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Search results for: UHF MEASUREMENTS
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Electrical conductivity relaxation measurements - oxidation and reduction of BaCe0.6Zr0.2Y0.1Tb0.1O3-δ
Open Research DataThe dataset consists of 2 main catalogs: measurements performed for oxidation/reduction in dry conditions and in humid conditions. For Electrical Conductivity Relaxation (ECR) measurements, platinum reversible electrodes were applied in a four-probe arrangement and the sample was measured in the ProboStat™ measurement system. The ECR measurements were...
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The mechanisms of isobutene hydration yielding tert-butanol catalyzed by a strong mineral acid (H2SO4) and Lewis-Brønsted superacid (HF/SbF5)
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Experimental Study of the Influence of Noise Level on the Uncertainty Value in a Measurement System Containing an Analog-to-Digital Converter
Open Research DataFor newly developed measuring systems it is easy to estimate type B uncertainties based on the technical data of the measuring modules applied. However, it is difficult to estimate A type un-certainties due to the unknown type and level of interferences infiltrating into the measuring sys-tem. This is a particularly important problem for measurements...
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X-ray diffractometry results of the Sr0.90Ti0.30Fe0.70O3-d material before and after H2-TPR measurement
Open Research DataThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr0.90Ti0.30Fe0.70O3-d material. The phase composition of the investigated powders was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder and powder after H2-TPR (temperature programmed...
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X-ray diffractometry results of the Sr0.95Ti0.30Fe0.70O3-d material before and after H2-TPR measurement
Open Research DataThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr0.95Ti0.30Fe0.70O3-d material. The phase composition of the investigated powders was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder and powder after H2-TPR (temperature programmed...
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GC Chromatograms for isomerization of alpha-pinene
Open Research DataData contain results of the catalytic tests for the isomerization of alpha-pinene for the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y,...
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Testing HIADAC high impedance analyzer in Trento University laboratory on Baunier's RC model using 3 wire probe
Open Research DataThe dataset presents impedance spectrum of Baunier's RC model. This object was used to test high-impedance analyzer for diagnostic of anticorossion coatings (HIADAC) realized in the frame of Eureka project E!3174. The impedance spectrum frequency range (1 mHz – 100 kHz) was selected in order to test the whole measureement range of the analyzer. In...
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Testing HIADAC high impedance analyzer in Trento University laboratory on "unknown" object using 2-wire probe
Open Research DataThe dataset presents impedance spectrum of "black-box" object with interesting phase characteristics. This object was used to test high-impedance analyzer for diagnostic of anticorossion coatings (HIADAC) realized in the frame of Eureka project E!3174. The impedance spectrum frequency range (1 Hz – 100 kHz) was selected in order to test the whole measureement...
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SPTNO ceramics measured by XPS method
Open Research DataSPTNO (Sr-Pr-Ti-Ni-O) ceramic were manufactured by solid state reaction, from oxides compounds. Synthesis conducted in air atmosphere at temperature in a range of 800-900 deg. Chemical composition of prepared materials were measured by XPS (X-Ray photoemision spectroscopy) method. UHV OmicronNanotechnology system with 128 channel Argus hemispherical...
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Reactions of (Ph)tBuP-P(SiMe3)Li·3THF with [(PNP)TiCl2] and [MeNacNacTiCl2·THF]. Synthesis of first PNP titanium(IV) complex with phosphanylphosphinidene ligand [(PNP)Ti(Cl){η2-P-P(Ph)tBu}]
PublicationLithium derivative of diphosphane (Ph)tBuP-P(SiMe3)Li (1) was isolated for the first time and investigated in reactions with β-diketiminate (MeNacnac− = [Ar]NC(Me)CHC(Me)N[Ar]; Ar = 2,6-iPr2C6H3) and PNP-pincer (PNP = N[2-PiPr2-4-methylphenyl]2) Ti(III) complexes. The β-diketiminate titanium(III) complex containing phosphanylphosphido ligand [MeNacNacTi(Cl){η2-P(SiMe3)-P(Ph)tBu}] (2) was prepared in reaction of [MeNacNacTiCl2·THF]...
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Potassium Tri-tert-butoxysilanethiolates: Synthesis, Properties, and Crystal and Molecular Structures of [(tBuO)3SiSK]6[THF]2·2THF, {[(tBuO)3SiS]2K2}n, and [(tBuO)3SiSK]4[H2O]4·C6H6
PublicationW reakcji tri-tert-butoksysilanotiolu z potasem otrzymano trzy nowe związki:[(tBuO)3SiSK]6[THF]2·2THF, {[(tBuO)3SiS]2K2}n, i[(tBuO)3SiSK]4[H2O]4·C6H6. Stanowią one dogodne substraty w syntezach kompleksów silanotiolanowych metali przejściowych. Charakteryzują się one również różnorodnością tworzonych układów. Rentgenowska analiza strukturalna wykazała, iż tworzą one trzy typy makrocząsteczkowych układów, w których...
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Selected results of measurements carried out in a ship power station with two generators working in parallel with the use of the NI PXIe-1062Q based measurement system
Open Research DataThe presented dataset is part of research focusing on the assessment of metrological properties of the instrument, Estimator/Analyzer (A/E v.2), developed and made at the Faculty of Electrical Engineering, Department of Marine Electrical Power Engineering, of Gdynia Maritime University. The attached data set contains the results of measurements made...
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Effective perturbation signal and measurement of corrosion rate. Response to the commentary of Diard and co-workers concerning the paper in Corros. Sci. 37, 913 (1995)
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<title>Cavity simulator and controller for VUV free electron laser SIMCON 2.1, part III: I/O ports and measurement results</title>
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A.D.A.M. test (Antibiofilm Dressing's Activity Measurement) — Simple method for evaluating anti-biofilm activity of drug-saturated dressings against wound pathogens
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Graphene oxide thin films deposited on a PCB board - chemical analysis
Open Research DataGraphene oxides based films were measured by X-ray photoemission spectroscopy (XPS) method. TheXPS measurements were carried out with the Omicron NanoTechnology UHV equipment. The hemispherical spectrophotometer was equipped with a 128-channel collector. The XPS measurements were performed at room temperature at a pressure below 1.1 × 10−8 mBar. The...
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Mechanisms of carbon monoxide hydrogenation yielding formaldehyde catalyzed by the representative strong mineral acid, H2SO4, and Lewis–Brønsted superacid, HF/AlF3
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General route for the synthesis of terminal phosphanylphosphido complexes of Zr(IV) and Hf(IV): Structural investigations of the first zirconium complex with a phosphanylphosphido ligand
PublicationReactions of R2P-P(SiMe3)Li with [Cp2MCl2] (M = Zr, Hf) in hydrocarbons yield the related terminal phosphanylphosphidocomplexes [Cp2M(Cl){(Me3Si)P-PR2-jP1}] (R = iPr and tBu). The solid state structures of [Cp2M(Cl){P(SiMe3)-PiPr2-jP1}] (M = Zr, Hf) were established by single crystal X-ray diffraction studies. The phosphido-P atoms adopt almost planar geometries and the phosphanyl P atoms adopt pyramidal geometries. The reaction...
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Burnout Investigation of Small Diameter Tubes Immersed in Nanofluids
PublicationThis paper deals with research into pool boiling critical heat flux (CHF) of water–Al2O3, water–TiO2 and water–Cu nanofluids on horizontal stainless steel tubes. The experiments were conducted under atmospheric pressure. Nanoparticles were tested at concentrations of 0.001%, 0.01%, 0.1% and 1% by weight. Ultrasonic vibration was used in order to stabilize the dispersion of the nanoparticles. Although dispersants were not used to...
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Tadeusz Stolarski prof. dr hab. inż.
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Estimation of the angular position of a two-wheeled balancing robot using a real IMU with selected filters
PublicationA low-cost measurement system using filtering of measurements for two-wheeled balancing robot stabilisation purposes has been addressed in this paper. In particular, a measurement system based on gyroscope, accelerometer, and encoder has been considered. The measurements have been corrected for deterministic disturbances and then filtered with Kalman, α-β type, and complementary filters. A quantitative assessment of selected filters...
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Processed measurements of AuAg nanostructures
Open Research DataExtensive processed UV-vis measurements of AuAg alloyed nanostructures created from thin films. Plasmonic band position dependence on fabrication parameters.
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XPS study of the TiO2-WO2 composites
Open Research DataValence state of W and Ti was measured in a TiO2-WO3 composites with a various composition.Powder samples of pure titanium dioxide, tungsten oxide and mix of 50% titanium oxide and 50% od tungsten oxide were measured. Oxides were annealed at the temperature in the range of 300 Celsius degree up to 900 deg. Measurements were performed by XPS UHV Omicron...
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Measurements of Activity Coefficients at Infinite Dilution for Organic Solutes in the Ionic Liquids N-Ethyl- and N-Octyl-N-methylmorpholinium Bis(trifluoromethanesulfonyl)imide. A Useful Tool for Solvent Selection
PublicationIn recent years, many papers describing ionic liquids (IL) as promising solvents in separation techniques have been published. The conscious choice of appropriate ionic liquid as absorption media in effective extraction of selected types of analytes requires deeper understanding of the analyte−IL interactions. Therefore, intensive research is conducted to determine the values of activity coefficient at infinite dilution, which...
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Electrical performance measurement of reference and SOFC with LSCNT layer fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)
Open Research DataThe dataset contains the electrical IV measurements collected during the cyclic measurements of H2S poisoning in DIR-SOFC with/-out LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.
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Comparative field test for measurement of PM10 dust in atmospheric air using gravimetric (reference) method and b-absorption method (Eberline FH 62-1)
PublicationThe paper presents the results of a field test carried out in Gdansk region between 01-01-2010 and 31-12-2010 in order to demonstrate equivalence of the Eberline FH 62-1 sampler to the reference gravimetric method of suspended PM10 dust measurement. The differences in PM10 dust concentration provided by both methods have been discussed for different seasons of the year. A method of estimation of the correction factors/correction...
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Different Ways to Apply a Measurement Instrument of E-Nose Type to Evaluate Ambient Air Quality with Respect to Odour Nuisance in a Vicinity of Municipal Processing Plants
PublicationThis review paper presents different ways to apply a measurement instrument of e-nose type to evaluate ambient air with respect to detection of the odorants characterized by unpleasant odour in a vicinity of municipal processing plants. An emphasis was put on the following applications of the electronic nose instruments: monitoring networks, remote controlled robots and drones as well as portable devices. Moreover, this paper presents...
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The Effect of Full-Cell Impregnation of Pine Wood (Pinus sylvestris L.) on Changes in Electrical Resistance and on the Accuracy of Moisture Content Measurement Using Resistance Meters
PublicationThe impact of the full-cell impregnation of pine wood was investigated with respect to changes in electrical resistance and the accuracy of moisture content measurement. This study compared the resistance of impregnated and untreated pine timber harvested from the northern part of Poland (Pomeranian region). The wood was impregnated by the vacuum-pressure method. The preservative (TANALITH E 3475) and coloring (TANATONE 3950) agents...
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O wyszukiwaniu niepoprawnych pomiarów w systemach DCS obiektów energetycznych = On search for incorrect measurement results in distributed control systems (DCS) of power objects
PublicationPrzedyskutowano problem rozpoznawania degradacji mierników pomiarowych w systemach DCS dużych obiektów energetycznych, przy równoczesnym występowaniu degradacji eksploatacyjnej urządzeń składowych tych obiektów. Zastosowano sieć neuronową (SNN) o skokowych funkcjach przejścia. Zastosowana SNN wykazała wysoką jakość. Sprawdzono możliwości rozpoznawania obu typów degradacji występującej w zastosowaniu do tzw. degradacji dwukrotnych.
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Corrigendum to “Fatigue life improvement using low transformation temperature weld material with measurement of residual stress” [Int. J. Fatigue 164 (2022) 107137]
PublicationWelding processes often produce high levels of tensile residual stress. Low transformation temperature (LTT) welding wires utilise phase transformation strains to overcome the thermal contraction of a cooling weld. In this paper, the residual stress within each weld was quantified using the milling/strain gauge method, being the strain change measured as the weldment was milled away. The fatigue tests were conducted under uniaxial...
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Measurement report: Spatial variations in ionic chemistry and water-stable isotopes in the snowpack on glaciers across Svalbard during the 2015–2016 snow accumulation season
PublicationThe Svalbard archipelago, located at the Arctic sea-ice edge between 74 and 81∘ N, is ∼60 % covered by glaciers. The region experiences rapid variations in atmospheric flow during the snow season (from late September to May) and can be affected by air advected from both lower and higher latitudes, which likely impact the chemical composition of snowfall. While long-term changes in Svalbard snow chemistry have been documented in...
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Impedance spectra of ZnO varistor type 440 model A ver. M
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 680 model A M ver. 93
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 680 model O M ver. 65 13
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 680 model A M ver. xx
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 280 model A ver. M
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 280 model 0 ver. 89
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 280 model O ver. 68
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 100 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 440 model O ver. 68
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 10 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Impedance spectra of ZnO varistor type 680 model O M ver. 65 60
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 10 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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International Journal of Computational Methods and Experimental Measurements
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IEE PROCEEDINGS-SCIENCE MEASUREMENT AND TECHNOLOGY
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Impedance spectra of ZnO varistor type 280 model O M ver. 89
Open Research DataThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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The Influence of Long-Term Heat Treatment on Microstructure of Zr-Modified Aluminide Coating Deposited by CVD Method on MAR M200+Hf Nickel Superalloy
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The magnetic field measurements in selected places of the industrial building
Open Research DataThe dataset is part of a comprehensive study on the assessment of the electromagnetic field intensity in a building of an operating industrial plant. Detailed results of magnetic field measurements, carried out in selected places of this building, are presented.
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Measuring and Analyzing Audio Levels in Film, Commercials, and Movie Trailers Using Leq(A) Values and the LUFS Loudness Model . Analiza pomiarów dźwięku w filmie oraz w reklamach filmowych z wykorzystaniem modelu głośności
PublicationThe purpose of this paper is to describe the measurement of loudness levels in movies, movie trailers, and commercials displayed before feature films at movie theaters. In the initial section, the paper discusses the issues related to measurement of loudness levels, provides recommendations regarding permissible loudness levels during movie screenings, and mentions the applied units of measurement. The following section of the...
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The loop impedance measurement
Open Research DataThe loop impedance measurement
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Measurements of photoionization of mercury atoms into the 6s 2S1/2, 5d96s2 2D5/2 and 5d96s2 2D3/2 ionic states over the energy range from 10.5 eV to 18.7 eV
PublicationPhotoionization of mercury atoms into the three lowest ionic states, 5d106s 2S1/2, 5d96s2 2D5/2 and 5d96s2 2D3/2 has been studied in the photon energy ranges from their respective thresholds to 18.7 eV. The photoionization spectra were obtained with high energy resolution at an angle of 0° with respect to the polarization vector of the photon beam. The high energy resolution and sensitivity achieved in the measurements permitted...
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Testing HIADAC high impedance analyzer in Trento University laboratory on protective foil using 2-wire probe 24h exposition
Open Research DataThe dataset presents impedance spectrum of anticorrosion foil (coating) protecting aluminium frame . This object was used to test high-impedance analyzer for diagnostic of anticorossion coatings (HIADAC) realized in the frame of Eureka project E!3174. The impedance spectrum frequency range (0.1 Hz – 100 kHz) was selected in order to test the whole...
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Testing HIADAC high impedance analyzer in Trento University laboratory on protective foil using 2-wire probe 48h exposition
Open Research DataThe dataset presents impedance spectrum of anticorrosion foil (coating) protecting aluminium frame . This object was used to test high-impedance analyzer for diagnostic of anticorossion coatings (HIADAC) realized in the frame of Eureka project E!3174. The impedance spectrum frequency range (0.1 Hz – 100 kHz) was selected in order to test the whole...