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Search results for: meldrum's acid
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Advanced oxidation (H2O2 and/or UV) of functionalized carbon nanotubes (CNT-OH and CNT-COOH) and its influence on the stabilization of CNTs in water and tannic acid solution
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Structural Insights into Autoreactive Determinants in Thyroid Peroxidase Composed of Discontinuous and Multiple Key Contact Amino Acid Residues Contributing to Epitopes Recognized by Patients’ Autoantibodies
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Effect of copper and silver modification of NH2-MIL-125(Ti) on the photoreduction of carbon dioxide to formic acid over this framework under visible-light irradiation
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The Stimulating Effect of Rosmarinic Acid and Extracts from Rosemary and Lemon Balm on Collagen Type I Biosynthesis in Osteogenesis Imperfecta Type I Skin Fibroblasts
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An influence of molecular weight, deacetylation degree of chitosan xerogels on their antimicrobial activity and cytotoxicity. Comparison of chitosan materials obtained using lactic acid and CO2 saturation.
PublicationThis paper presents a comparison of the antimicrobial activity and cytotoxicity against L929 cells of chitosan xerogels prepared by dissolving the polymer in a solution of lactic acid (LA) or carbonic acid (CO2) and then freeze-drying. There was no simple relationship between the antimicrobial activity and cytotoxicity of the samples obtained using both techniques (LA and CO2). Chitosan materials obtained by the LA method in a...
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Effect of copper and silver modification of NH2-MIL-125(Ti) on the photoreduction of carbon dioxide to formic acid over this framework under visible-light irradiation
PublicationCu and Ag enhance the photocatalytic activities of metal–organic frameworks (MOFs) toward CO2 conversion because of their CO2 adsorption capacities and effects on the lowest unoccupied molecular orbital (LUMO) overpotentials of MOFs. However, to date, targeted introduction of metals into MOFs to achieve visible (Vis)- light-active photocatalysts for CO2 photoconversion has not been realized. Herein, a series of aminefunctionalized...
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Ultrasound assisted dispersive solid phase microextraction using polystyrene-polyoleic acid graft copolymer for determination of Sb(III) in various bottled beverages by HGAAS
PublicationA new polyoleic acid-polystyrene (PoleS) block/graft copolymer was synthesized and applied as adsorbent for ultrasound assisted dispersive solid phase microextraction (UA-DSPME) of Sb(III) in different bottled beverages and analysis using hydride generation atomic absorption spectrometry (HGAAS). Adsorption capacity of the PoleS was 150 mg g−1. Several sample preparation parameters such as sorbent amount, solvent type, pH, sample...
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Impact of the Alkyl Side Chains of Cations and Anions on the Activity and Renaturation of Lysozyme: A Systematic Study Performed Using Six Amino‐Acid‐Based Ionic Liquids
PublicationThe impact of the structure of ionic liquid on the activity and renaturation of lysozyme from the hen egg white (HEWL) was investigated. A set of six ionic liquids based on morpholinium cation and N-acylated amino acids as anions were exploited. The matrix used was based on two homologous series: one with N-acetyl-L-valinate [Val] as a common anion and morpholinium cation with a different number of carbon atoms in the n-alkyl chain...
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Determination of mefenamic acid in urine and pharmaceutical samples by HPLC after pipette-tip solid phase microextraction using zinc sulfide modified carbon nanotubes
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Application of molecularly imprinted polymer pipette tip micro-solid phase extraction of nalidixic acid and acetaminophen from pills and seawater samples and their determination by spectrophotometry
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Łukasz Kulas dr hab. inż.
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The XRD diffraction patterns of Ce0.9Gd0.1O2 prepared using modified Pechini/EDTA method
Open Research DataThe dataset includes XRD patterns of Ce0.9Gd0.1O2-s nanopowder (nanoparticles) prepared using modified Pechini method consisting of CA (citric acid), PEG (propylene glycol) and EDTA. Exact amount of metal nitrates were dissolved in water followed by addition of gelling agents and heated to 100C. Obtained gel was calcined at 600C for 4h. The powder...
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Hearing aid fitting method based on fuzzy logic processing
PublicationWażnym etapem dopasowania współczesnych aparatów słuchowych jest wyznaczanie charakterystyki dynamiki słuchu. Charakterystyka ta wyznaczana jest na podstawie wyników testu skalowania głośności. Niestety wyniki te wyrażone są w skali kategorii głośności, natomiast aparaty słuchowe wymagają para-metrów numerycznych. Problem ten można rozwiązać za pomocą logiki rozmytej. W niniejszym referacie przedstawiono metodę przetwarzania rozmytego...
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Hearing aid fitting method based on fuzzy logic processing
PublicationWażnym etapem dopasowania współczesnych aparatów słuchowych jest wyznaczanie charakterystyki dynamiki słuchu. Charakterystyka ta wyznaczana jest na podstawie wyników testu skalowania głośności. Niestety wyniki te wyrażone są w skali kategorii głośności, natomiast aparaty słuchowe wymagają para-metrów numerycznych. Problem ten można rozwiązać za pomocą logiki rozmytej. W niniejszym referacie przedstawiono metodę przetwarzania rozmytego...
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Bioethical challenges in postwar development aid: The Rwandan case study
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Automatic assessment of the hearing aid dynamics based on fuzzy logic
PublicationPrzedstawiono podstawy koncepcyjne systemu dopasowania protez słuchu opartego na logice rozmytej. Przeprowadzono dyskusje na temat metody skalowania głośności. Następnie podano szczegóły procesu aproksymacji funkcji przynależności odzwierciedlające słuchowe wrażenia głośności. Załączono wnioski.
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Hydroacoustic ships berthing aid systems in Gdańsk north harbour
PublicationManewry dobijania statków do nabrzeży portowych są trudnymi operacjami, przy których należy uwzględniać m. in. na pływy, wiatry, widzialność, prędkość, masę statku, odległość od pirsu. Ewentualna kolizja z pirsem niesie poważne konsekwencje, szczególnie groźne dla wielkich statków a zwłaszcza tankowców. Referat prezentuje hydroakustyczne systemy kontroli manewrów statków wykonane przez zespół pracowników Katedry Systemów Elektroniki...
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Hydrogen-bonded one-dimensional networks in 1:1 complexes of N,N`-bis(2-pi-rydyl)aryldiamines with anilic acid. Acta Cryst. Sect. C Crystal Struct.Commun.**2002 vol. 58 s. o735-o738, 4 rys. 4 tab. bibliogr. 15 poz. Jednowymiarowe sieci krystaliczne tworzone w wyniku oddziaływań wodorowych pomiędzy N,N`-bis(2-pirydylo)aryloaminami a kwasem anilowym.
PublicationOtrzymano związki kompleksowe kwasu anilowego z N,N`-bis(2-pirydylo)-1,4-diaminobenzenem oraz N,N`-bis(2-pirydylo)-4,4`-diaminobifenylem o stechiometrii1:1, a następnie przeprowadzono analizę rentgenograficzną monokryształów. Wobu przypadkach cząsteczki, wchodzące w skład kompleksu są powiązane ze sobąkonwencjonalnymi oddziaływaniami wodorowymi. Tym samym tworzy się jednowy-miarowa sieć krystaliczna z dziewięcioczłonowym pierścieniowym...
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Modelling of a medium-term dynamics in a shallow tidal sea, based on combined physical and neural network methods
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The Medium Composition Impacts Staphylococcus aureus Biofilm Formation and Susceptibility to Antibiotics Applied in the Treatment of Bone Infections
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Entrepreneurship in small and medium-sized enterprises: Comparative study between Slovakia and Poland for the years 2001–2007
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INDUSTRIAL CLUSTERS AS A DEVICE OF STIMULATION OF COOPERATION AND INNOVATION OF SMALL AND MEDIUM-SIZED ENTERPRISES IN THE AREA OF BIO-ECONOMY
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Internet jako idealne medium dla pomiaru poziomu zaufania społeczeństwa informacyjnego do nowych technologii
PublicationInternet, jak nic dotąd, zrewolucjonizowało urządzenie, jakim jestkomputer oraz komunikacje w świecie. Wynalazki telegrafu, telefonu, radia i komputera stworzyły zdolność bezprecedensowej integracji. Internet stał się niemal natychmiast ogólnoświatowym medium dla współpracy i współdziałania między społeczeństwami, gospodarkami i osobami korzystającymi z komputerów bez względu na położenie geograficzne.
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Tilting pad thrust bearing with novel material selection - experimental comparison of low and medium speed operation
PublicationThe advances in material engineering led to the development of hard carbon based coatings applied in numerous applications in order to prevent or minimize wear of the parts in contact. With Triondur® coatings, the bearing company Schaeffler has succeeded in halving the friction losses in the valve trains of passenger cars. The coatings are optimized for high abrasive wear protection and low sliding friction moments. Altogether...
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Analysis of the selection of low temperature medium for a turbine power plant using ocean thermal energy (OTEC)
PublicationThe paper presents the results and conclusions of numerical calculations modelled in the EES program of a closed OTEC cycle. The following mediums were analysed: ammonia, R32, R41, R404a, R407c, R410a, R423a, R500, R502, R507a and R114, R152a, R234fa, R600, R1234yf, R1234ze. Analogous assumptions were adopted as in the ORC cycle with heat regeneration for dry refrigerants without regeneration for wet refrigerants. Each of them...
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Ciecze jonowe jako medium sorpcyjne w mikroekstrakcji do pojedynczej kropli. Cz.II. Praktyka analityczna
PublicationPomimo rosnącego zainteresowania metodami analitycznymi opartymi na użyciu cieczy jonowych ich sprzężenie wraz z techniką mikroekstrakcji do pojedynczej kropli nie osiągnęło zadowalającej popularności oraz akceptacji ze strony środowiska naukowego.
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Medium-sized cyclic bis(anisylphosphonothioyl)- disulfanes and their corresponding cyclic sulfane-structures and most characteristic reactions
PublicationCyclic 8-, 9-, 10-, and 12-membered bis(anisylphosphonothioyl)disulfanes were synthesized. Next, structurally related 7 to 9-membered cis and trans sulfanes were isolated as a result of sulfur atom extrusion from the parent cyclic disulfanes. The results of the desulfurization of the disulfanes were compared to the results obtained for desulfurization of the respective bis(anisylphosphodithioates). Cyclic disulfanes predominantly...
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Processes and the Resulting Water Quality in the Medium size Turawa Storage Reservoir after 60 Year Usage
PublicationThe Turawa reservoir built on the Mała Panew river is one of important storage reservoirs in Poland. Quite many physico-chemical parameters of water in the reservoir itself and also in the reservoir inflowing rivers at different times of the year were measured and compared. The changes of water characteristics as well as their reasons and consequences were discussed.
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The new silica-based coated SPME fiber as universal support for the confinement of ionic liquid as an extraction medium
PublicationThe new silica-based SPME fiber coating is reported for the first time as universal support purposed to confinement of ionic liquid as an extraction medium. Fiber coating was prepared by the sol-gel process, using potassium silicate (K2SiO3) as a precursor and dimethylformamide (DMF) as a pore-forming medium. The concept of synthesis assumes obtaining a solid porous material on the surface of the glass rod and, being characterized...
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On the influence of a surface roughness on propagation of anti-plane short-length localized waves in a medium with surface coating
PublicationWe discuss the propagation of localized surface waves in the framework of the linear Gurtin–Murdoch surface elasticity and taking into account a roughness of a free boundary. We derive a boundary-value problem for anti-plane motions with curvilinear boundary and surface stresses. Using the asymptotic technique developed earlier, we obtain the form of a localized wave and analyze its amplitude evolution. As the main result we present...
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Analysis of the selection of low-temperature medium for a turbine power plant using ocean thermal energy (OTEC)
PublicationThe paper presents the results and conclusions of numerical calculations modelled in the EES program of a closed OTEC cycle. The following mediums were analysed: ammonia, R32, R41, R404a, R407c, R410a, R423a, R500, R502, R507a and R114, R152a, R234fa, R600, R1234yf, R1234ze. Analogous assumptions were adopted as in the ORC cycle with heat regeneration for dry refrigerants without regeneration for wet refrigerants. Each of them...
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The competencies of a small and medium-sized company owner-manager. Kompe-tencje właściciela-menedżera małego i średniego przedsiębiorstwa. W:Entre-preneurship and small business development in the 21st century. Przedsię-biorczość i rozwój małych i średnich przedsiębiorstw w XXI wieku. Ed. B. Piasecki. Łódź: Uniw. Łódz.**2002 s. 69 - 90 bibliogr. 14 poz.
PublicationArtykuł nawiązuje do charakterystyki przedsiębiorcy w świetle paradygmatukompetencji. Przedstawia obszary kompetencji: zarządzanie celami i czynno-ściami, przywództwo, zarządzanie zasobami ludzkimi, kierowanie podwładnymi ispecjalistyczną wiedzą.
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Discrete and Continuous Dynamical Systems-Series S
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Distinguishing of cocrystals from simple eutectic mixtures: phenolic acids as potential pharmaceutical coformers
PublicationThe multiparameter model comprising 1D and 2D QSPR/QSAR descriptors was proposed and validated for phenolic acid binary systems. This approach is based on the optimization of regression coefficients for maximization of the percentage of true positives in the pool of systems comprising either simple binary eutectics or cocrystals. The training set consisted of 58 eutectics and 168 cocrystals. The solid dispersions collection used...
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Photocatalytic mineralisation of humic acids using TiO2 modified by tungsten dioxide/ hydrogen peroxide
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An assessment of wastewater pollution, treatment efficiency and management in a semi-arid urban area of Pakistan
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Chemistry induced by low-energy electrons in condensed multilayers of pure small organic acids
PublicationPrzedstawiono reakcje indukowane przez niskoenergetyczne elektrony (0.7 - 20 eV) w kondensowanych warstwach kwasu mrówkowego (HCOOH), częściowo deuterowanego kwasu octowego (CH3COOD) oraz kwasu trifluorooctowego (CF3COOD).
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Effects of Dietary n–3 and n–6 Polyunsaturated Fatty Acids in Inflammation and Cancerogenesis
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Targeting mTORs by omega-3 fatty acids: A possible novel therapeutic strategy for neurodegeneration?
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Lawesson's reagent (LR) for direct thionation of hydroxamic acids. Substituent effect on LR reactivity
PublicationOkreślono zakres stosowalności i ogranicznia metody bezpośredniej tionacji kwasów hydroksamowych (HAA) za pomocą odczynnika Lawessona (LR). Przedmiotem badań było 35 HAA o wzorze ogólnym R1CON(R2)OH gdzie: R1 = alkil, aryl, benzyl, etoksykarbonylometylen, cynamyl, heteroaryl, a R2 = alkil, aryl. Ustalono, że wydajności kwasów tiohydroksamowych są niskie, gdy wyjściowy HAA posiada w swojej strukturze duże objętościowo reszty R1...
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Calculations of electron impact ionization cross section for simple biomolecules: formic and acetic acids
PublicationObliczono przekroje czynne na jednokrotną jonizację kwasu mrówkowego oraz kwasu octowego. Obliczenia przeprowadzono używając formalizmu BEB w zakresie energii od progu na jonizację do 400 eV. Wyniki porównano z dostępnymi danymi doświadczalnymi.
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Optical activity of the guest azobenzene molecule generated by inclusion complexation with steroidal bile acids.
PublicationZsyntetyzowano krystaliczne kompleksy inkluzyjne azobenzenu z kwasami cholowym i deoksycholowym. Otrzymane związki inkluzyjne poddano badaniom przy wykorzystaniu spektroskopii dichroizmu kołowego w fazie stałej (KBr). Dodatni efekt Cottona, odpowiadający niskoenergetycznemu przejściu elektronowemu n-pi*, skorelowano z helikalnością M,M skręconej cząsteczki azobenzenu. Ponadto w celach porównawczych zmierzono dichroizm kołowy w...
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Biorefinery Approach for H2 and Acids Production Based on Uncontrolled pH Fermentation of an Industrial Effluent
PublicationIn this work, the feasibility of uncontrolled pH acidogenic fermentation of industrial organic effluent from corn-bioethanol production was studied and modelled by using a Monod-based mathematical model. In order to do that, several tests were carried out at different initial pH values, ranging from 4 to 6. The experimental data showed a pH reduction during the fermentation process due to the generation of short-chain acids. When...
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Microscopic Imaging to Visualize the Distribution of Dietary Nucleic Acids in Food Products of Various Origins
PublicationDietary nucleic acids (dietNAs) are being increasingly recognized as important food components with nutritional value. However, the precise dietary recommendations for dietNAs are limited, because established methods for determining the quantity and nutritional role of dietNAs are still lacking. One of the tools to narrow this gap could be microscopic imaging, as a convenient approach to visualize the abundance and distribution...
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Synthesis of disubstituted 1,3,4,9-tetrahydropyrano-[3,4-b]indole-1-acetic acids derivatives
Publication1,3,4,9-tetrahydropyrano[3,4-b ]indole-1-acetic acid derivatives are of interest for pharmaceutical research as a core structure for synthesis of biological active substance - Etodolac (selective Cyclooxygenase-2 inhibitor, which belongs to the Non-steroidal Anti-inflammatory Drug, NSAID, that shows a clin-ically effective analgesic and anti-inflammatory activity). Here the way of synthesis of two 1,3,4,9-tetrahydropyrano[3,4-b...
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Studies on applicability of new solid-phase microextraction and determination of short - chain monocarboxylic acids
PublicationA convenient approach to monitor the short-chain monocaroboksylic acids (SCAMs) in different samples is gas chromatography (GC) preceded by sample preparation based on solid-phase microextraction (SPME). The fiber with polar coatings were used to extract the SCAMs from headspace of liquid and solid samples. Recently polimeric ionic liquid (PIL) fiber coatings have been proposed to extract volatile organic compounds, minly polar...
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Interactions of telomeric proteins with nucleic acids: sequence recognition on intact and oxidatively damaged telomeres
PublicationTelomeres are complex nucleoprotein assemblies that play a vital role in the maintenance of functional ends of linear chromosomes. Telomeric DNA, composed of tandem repeats of the 5'-TTAGGG-3' motif, solves the so-called end replication problem: as chromosomes shorten with each cell division, no information is lost, and the telomere can be re-extended. In the cell, many protein factors regulate telomere length, nuclear positioning...
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State aid for entrepreneurs at special economic zones
Open Research DataThe dataset encompasses a choice of important legal acts, a list of selected Polish bibliography and a list of important individual sentences issued on the topic of state aid for entreprenuers investing at special economic zones. Thanks to that the reader gets the possibility do acquire basic knowledge on the above mentioned topic.
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Determination of changes in viscosity of hydrogel depending on shear rate (1.1 to 55 s-1).
Open Research DataThe rheological characteristics of hydrogel were made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 25 spindle and shear rates from 1.1 to 55 s-1.
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Determination of changes in viscosity of hydrogel depending on shear rate (1.7 to 34 s-1).
Open Research DataThe rheological characteristics of hydrogel were made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 27 spindle and shear rates from 1.7 to 34 s-1.