of parameters and variables in dynamic networks by recursive algorithms with moving measurment window
PublicationW artykule rozważana jest łączna estymacja przedziałowa zmiennych i parametrów w złożonej sieci dynamicznej w oparciu niepewne modele parametryczne i ograniczoną liczbę pomiarów. Opracowany został rekursywny algorytm estymacji z przesuwnym oknem pomiarowym, odpowiedni dla monitorowania sieci on-line. Okno pomiarowe pozwala na stabilizowanie klasycznego algorytmu rekurencyjnego estymacji i znacznie poprawienie obcisłości estymat....
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How Good Is My Project? Experiences from Projecting Software Quality Using a Reference Set
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Pomiary parametrów i charakterystyk statycznych, dynamicznych, szumowych i termicznych przyrządów z SiC
PublicationW artykule przedstawiono podsumowanie wyników projektu pt. Pomiary parametrów i charakterystyk statycznych, dynamicznych, szumowych i termicznych przyrządów z SiC.
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Rozproszona automatyka SZR w sieciach rozdzielczych średniego napięcia zgodnych z IEC 61850
PublicationNowe możliwości w realizacji automatyki zabezpieczeniowej wnoszą wymagania normy IEC 61850 (PN-EN 61850) publikowanej od roku 2002 - do chwili obecnej. Zasadniczym celem standardu 61850 jest zapewnienie kompatybilności urządzeń pochodzących od różnych producentów. W artykulke przedstawiono najnowsze wymagania dotyczące czasów rekonfiguracji komunikacji po jej fizycznym przerwaniu. Zaproponowano wielopierścieniową topologię i protokół...
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Układy sterowania bramkowego tranzystorów z węglika krzemu SiC JFET w falownikach napięcia
PublicationZastosowanie technologii węglika krzemu (SiC) w falownikach napięcia pozwala na zwiększenie częstotliwości przełączeń oraz temperatury pracy przyrządów półprzewodnikowych. W celu zapewnienia minimalizacji strat oraz określonych właściwości dynamicznych tranzystorów z węglika krzemu wymagane jest stosowanie zaawansowanych układów sterowania bramkowego. W referacie przedstawiono analizę teoretyczną, wyniki badań symulacyjnych oraz...
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Emplying set of experience knowledge structure and decisional DNA to enhance industrial design: conceptual approach
PublicationZaprezentowano koncepcje wspomagania projektowania przemyslowego przy pomocy nowoczenego podejscia do reprezentacji wiedzy w postaci SOEKS oraz Decyzyjnego DNA
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Enhancing set of experiance knowledge structure (SOEKS) with w nearest neighbour algorithm Relief-F
PublicationPrzedstawiono koncepcje uzupelnienia i wpsomagania struktury wiedzy opartej na SOEKS przy pomocy algorytmu przypisujacego wagi atrybutow.
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Sea navigation-based Thai Canal implication: an analysis of its effect on the Vietnamese maritime industry
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Temporal Satellite Images in The Process of Automatic Efficient Detection of Changes of the Baltic Sea Coastal Zone
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Altered Expression of ESR1, ESR2, PELP1 and c-SRC Genes Is Associated with Ovarian Cancer Manifestation
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Effect of pyrolysis temperature on the microstructure and thermal conductivity of polymer-derived monolithic and porous SiC ceramics
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Sex-related patient-reported brain fog symptoms in non-hospitalised COVID-19 patients
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Impact of Movement Tempo Distribution on Bar Velocity During a Multi-Set Bench Press Exercise
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Projektowanie i badania wysokosprawnej ładowarki dwukierunkowej z tranzystorami z węglika krzemu (SiC)
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The influence of street conditions on sea buckthorn fruit quality and content of micro- and macronutrients in berries and in soil
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Computational simulation of motion of a rescue module during its launching from ship at rough sea
PublicationThis paper is a continuation of the work titled : “A comp utational model for simulation of motion of rescue module during its launching from stern ramp of a ship at rough sea”. It presents results of computer simulations of motion of a rescue module with embarked persons during its launching on rollers along stern ramp of a ship at rough sea. The simulations were conducted for a selected ship fitted with a launching ramp , for...
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Efficient Usage of Dense GNSS Networks in Central Europe for the Visualization and Investigation of Ionospheric TEC Variations
PublicationThe technique of the orthogonal projection of ionosphere electronic content variations for mapping total electron content (TEC) allows us to visualize ionospheric irregularities. For the reconstruction of global ionospheric characteristics, numerous global navigation satellite system (GNSS) receivers located in different regions of the Earth are used as sensors. We used dense GNSS networks in central Europe to detect and investigate...
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Real and imaginary motion classification based on rough set analysis of EEG signals for multimedia applications
PublicationRough set-based approach to the classification of EEG signals of real and imaginary motion is presented. The pre-processing and signal parametrization procedures are described, the rough set theory is briefly introduced, and several classification scenarios and parameters selection methods are proposed. Classification results are provided and discussed with their potential utilization for multimedia applications controlled by the...
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Design of a SiC based triple active bridge ceil for a multi-megawatt DC-DC converter
PublicationThe paper describes the design methodology of a novel Triple Active Bridge cell used as the building block for modular DC-DC converters. The intended application is for Medium Voltage Direct Current grids, such as the DC collector for offshore wind farms. The latest generation of SiC MOSFET semiconductors is utilized to operate in the medium frequency range while optimizing the efficiency. The dimensioning of the main cell components,...
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Support Product Development Framework by Means of Set of Experience Knowledge Structure (SOEKS) and Decisional DNA
PublicationIn this paper, we propose a framework to support product development activi-ties by utilizing Set of Experience Knowledge Structure (SOEKS) and Decisional DNA (DDNA). This idea will provide a new direction to researchers working on product development, especially designers and manufacturers. They will be working on the same platform and this will be reducing their communication gap. Once the final idea is perceived about product...
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Rozproszona automatyka SZR w sieciach rodzielczych średniego napięcia zgodnych z IEC 61850
PublicationNorma IEC 61850 została opublikowana w latach 2002 - 2010 w 14 częściach i jest ciągle aktualizowana. Ujednolica ona zasady wymiany danych pomiędzy urządzeniami systemów elektroenergetyki. Zasadniczym celem standardu 61850 jest zapewnienie kompatybilności urządzeń pochodzących od różnych producentów. Standard zakłada zastosowanie mikroprocesorowych urządzeń stacyjnych IED (ang. Intelligent Electronic Devices), takich jak zabezpieczenia...
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Conception of selecting reliability models for taking operating decisionsrelated to sea-going ship´s systems
PublicationPrzedstawiono możliwości podejmowania decyzji dotyczących sytuacji, gdy decydent dysponuje informacją aprioryczną o stanie technicznym urządzeń, na przykład uzyskaną z badań niezawodności urządzeń niezbędnych do wykonania zadania, wyrażoną w formie prawdopodobieństwa. Do opracowania modelu umożliwiającego podejmowanie takich decyzji eksploatacyjnych wykorzystano elementy bayesowskiej statystycznej teorii decyzji.
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Advances in analysis, quantification and modelling of N2O emission in SBRs under various DO set points
PublicationNitrous oxide (N2O), considered a major greenhouse gas (GHG) in wastewater treatment plants (WWTPs), is produced during both nitrification and denitrification processes; hence, it needs to be controlled by internal and external strategies. Various factors, such as DO, temperature, and pH, could be incorporated into the mitigation of emissions in WWTPs. In this research, potential operational strategies were investigated in order...
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Sex contribution to average age at onset of Huntington's disease depends on the number of (CAG)n repeats
PublicationHuntington’s disease (HD) is a hereditary neurodegenerative disorder caused by the extension of the CAG repeats in exon 1 of the HTT gene and is transmitted in a dominant manner. The present study aimed to assess whether patients’ sex, in the context of mutated and normal allele length, contributes to age on onset (AO) of HD. The study population comprised a large cohort of 3723 HD patients from the European Huntington’s Disease...
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Data set generation at novel test-rig for validation of numerical models for modeling granular flows
PublicationSignificant effort has been exerted on developing fast and reliable numerical models for modeling particulate flow; this is challenging owing to the complexity of such flows. To achieve this, reliable and high-quality experimental data are required for model development and validation. This study presents the design of a novel test-rig that allows the visualization and measurement of particle flow patterns during the collision...
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Innovative Urban Blue Space Design in a Changing Climate: Transition Models in the Baltic Sea Region
PublicationWaterfront areas in cities are subject to constant changes. The desire to integrate the transformed waterside areas with the urban fabric involves shaping high-quality public spaces related to water, which are often referred to as urban blue spaces (UBS). The aim of the research was to examine the transformation processes of urban waterfront areas in the Baltic Sea Region and identify emerging transition models and types of blue...
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Application of unmanned USV surface and AUV underwater maritime platforms for the monitoring of offshore structures at sea
PublicationThe operation of offshore structures at sea requires the implementation of advanced systems for their permanent monitoring. There is a set of novel technologies that could be implemented to deliver a higher level of effective and safe operation of these systems. A possible novel solution may be the application of a new maritime unmanned (USV) surface and underwater vehicles/platforms (AUV). Application of such vehicles/platforms...
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Comprehensive evaluation of the carbon footprint components of wastewater treatment plants located in the Baltic Sea region
PublicationFinland and Poland share similar environmental interests with regard to their wastewater effluents eventually being discharged to the Baltic Sea. However, differences in the influent wastewater characteristics, treatment processes, operational conditions, and carbon intensities of energy mixes in both countries make these two countries interesting for carbon footprint (CF) comparison. This study aimed at proposing a functional...