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Search results for: CYANIDE DETERMINATION
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Nowa metoda oznaczania komponentów skomplikowanych mieszanin typu specyfiki farmaceutyczne z wykorzystaniem rozdzielania grupowego i wielowymiarowegej wysokosprawnej chromatografii cieczowej = New method of complex mixtures like pharmaceutical specifics determination using multidimensional high performance liquid chromatography and group type separation
PublicationW pracy porównano różne techniki ekstrakcji/ługowania analitów ze skomplikowanych matryc (2 specyfiki farmaceutyczne) oraz wykazano korzyści ze stosowania różnego typu układów chromatograficznych do ich rozdzielania. Wykorzystano chromatografię wykluczania bez oraz z jednoczesnymi oddziaływaniami sorpcyjnymi i chromatografię w odwróconym układzie faz. Wyniki kilku tego typu analiz były podstawą do rozwiązania układów równań linowych...
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Free-air anomaly grid on the Gulf of Gdańsk
Open Research DataWe present an attempt to determine the accuracy of shipborne gravimetry for the needs of geoid determination. The shipborne gravity campaign, is the beginning of a series of gravimetry measurements in the Polish Exclusive Economy Zone. The campaign was conducted in the area where the accuracy of geoid determination is crucial for the safety of navigation...
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Analysis of free‐air anomalies on the seaway of the Gulf of Gdańsk. A case study
PublicationIn this paper, we present an attempt to determine the accuracy of shipborne gravimetry for the needs of geoid determination. The shipborne gravity campaign, described in this article, is the beginning of a series of gravimetry measurements in the Polish Exclusive Economy Zone. The campaign was conducted in the area where the accuracy of geoid determination is crucial for the safety of navigation on numerous intersecting ships routes....
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Determination of the minimum inhibitory concentration of C-1311 derivatives (C-1296, C-1410, Compound 1, Compound 1-R8) against Candida strains
Open Research DataThe datasets contain the results of determining the minimum inhibitory concentration of imidazoacridinone derivatives against C. albicans ATCC 10231, C. glabrata ATCC 90030, C. krusei ATCC 6258 and C. parapsilosis ATCC 22019 and C. albicans clinical strains by the modified M27-A3 specified by the CLSI.
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Development of gas chromatography - tandem mass spectrometry procedure for development of pesticide residues in honey and honeybee samples
PublicationA new analytical procedure of determination of multiresidue of pesticides based on application of the modified QuEChERS approach at the step of sample preparation and technique GC-MS/MS has been developed and applied for studies the real honey and honeybee samples. Samples were collected from northern Poland (Pomerania). The proposed procedure enables for the determination of 34 and 30 pesticides residues respectively on honey...
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Analysis of pesticide residues in fruits and vegetables using QuEChERS sample preparation method and gas chromatography with electron capture detection
PublicationPesticides are a numerous and diverse group of chemical compounds. They are some of the most toxic substances contaminating the environment, which are used to eliminate pests in agriculture and the household. Despite considerable progress in the development of methods for preparing samples for analysis and for the final determination of analytes, the analysis of pesticides in biological samples continues to present challenges to...
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Mass transfer in Spinning Fluids Reactor — Measurement and prediction
PublicationSpecific mass transfer area (a) and overall volumetric mass transfer coefficient (kLa) are mass transfer parameters commonly used in the description and comparison of various chemical reactors’ constructions. Determination of these was performed for Spinning Fluids Reactor (SFR). Sodium sulfite oxidation in the presence of cobalt ion catalyst was used for the determination of a and kLa. The a and kLa were successful predicted....
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Wojciech Chrzanowski dr hab. inż.
PeopleWojciech Chrzanowski was born in 1952 in Toruń. He completed his studies in Chemical Technology in 1975, getting his MSc in Inorganic Technology (specialty: Anti-Corrosion Protection) At the Faculty of Chemistry, Gdańsk University of Technology (with distinction). Later this year he was employed in the Department of Analytical Chemistry of then Institute of Chemical Engineering and Measuring Techniques, initially as a technical...
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Efficient quadrature for fast oscillating integralof paraxial optics
PublicationThe study concerns the determination of quadrature for the integral solutionof the paraxial wave equation. The difficulty in computation of the integral isassociated with the rapid change of the integrand phase. The developed quadraturetakes into account the fast oscillating character of the integrand. The presentedmethod is an alternative to the commonly used methods based on the use of theFourier transform. The determination...
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Precise Point Positioning Method Based on Wide-lane and Narrow-lane Phase Observations and Between Satellites Single Differencing
PublicationThe issue of using PPP method in position determination was formed in 1997. In most developed methods, ionospheric-free linear combination is used in order to eliminate the impact of the ionospheric delay. However, this approach does not provide the directly determination of the total value of the ambiguities, and the ambiguities for the individual signals. Therefore, in many publications methods of avoiding these deficiencies...
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Polychlorinated Biphenyls (PCBs) and Polycyclic Aromatic Hydrocarbons (PAHs): Sediments and Water Analysis
PublicationUnfavorable side effects of different forms of anthropogenic activities can be found anywhere in the world. One of the basic characteristics of pollutants entering marine and ocean waters is their spread and movement in the global ocean. A portion of the substances entering the marine environment is rapidly degraded by chemical processes occurring in the air, sediments, and water, thereby losing their toxic properties. The biggest...
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AMDDM: Algal Model for the Determination of Diclofenac Mitotoxicity Application of the algal model to determine the non-steroidal anti-inflammatory drugs mitotoxicity – diclofenac as a case study
ProjectsProject realized in Uniwersytet Gdanski according to 2021/41/N/NZ8/00124 agreement from 2022-01-13
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A solid phase extraction–ion chromatography with conductivity detection procedure for determining cationic surfactants in surface water samples
PublicationA new analytical procedure for the simultaneous determination of individual cationic surfactants (alkyl benzyl dimethyl ammonium chlorides) in surface water samples has been developed. We describe this methodology for the first time: it involves the application of solid phase extraction (SPE – for sample preparation) coupled with ion chromatography–conductivity detection (IC-CD – for the final determination). Mean recoveries of...
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A new tool for the evaluation of the analytical procedure: Green Analytical Procedure Index
PublicationA new means for assessing analytical protocols relating to green analytical chemistry attributes has been developed. The new tool, called GAPI (Green Analytical Procedure Index), evaluates the green character of an entire analytical methodology, from sample collection to final determination, and was created using such tools as the National Environmental Methods Index (NEMI) or Analytical Eco-Scale to provide not only general but...
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The optimisation of analytical parameters for routine profiling of antioxidants in complex mixture by HPLC coupled post-column derivatisation
PublicationIntroduction: The wide application of natural and artificial antioxidants in food, cosmetic and pharmaceutical industry as well as the recognition of the importance of food antioxidants for supporting human health created demand for reliable and industrially applicable methods of determining antioxidative activity. This requirement can be fullfilled with the recently proposed HPLC-post-column derivatisation approach enabling the...
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Green chromatography
PublicationAnalysis of organic compounds in samples characterized by different composition of the matrix is very important in many areas. A vast majority of organic compound determinations are performed using gas or liquid chromatographic methods. It is thus very important that these methods have negligible environmental impact. Chromatographic techniques have the potential to be greener at all steps of the analysis, from sample collection...
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OCENA NOŚNOŚCI STAREGO MOSTU ŁUKOWEGO W JAGODNIKU
PublicationArtykuł opisuje przeprowadzoną analizę statyczno-wytrzymałościowa 95-letniego betonowego mostu łukowego zlokalizowanego w Jagodniku w północnej Polsce. Trwałość i wytrzymałość starego betonu są określane na podstawie wybranych właściwości mechanicznych, fizycznych i chemicznych. Program badań laboratoryjnych składał się z następującego zestawu badań: pomiary głębokości strefy skarbonatyzowanej i gęstości w stanie suchym, badania...
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A new time-frequency detection method of stray current field interferenceon metal structures.
PublicationA new detection method has been presented of stray current field interference on underground metal structures. The method employs short time Fourier transformation (STFT). This method of analysis allows determination of signal spectral power density changes (e.g., structure potential) in the function of time. In the paper results have been presented of total time–frequency analysis of a pipeline potential in a stray current field...
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New approaches to cutting resistance estimation of wood cutting process with circular-saw blades
PublicationTheoretical and experimental determination of values of cutting resistance belongs to the basic and simultaneously the most developed field of mechanics of this process. Energetic effects of wood sawing process are mainly calculated on the basis of the specific cutting resistance which, in wood cutting, is a function on a lot of factors. In this paper new method for calculation of cutting resistance is described. The latter method...
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SESSILE DROPLET CONTACT ANGLE OF WATER-Al2O3, WATER-TiO2 AND WATER-Cu NANOFLUIDS
PublicationThe goal of the present work was the experimental determination of the contact angle of droplets of three nanofluids on various substrates. Of particular interest was effect of nanoparticle concentration on droplet contact angle.
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Comparative Greenness Evaluation
PublicationGreenness of analytical procedure is multivariable aspect as many greenness criteria should be taken into consideration. On the other hand, modern analytical chemistry offers dozens of analytical procedures, based on different sample preparation and final determination techniques that are used for the determination of a given analyte in a given matrix. For such complex decision-making processes, multi-criteria decision analysis...
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Determination of flow properties of a serial connection of a directional control valve with (C=5.7, b=0.32) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.1, b=0.14) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=7.3, b=0.49) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.8, b=0.25) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=5.5, b=0.37) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=6.4, b=0.45) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=6.2, b=0.38) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.4, b=0.26) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=3.3, b=0.40) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.0, b=0.11) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.5, b=0.37) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.5, b=0.37) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=4.4, b=0.42) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=5.3, b=0.38) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.2, b=0.38) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=3.3, b=0.40) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.4, b=0.45) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...