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Nonlinear impedance of Bi2VO5.5 glass-ceramic annealed at 423 K was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic annealed at 423 K was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at low temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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Thermgravimetric analysis (TGA) data of cement pastes containing pristine and silica-coated bismuth oxide and gadolinium oxide particles
Open Research DataThermogravimetric (TGA) data of cement pastes after 2, 7 and 28 days. Samples designations: Control, BG, BG-A and BG-B are associated with the specimen names in the associated publication.
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Kontrola jakości ograniczników przepięć wytwarzanych w APATOR S.A.
PublicationArtykuł omawia cykl produkcyjny warystorów tlenkowo - cynkowych (ZnO). Przedstawiono wprowadzone w zakładach Apator S.A. zasady kontroli jakości wraz z przykładowymi wynikami badań dla ograniczników przepięć niskiego napięcia.
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Synteza, badania strukturalne i spektroskopowe kompleksów cynku i kadmu z ligandem tris(2,6-diizopropylofenoksy)silanotiolanowym
PublicationW pracy doktorskiej przedstawiono nowy związek krzemo-siarkowy tris(2,6-diizopropylofenoksy)silanotiolanowy (TDST) zastosowany do syntezy modelowych kompleksów cynku i kadmu, które modelują bezpośrednio środowisko jonu metalu w β anhydrazie węglanowej oraz dehydrogenazie alkoholowej. Zastosowanie związku krzemo-siarkowego tris(2,6-diizopropylofenoksy)silanotiolanowy (TDST) jako liganda do syntezy modelowych kompleksów cynku i kadmu...
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Ekologia- zao
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Diagnostyka niskonapięciowych warystorowych ograniczników przepięć
PublicationW artykule omówiono stosowane w praktyce metody oceny stanu ograniczników przepięć niskiego napięcia. Zestawiono wyniki pomiarów, które umożliwiły określenie stanu technicznego nowych i eksploatowanych warystorów ZnO w zakresie charakterystyki przedprzebiciowej.
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ZT_Technologie ochrony powietrza - laboratorium
e-Learning CoursesObliczanie przygruntowych stężeń zanieczyszczeń. Usuwanie zanieczyszczeń powietrza w procesach absorpcyjnych. Zapobieganie emisji SO2 za pomocą ZnO lub CaCO3. Oczyszczanie powietrza z lotnych związków organicznych: fotokatalityczna degradacja. Powierzchnie samoczyszczące w technologiach ochrony powietrza. Biofiltracja powietrza zanieczyszczonego związkami odorowymi.
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Ultrasound-assisted deep eutectic solvent-based liquid–liquid microextraction for simultaneous determination of Ni (II) and Zn (II) in food samples
PublicationA new approach was developed for the simultaneous pre-concentration and determination of Ni (II) and Zn (II) in food samples. This method is based on ultrasound-assisted liquid–liquid micro extraction using hydrophobic deep eutectic solvent (DES) and 1,10-phenanthroline as chelating agent. The effect of several parameters, such as pH, selection and volume of DES, amount of chelating agent, time of sonication and centrifugation,...
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Równolegle przebiegające procesy separacji pianowej jonów Al(III), Cu(II) i Zn(II) z roztworów ich mieszanin
PublicationMetody flotacji jonowej i precypitacyjnej należą do procesów separacji pianowej, wykorzystujących zdolność selektywnej adsorpcji niektórych składników roztworu na powierzchni międzyfazowej gaz – ciecz. Do zalet separacji pianowej zalicza się m.in. niewysokie koszty inwestycyjne i eksploatacyjne oraz wysoką skuteczność w obróbce roztworów rozcieńczonych. Celem pracy jest ocena wpływu kluczowych parametrów na wydajność i przebieg...
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Concentrations and loads of metals (V, Cr, Mn, Fe, Cu, Zn, As, Rb, Y, Zr) from the cliff erosion to the Gulf of Gdansk
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Wykorzystanie kapusty białej (brassica oleracea var. capitata) do fitoekstrakcji metali ciężkich (zn, cd, cu, pb) z gleby*
PublicationGatunki roślin z rodziny Brassicaceae uważane są za przydatne w fitoremediacjimetali ciężkich z gleby. Przeprowadzone badania mają na celu potwierdzenie zasadności wykorzystaniakapusty białej, odmiany 'Kamienna Głowa' do fitoekstrakcji Zn, Cd, Cu, Pb. Poziomwybranych metali badano w glebie oraz liściach i głąbach kapusty uprawianej na tych glebach,pochodzących z upraw wazonowych (Kraków) oraz polowych (Czapielsk). Zawartość metaliciężkich...
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STUDY OF CuO AND V2O5 EFFECT ON IR SPECTRA OF POLYCRYSTALLINE BISMUTH NIOBATE
PublicationBismuth niobate (BiNbO4) ceramics were fabricated by mixed oxide method and sintered by presureless sintering method. BiNbO4 ceramics doped with V2O5 additive in amount 0.125 wt%, 0.250 wt% and 1 wt% of was sintered at T = 910°C whereas BiNbO4 ceramics doped with 2 wt% of CuO additive was sintered at T = 890°C and T = 910°C. It was found that V2O5 additive improved morphology of the ceramic samples. However, the chemical composition...
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Transmission electron microscope (TEM) and optical microscope images of pristine and silica-coated bismuth oxide and gadolinium oxide particles
Open Research DataCollection of raw transmission electron microscope (TEM) micrographs and optical microscope images used in the associated manuscript. All data in accessible *.tif format. Zip package contains:
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Fabrication of Bi6Fe2Ti3O18 Ceramics by Mixed Oxide Method
PublicationIn the present study Bi6Fe2Ti3O18 (BFTO) ceramics has been fabricated by solid state reaction from the mixture of simple oxides viz. Bi2O3, TiO2 and Fe2O3. Stoichiometric mixture of the powders was thermally analyzed so parameters of the thermal treatment were determined. The EDS measurements have shown conservation of the chemical composition of the ceramic powder after calcination. Hot-pressing method was used for final densification...
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Electrochemical formation of the adduct between antitumor agent C_1311 and DNA nucleoside dG. 75.
PublicationPrzyjmuje się, że metaboliczna aktywacja przeciwnowotworowej pochodnej C_1311 jest procesem koniecznym dla jej aktywności przeciwnowotworowej. Wykazano wcześniej, że taka aktywacja prowadzi do kowalencyjnego wiązania się leku z DNA w komórce nowotworowej. Aby zbadać molekularny mechanizm powyższej reakcji metabolicznej przeprowadzono badania elektrochemicznego utleniania pochodnej C_1311. Wykazano w pracy, że dwa produkty elektrochemicznego...
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The bismuth atom neighbourhood in bismuth-silicate glasses from X-ray absorption experiment
PublicationPraca zawiera wyniki strukturalnej analizy EXAFS lokalnego otoczenia atomów bizmutu w krystalicznym tlenku bizmutu (odmiana alfa) i w szklach bizmutowo-krzemianowych o składzie xBi2O3 (1-x)SiO2,x=0.3, 0.4, 0.5, 0.6. Analizę XA- FS realizowano w oparciu o metodę GNXAS. Otrzymane wyniki porównano z danymi literaturowym.
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A DFT/TD DFT study of the structure and spectroscopic properties of 5-methyl-2-(8-quinolinyl)benzoxazole and its complexes with Zn(II) ion
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Facilitated transport of Zn(II), Cd(II) and Pb(II) ions trough polymer inclusion membranes with calix[4]-crown-6 derivaties
PublicationBadano transport mieszaniny równomolowych ilości jonów Zn(II), Cd(II) i Pb(II)z wodnej fazy azotanowej (cMe=0,001M) przez polimerowe membrany inkluzyjne(PIM) zawierające pochodne kaliks[4]korony-6 jako nośniki jonów. Badany był wpływ różnych podstawników na wydajność procesu. Selektywność transportu przez membrany zawierające jonofory 4 i 5 malała w kolejności Pb(II), Zn(II), Cd(II), natomiast z jonoforem 3 Pb(II), Zn(II)Cd(II)....
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Study on effectiveness of PVC/β-diketone sorbent in removing residue of Zn(II), Cr(III) and Ni(II) from post-galvanic wastewater
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Studies on removal of Zn(II), Cd(II) and Pb(II) ions in polymer inclusion membrane transport with calix[4]-crown-6 derivatives
PublicationZbadano selektywność procesu wydzielania jonów cynku(II), kadmu(II) i ołowiu(II) z wodnych roztworów azotanowych zawierających równomolową mieszaninę tych trzech metali (cMe= 0,01 M) w procesie transportu przez polimerowe membrany inkluzyjne (PIM) przy użyciu w roli przenośników jonów pochodnych kaliks[4]-korony-6. Membrany typu PIM syntezowano z trójoctanu celulozy (nośnik), eteru o?nitrofenylopentylowego (pastyfikator) i pochodnych...
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Simulation investigation of perovskite-based solar cells
PublicationThree models of thin-layer lead-halide perovskite solar cells with different electron-transport layers (TiO2,SnO2,ZnO) were investigatedby the simulation method. The perovskite layer thickness was optimized for all the systems. The analysis of the standard photovoltaic cell performanceparameters at various operating temperatures was performed. The best performance was achieved for the system with theSnO2conductive layer.
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Influence of controlled crystallization and SrF2 content on the structure and properties of Eu3+ doped phosphate glasses
PublicationNew phosphate glasses and glass-ceramics P2O5–Bi2O3–K2O–Nb2O5-SrF2 doped with Eu were synthesized and studied in this work. The influence of the SrF2 content (0–15 mol%) and the parameters of the heat treatment on their structural and optical properties were investigated. For the above purpose, the structural characterization by FTIR spectroscopy and XRD measurements was carried out, which showed a significant effect of SrF2 on...
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Study of Phase and Chemical Composition of Bi1-xNdxFeO3 Powders Derived by Pressureless Sintering
PublicationIn the present paper studies on Bi1xNdxFeO3 for x =0.1-0.4 are reported. The mixed oxide method followed with pressureless sintering was employed for ceramics fabrication. Thermal behavior of stoichiometric mixtures of simple oxide powders, viz. Bi2O3, Nd2O3 and Fe2O3 was studied by simultaneous thermal analysis. It was found that with an increase in neodymium content the weight loss increased from 0.75% to 3.16% for x =0.1 and...
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X-RAY DIFFRACTION STUDY OF BISMUTH LAYER-STRUCTURED MULTIFERROIC CERAMICS
PublicationGoal of the present research was to apply a solid state reaction route to fabricate bismuth layer-structured multiferroic ceramics described with the formula Bi5FeTi3O15 and reveal the influence of processing conditions on its crystal structure and phase composition. Simple oxide powders Bi2O3, TiO2 and Fe2O3 were used to fabricate Aurivillius-type bismuth layer-structured ferroelectrics. Pressureless sintering in ambient air was...
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Coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol – Crystal structures and formation constants in aqueous solution
PublicationStability constants were determined for a series of coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol in aqueous solution. The tendency of histaminol to form chelate complexes has been confirmed by the isolation of several complex species in the monocrystalline form and determination of their molecular structures.
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N,N’-Bis(salicylidene)ethylenediamine (Salen) as an Active Compound for the Recovery of Ni(II), Cu(II), and Zn(II) Ions from Aqueous Solutions
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Pozorne objętości molowe oraz ściśliwości adiabatyczne nadchloranów i chlorków metali szeregu Mn(II) - Zn(II) w N,N-dimetyloacetamidzie
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Experimental data of galvanic electric cells measurements
Open Research DataInternal temperature of an electric cell can be measured and monitored using microsphere-based fiber-optic sensors with thin ALD ZnO coating. Their compact size will allow to integrate them easily and effectively within the electric cells. Utilization of presented sensors allows to detect, in real time, damages to the structure of the sensor head that...
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Współczesne Narzędzia Obliczeniowe I - 2022
e-Learning CoursesKurs dotyczący zadań domowych i projektowych z WNO
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 2.88 mm was measured at 693 K with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of temperature and frequency for Bi2VO5.5 ceramic of thickness 2.52 mm was measured at different A.C. voltage with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 1.63 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 1.63 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 4.03 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 4.03 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 2.91 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.91 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of frequency for Bi2VO5.5 ceramic of thickness 2.88 mm was measured at high temperature range with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage and temperature for Bi2VO5.5 ceramic of thickness 2.52 mm (after first heat-treatment at 913 K) was measured at different frequencies with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Ionic conductivity behavior by activated hopping conductivity (AHC) of barium aluminoborosilicate glass–ceramic system designed for SOFC sealing
PublicationNon-conducting BaO-B2O3-Al2O3-SiO2 parent glasses designed for solid oxide fuel cell (SOFC) sealing applications were prepared using the melt-quenching technique. The glass formation region was determined according to phase equilibrium relations and was found to be in the composition range 70BaO-(x)Al2O3-(10−x)B2O3-20SiO2 where 3.0 < x < 6.0 wt%. The conductivity values obtained conductivity ranged from 10−5 to 10−10 S/cm at temperatures...
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Flowing Liquid Anode Atmospheric Pressure Glow Discharge as an Excitation Source for Optical Emission Spectrometry with the Improved Detectability of Ag, Cd, Hg, Pb, Tl, and Zn
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Nitrogen dioxide gas-sensing detection with GO modified CuO thin films
PublicationGas sensors have been continuously developed over the last few decades for several applications including air quality monitoring, automotive industry and recently for medical use. Gas sensors are usually based on metal oxides (MOXs), such as SnO2, TiO2, ZnO, WO3, CuO. Recently, new materials such as graphene oxide and heterostructures of graphene oxide and metal oxides are utilized for gassensing applications.
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Synthesis and structure of Bi 5 FeTi 3 O 15 ceramics
PublicationAim of the present research was to fabricate and study crystal structure and phase composition of Bi5FeTi3O15 (BTFO) ceramics exhibiting Aurivillius - type structure. By means of simultaneous thermal analysis and X-ray diffraction analysis the process of synthesis of BTFO ceramics has been studied. Mixed oxide method followed by pressureless sintering was used for ceramics preparation. Three endothermic thermal effects have been...
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Solid-contact lead(II) ion-selective electrodes for potentiometric determination of lead(II) in presence of high concentrations of Na(I), Cu(II), Cd(II), Zn(II), Ca(II) and Mg(II)
PublicationLead and its compounds are a serious threat to the environment. Monitoring of this toxic heavy metal is a driving force for the continuous development of novel lead(II) ionophores to be applied in ion-selective electrodes. In this work a highly selective lead(II) ionophore, namely 25,26,27,28-tetrakis(piperidinylthiocarbonylmethylene)-p-tert-butylcalix[4]arene, was used in solid-contact ion-selective electrodes for determination...
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ZT_Technologie ochrony powietrza - laboratorium - Nowy
e-Learning CoursesZajęcia terenowe Oczyszczanie spalin w Porcie Czystej Energii. Obliczanie przygruntowych stężeń zanieczyszczeń. Usuwanie zanieczyszczeń powietrza w procesach absorpcyjnych. Zapobieganie emisji SO2 za pomocą ZnO lub CaCO3. Oczyszczanie powietrza z lotnych związków organicznych. Powierzchnie samoczyszczące w technologiach ochrony powietrza. Biofiltracja powietrza zanieczyszczonego związkami odorowymi. Pomiary wybranych parametrów...
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Adam Boryczko dr hab. inż.
PeopleStudia na Wydziale Mechanicznym Technologicznym Politechniki Gdańskiej w latach 1967 – 1973 oraz dyplom mgr inż. mechanika – Technologia Budowy Maszyn. W latach 1973 – 1975 praca w Zakładzie Doświadczalnym Hydrauliki Okrętowej przy ZUO „HYDROSTER” PP w Gdańsku, stanowiska: technolog badania wyrobów, konstruktor badania wyrobów, konstruktor. Od 1975 r. pracuje w Politechnice Gdańskiej na Wydziale Mechanicznym Technologicznym,...
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Formation of Highly Conductive Boron-Doped Diamond on TiO2 Nanotubes Composite for Supercapacitor or Energy Storage Devices
PublicationIn the present paper, we report the phenomena of the formation of the novel composite nanostructures based on TiO2 nanotubes (NTs) over-grown by thin boron-doped diamond (BDD) film produced in Microwave Plasma Enhanced Chemical Vapor Deposition (PE MWCVD). The TiO2 nanotube array overgrown by boron-doped diamond immersed in 0.1 M NaNO3 can deliver high specific capacitance of 7.46 mF cm−2. The composite electrodes were characterized...
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Nonlinear impedance of Bi2VO5.5 ceramic of thickness 2.52 mm (after second heat-treatment at 913 K) was measured at high temperature range with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm (after second heat-treatment at 913 K) was measured by impedance spectroscopy method.
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Facile synthesis of accordion-like porous carbon from waste PET bottles-based MIL-53(Al) and its application for high-performance Zn-ion capacitor
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Synthesis and characterization of mononuclear Zn(II), Co(II) and Ni(II) complexes containing a sterically demanding silanethiolate ligand derived from tris(2,6-diisopropylphenoxy)silanethiol
PublicationFour heteroleptic complexes of zinc(II), cobalt(II) and nickel(II) containing a monodentate silanethiolate ligand derived from tris(2,6-diisopropylphenoxy)silanethiol (TDST), were prepared and characterized. The geometries of ligands in the complexes are typical: distorted tetrahedral in zinc and cobalt(II) complexes and square planar in nickel(II) compound. Magnetic studies performed for Ni(II) and Co(II) compounds confirm the...
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Właściwości elektryczne szkieł boro-krzemianowych o dużej zawartości tlenku manganu
PublicationW niniejszej pracy podjęto próbę otrzymania klasyczną metodą topienia szkła złożonego wyłącznie z tlenków manganu, krzemu i boru, zawierającego od 10 mol% do 70 mol% tlenku manganu. Na podstawie serii pomiarów wyznaczono zakres składu chemicznego, dla którego możliwe jest otrzymanie stabilnego szkła. Badania struktury otrzymanych próbek wykazały, ˙ze tlenek manganu(II) pełni w układzie rolę głównego tlenku szkłotwórczego w postaci...