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Search results for: MELDRUM'S ACID
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Degradation of bisphenol S – a contaminant of emerging concern - by synergistic ozone and percarbonate based AOP
PublicationDegradation of bisphenol S was studied using ozone activated by sodium percarbonate and the effectiveness of optimized process was compared with the peroxone process. The influence of several factors including sodium percarbonate concentration, ozone dose, pH, and water matrix were investigated. A synergetic coefficient of 3.84 was achieved for the combination of sodium percarbonate and ozone, confirming the effectiveness of this...
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Study of Integer Spin S = 1 in the Polar Magnet β-Ni(IO3)2
PublicationPolar magnetic materials exhibiting appreciable asymmetric exchange interactions can potentially host new topological states of matter such as vortex-like spin textures; however, realizations have been mostly limited to half-integer spins due to rare numbers of integer spin systems with broken spatial inversion lattice symmetries. Here, we studied the structure and magnetic properties of the S = 1 integer spin polar magnet β-Ni(IO3)2...
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Synthesis, structure and properties of novel poly(hydroxyurethane)s obtained by non-isocyanate route
PublicationNon-isocyanate polyurethanes (NIPUs) can be synthesized by polyaddition of five-membered bis(cyclic carbonate)s and primary diamines. NIPUs are an alternative for the commonly used (in the form of foams, elastomers, coatings or fibers) in the industry polyurethanes obtained using toxic and moisture sensitive diisocyanates, polyols and low-molecular weight chain extenders. The main aim of this work was to synthesize non-isocyanate...
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New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublicationNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
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Bee Products and Essential Oils as Alternative Agents for Treatment of Infections Caused by S. aureus
PublicationBacteria of the genus Staphylococcus are important human and veterinary pathogens. A crucial characteristic for this group of bacteria is that they can easily acquire mechanisms of antibiotic resistance for a plethora of antibiotics currently in use for human and animal therapies. Therefore, there is a great need to find novel, non-antibiotic chemotherapeutics with marked antistaphylococcal activity. Promising but still underestimated...
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Degradibility in vitro of polyurethanes based on synthetic atactic poly[)R,S)-3-hydroxybutyrate
PublicationThe aim of the paper was to determine the degradibility of aliphatic polyurethanes in hydrolytic and oxidative solutions. DSC, GPC, density, polymer surface morphology were studied.
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Application of Cohen´s class time-frequency distributions in the Belousov-Zhabotinsky reaction analysis
PublicationPrzedstawiono rezultaty spektralnej analizy rejestrów Biełousowa-Żabotyńskiego za pomocą czasowo-częstotliwościowych metod analizy sygnałów należących do klasy Cohen´a. Przykładowy rejestr zmian potencjału elektrody bromo-selektywnej został poddany analizie z wykorzystaniem rozkładu Wignera-Ville´a oraz rozkładu stożkowego. Zastosowanie powyższych algorytmów pozwoliło na uzyskanie spektrogramów przedstawiających zależność pomiędzy...
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Pomiar obrotów i przemieszczenia cząstek T-S w zlokalizowanej strefie deformacji.
PublicationPrzedstawiono nowe stanowisko do badań eksperymentalnych w warunkach dwuosiowego ściskania z materiałem Taylor-Schneebeli (T-S). Unikatowe stanowisko badawcze, w skali badań mechaniki ośrodków rozdrobnionych w ogóle, wykorzystuje oryginalną technikę pomiarów cyfrowych dla określenia obrotów i przemieszczenia cząstek T-S w skali mikro. Cyfrowa technika pomiarów wykorzystuje konwencjonalny sprzęt wideo kamer lub aparatów...
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Nowy system cyfrowej transmisji sygnału mowy o szybkości 16 kbit/s
PublicationCelem pracy jest przedstawienie nowego systemu cyfrowej transmisji sygnału mowy wykorzystującego kanał cyfrowy o prędkości transmisji 16 kbit/s. Nowa metoda kodowania sygnału mowy zaproponowana w pracy pozwala zmniejszyć czterokrotnie, w porównaniu z telefonią cyfrową, wymaganą szybkość transmisji, przy zachowaniu akceptowanej jakości przesyłanej mowy, a jednocześnie nie wymaga drogich numerycznie algorytmów wykorzystywanych w...
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Modelirovanie i prognozirovanie svoistv betonov s pomoŝ'û iskusstvennyh nejronovyh setej.
PublicationPrzedstawiono podstawowe informacje na temat sieci neuronowych. Pokazano wpływ własciwości kompozycji impregnacyjnych takich jak lepkość, gęstość, temperatura na głębokość wnikania w strukturę betonu a także możliwość wykorzystania sieci neuronowych do przewidywania wytrzymałości betonów impregnowanych.
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Zastosowanie S-funkcji w symulacji trójpoziomowego modulatora SVPWM w programie Simulink
PublicationBlok S-funkcjo w programie Simulink pozwala na efektywne wykorzystanie narzędzi tego środowiska. S-funkcaja napisana w języku C, wprowadzona do schematu symulacyjnego jako blok użytkownika jest odpowiednikiem bloku USERa z programu TCad.
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Cullet As Filter Medium For Swimming Pool Water Treatment
PublicationKontrola jakości wody w basenach kąpielowych może być prowadzona poprzez oczyszczanie wody z uwzględnieniem filtracji i dodawaniemśrodków dezynfekcyjnych. Zanieczyszczenia wody nie zawsze mogą byćskutecznie usuwane przy stosowaniu konwencjonalnych metod uzdatnianiawody. W doświadczeniu zbadano osady powstałe na złożu piaskowym,stwierdzono nieefektywną pracę filtrów piaskowych. Porównano dwazłoża filtracyjne: piasek kwarcowy i...
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Voltage Harmonics Measuring Issues in Medium Voltage Systems
PublicationW rozdziale przedstawiono zagadnienia związane z dokładnością pomiarów zniekształceń harmonicznych napięcia z wykorzystaniem przekładników napięciowych w sieciach średnich napięć.
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Photocatalytic treatment of wastewater generated on small and medium vessels
PublicationW związku z uregulowaniami prawnymi zabronione jest wprowadzanie ścieków szarych z ze statków bezpośrednio do wód morskich. Zanieczyszczenia znajdujące się w tych ściekach muszą być usunięte przed ostatecznym zdeponowaniem. Pozwala na to zastosowanie oczyszczania fotokatalitycznego oraz fotokatalizatorów aktywowanych promieniowaniem z zakresu widzialnego. W artykule przedstawiono pływającą jednostkę badawczą wyposażoną w system...
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ANALYSIS OF MEDIUM TERM WAVE CLIMATE IN A TIDAL BASIN
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Modelling and analysis of medium frequency transformers for power converters
PublicationThe evolutions in power systems and electric vehicles, related to the economic opportunities and the environmental issues, bring the need of high power galvanically isolated DC-DC converter. The medium frequency transformer (MFT) is one of its key components, enabled by the increasing switching frequency of modern power semiconductors like silicon carbide transistors or diodes. The increased operating frequency offers small...
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Polish small and medium enterprises : chances, barries and challenges
PublicationLata dziewięćdziesiąte przyniosły gospodarce polskiej bardzo szybki wzrost sektora małych i średnich przedsiębiorstw. Jego dynamika miała jednak tendencję gasnącą, szczególnie u progu XXI wieku. Wyjaśnienie przyczyn tych zjawisk może stanowić przesłankę dla oceny bieżącej polityki państwa wobec MSP, a także dla formułowania założeń przyszłej polityki na tym obszarze. Prezentowane opracowanie pokazuje, jak działania państwa w zakresie...
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Modeling of the acoustic waves propagation in non-homogeneous medium
PublicationRozważano zagadnienie propagacji fal w ośrodku niejednorodnym. Przedstawiono model matematyczny i przykładowe wyniki badań numerycznych. Model matematyczny zbudowano w oparciu o równanie KZK. Do rozwiązania zagadnienia zastosowano metodę różnic skończonych. Badano zmiany ciśnienia i zmiany widma odpowiednio w ośrodku jednorodnym i niejednorodnym.
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Subcritical Thermodynamic Cycles with Organic Medium and Isothermal Expansion
PublicationThe efffciencies of the Organic Rankine Cycle (ORC) are not very high and only very seldom do they exceed 20%. The increase and optimization of initial parameters and certain modifications of the thermodynamic cycle make it possible to overcome these drawbacks. A new modified cycle has been described and analyzed in detail in the paper. Similarly to the Ericsson cycle for gas turbines, isothermal expansion in the turbine is suggested...
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Resonant Frequencies in Microstrip Structure with Omega Medium Substrate
PublicationThe paper presents the research on a rectangular microstrip structure with multilayer substrate containing dielectric and omega medium layers. The effect of pseudochiral medium layer location in the substrate and its thickness on the resonant frequency of the rectangular microstrip structure is investigated. The numerical analysis of investigated structures is based on expansion of electric and magnetic fields. Utilizing the continuity...
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Determination of Mathematical Model Parameters of a Medium Frequency Transformer
PublicationThe paper presents the results of experimental studies of the medium frequency transformer. The object of the research was a prototype of a single-phase transformer with a core made of ferrite I-core elements and windings made of Litz conductors. The research was carried out to determine the parameters of the transformer's mathematical model. The scope of the tests included determining the magnetic hysteresis loop and measuring...
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Hysteresis modelling of a medium frequency single-phase transformer
PublicationThe article describes a feedback Preisach hysteresis model equivalent circuit implementation of a medium frequency single-phase transformer being a part of a high power and high efficiency DC-DC converter. The macroscopic models of magnetic hysteresis are introduced and the feedback Preisach model is selected for further analysis. The hysteresis model is developed for a prototype transformer and the hysteresis loops are compared...
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Some geomechanical properties of a biopolymer treated medium sand
PublicationSome geomechanical properties of a biopolymer treated medium sand. This paper presents a laboratory assessment of geomechanical properties of sandy soil improved by biopolymer application. Additives (biosubstance) consist of polysaccharides and water. Biosubstance used in the project was xanthan gum, which comes from bacteria Xanthomonas campestris. Triaxial shear compression tests and unconfi ned compression tests were carried...
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Stanisław Galla dr inż.
PeopleStanisław Galla was born in 1970 in Gdańsk. He graduated from the Secondary Technical School of Mechanical and Electrical Engineering in Gdansk (1990). He studied at the Faculty of Electrical Engineering at Gdansk University of Technology (graduated in 1996). His PhD thesis entitled "Methodology for increasing the accuracy of low frequency measurements of periodic disturbance indicators in low voltage networks" was defended in...
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Modification of Bacterial Cellulose with Quaternary Ammonium Compounds Based on Fatty Acids and Amino Acids and the Effect on Antimicrobial Activity
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Rheology studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains rheology measurements carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was performed by melt mass-flow rates (MFR)....
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Electrochemical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains electrochemical investigation on electrodes 3D printed using a new composite composed of poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The presented results contain:1. electrochemical characterisation...
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Mechanical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains mechanical tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was dynamic mechanical analysis (DMA). The measurements...
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In vitro enzyme kinetics and NMR-based product elucidation for glutathione S-conjugation of the anticancer unsymmetrical bisacridine C-2028 in liver microsomes and cytosol: major role of glutathione S-transferase M1-1 isoenzyme
PublicationThis work is the next step in studying the interplay between C-2028 (anticancer-active unsymmetrical bisacridine developed in our group) and the glutathione S-transferase/glutathione (GST/GSH) system. Here, we analyzed the concentration- and pH-dependent GSH conjugation of C-2028 in rat liver microsomes and cytosol. We also applied three recombinant human GST isoenzymes, which altered expression was found in various tumors. The...
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Inactivation of glucosamine-6-phosphate synthase by N3-oxoacyl derivatives of L-2,3-diaminopropanoic acid
PublicationN3-oksoacylowe pochodne kwasu l-2,3-diaminopropanowego zawierające ugrupowanie epoksydowe lub układ sprzężonych wiązań podwójnych inaktywują syntaze glukozamino-6-fosforanu (GlcN-6-P) z S. cerevisiae. Wyniki badań kinetycznych inaktywacji enzymu wskazują na dwuetapowy przebieg tej reakcji, przy czym tworzenie kompleksu enzym:ligand poprzedza nieodwracalną modyfikację enzymu. Badane związki różniły się powinowactwem do centrum aktywnego...
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Synthesis and biological activity of novel mycophenolic acid conjugates containing nitro-acridine/acridone derivatives
PublicationOpracowano warunki reakcji kwasu mykofenolowego z aminowymi pochodnymi akrydyn i akrydonów. Tak otrzymane koniugaty zostały scharakteryzowane, a następnie przebadane in vitro pod względem aktywności przeciwbiałaczkowej oraz immunosupresyjnej.
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On the origin of surfaces-dependent growth of benzoic acid crystal inferred through the droplet evaporation method
PublicationCrystal growth behavior of benzoic acid crystals on different surfaces was examined. The performed experiments documented the existence of very strong influence introduced by polar surfaces as glass, gelatin, and polyvinyl alcohol (PVA) on the growth of benzoic acid crystals. These surfaces impose strong orientation effect resulting in a dramatic reduction of number of faces seen with x-ray powder diffractions (XPRD). However,...
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On the origin of surfaces-dependent growth of benzoic acid crystal inferred through the droplet evaporation method
PublicationCrystal growth behavior of benzoic acid crystals on different surfaces was examined. The performed experiments documented the existence of very strong influence introduced by polar surfaces as glass, gelatin, and polyvinyl alcohol (PVA) on the growth of benzoic acid crystals. These surfaces impose strong orientation effect resulting in a dramatic reduction of number of faces seen with x-ray powder diffractions (XPRD). However,...
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On the origin of surfaces-dependent growth of benzoic acid crystal inferred through the droplet evaporation method
PublicationCrystal growth behavior of benzoic acid crystals on different surfaces was examined. The performed experiments documented the existence of very strong influence introduced by polar surfaces as glass, gelatin, and polyvinyl alcohol (PVA) on the growth of benzoic acid crystals. These surfaces impose strong orientation effect resulting in a dramatic reduction of number of faces seen with x-ray powder diffractions (XPRD). However,...
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Elucidation of the effect of some cholinium amino acid ionic liquids on the thermal and the conformational stability of insulin
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Interspecies distances between propionic acid degraders and methanogens in syntrophic consortia for optimal hydrogen transfer
PublicationA mixed culture from an anaerobic biowaste digester was enriched on propionate and used to investigate interspecies hydrogen transfer in dependence of spatial distances between propionate degraders and methanogens. From 20.3 mM propionate, 20.8 mM acetate and 15.5 mM methane were formed. Maximum specific propionate oxidation and methane formation rates were 49 and 23 mmol mg−1day−1, respectively. Propionate oxidation was inhibited by...
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The usefulness of ascorbic acid degradation to analyze the effectiveness of water filtration in household water filter jugs
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The new esters derivatives of betulin and betulinic acid in epidermoid squamous carcinoma treatment – In vitro studies
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8-Oxo-7,8-dihydroguanine and uric acid as efficient predictors of survival in colon cancer patients
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Modulating D-amino acid oxidase (DAAO) substrate specificity through facilitated solvent access
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Preparation of a Ceramic Matrix Composite Made of Hydroxyapatite Nanoparticles and Polylactic Acid by Consolidation of Composite Granules
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Expression Changes in Fatty acid Metabolic Processrelated Genes in Porcine Oocytes During in Vitro Maturation
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Short-Term Effects of Intra-Articular Hyaluronic Acid Administration in Patients with Temporomandibular Joint Disorders
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The acid strength of the HF/AlX3 Lewis-Brønsted complexes involving various electron acceptors as ligands
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Effect of TiO2 Precursor on the Photoactivity of Fe-C-TiO2 Photocatalysts for Acid Red (AR) Decomposition
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New Insight into the Synthesis and Biological Activity of the Polymeric Materials Consisting of Folic Acid and β‐Cyclodextrin
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Amber extract as a bio‐additive to poly(lactic acid) films: Multimethod analysis of crystallinity and stability
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Preliminary Investigation on Rapid Potassium Efflux from Activated Sludge in Response to Use of Peroxyacetic Acid
PublicationPreliminary research on activated sludge potassium efflux (GGKE - glutathione-gated potassium efflux) as a result of peroxyacetic acid (PAA) dosing were performed. Similarily as in case of chlorine dosing the PAA dosing causes initiation of bacteria defense mechanisms, related to the transformations of glutathione tripeptide, resulting in the increase of potassium ions concentration in the activated sludge environment. In the range...
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Preparation and characterization of activated carbons obtained from the waste materials impregnated with phosphoric acid(V)
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Effects of strongly aggregated silica nanoparticles on interfacial behaviour of water bound to lactic acid bacteria
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