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Wyniki wyszukiwania dla: CLEVENGER APPARATUS, DRYING, DERYNG APPARATUS, DISTILLATION, GC/MS ANALYSIS, LIKENS-NICKERSON APPARATUS
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Mosty tymczasowe typu BAILEY - MS 22-80 w świetle badań in SITU
PublikacjaW pracy przedstawiono i omówiono zakres badań, wybrane modele obliczeniowe, wyniki analiz teoretycznych i badań odbiorowych (próbnych obciążeń o rozszerzonym zakresie), oraz spostrzeżenia dotyczące zachowania się konstrukcji na przykładzie kilku badanych obiektów mostów tymczasowych typu bailey - MS 22-80.
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Two-Dimensional Gas Chromatography Coupled With Mass Spectrometry in Food Analysis
PublikacjaThe development of instrumental analytical techniques provided the opportunity for in-depth characterization of many food matrices. In particular, the use of gas chromatography coupled with mass spectrometry gives impressive results in terms of quality and authenticity testing, conducting food freshness evaluations and contamination assessments. A new variant of gas chromatography, namely two-dimensional gas chromatography (GC...
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Influence of selected CO2 absorption promoters on the characteristics of calcium carbonate particles produced by carbonation of the post-distillation liquid from the Solvay process
PublikacjaThe aim of this work is to compare the effect of selected process parameters, gas flow rate, CO2 absorption promoter concentration and its pKa, on the precipitation of CaCO3 by the gas-liquid method using a model post-distillation liquid from the Solvay process. To ensure effective capture of CO2, the absorption promoters used were ammonia, triethanolamine and triethylamine. The Box-Behnken Design was applied to plan the experiments....
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Quantification of methadone and its metabolites: EDDP and EMDP determined in autopsy cases using LC‐MS/MS
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HPLC–MS/MS method for dexmedetomidine quantification with Design of Experiments approach: application to pediatric pharmacokinetic study
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Składowiska odpadów komunalnych jako źródła emisji zanieczyszczeń do środowiska
PublikacjaCelem pracy było przeprowadzenie badań mających na celu określenie związków uwalnianych do powietrza ze składowisk odpadów komunalnych oraz charakterystyka ich właściwości zapachowych i toksycznych. Próbki powietrza analizowano za pomocą techniki TD-GC-MS. Przeprowadzone badania pozwoliły na zidentyfikowanie następujących związków: styren, benzen, ksylen, toluen, etylobenzen, disiarczek dimetylu, dekan, kwas butanowy i octowy....
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Membrane distillation assisting food production processes of thermally sensitive food liquid items: a review
PublikacjaPhysical separation technologies have become important tool for processing in the current food manufacturing industries, especially for the products containing bioactive compounds thanks to their health benefits in costumers. As for the processing of bioactive food ingredients implies the implementation of integrated systems oriented to their separation, fractionation, and recovery. In this field, membrane distillation (MD), which...
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New insights of nanomaterials usage toward superhydrophobic membranes for water desalination via membrane distillation: A review
PublikacjaMembrane distillation (MD) is a promising technology for seawater desalination due to the ability to process high-salinity waters and the ability to be driven by low-grade or waste heat. However, practical applications of MD membranes are limited by the low vapor flux and fouling problem. Recently, there is a growing interest in developing novel MD membrane materials with enhanced hydrophobicity to improve the efficiency of desalination...
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Badania emisji lotnych związków organicznych z asfaltów drogowych z wykorzystaniem techniki dynamicznej analizy fazy nadpowierzchniowej i chromatografii gazowej sprzężonej ze spektrometrią mas (DHS - GC - MS)
PublikacjaAsfalty drogowe pochodzenia naftowego są wytwarzane z pozostałości z destylacji próżniowej ropy naftowej. Ze względu na częciowy kraking termiczny mający miejsce na etapie destylacji próżniowej oraz jej utleniania (oksydacji) prowadzącego do powstania finalnegoproduktu, w gotowej masie bitumicznej występują lotne związki organiczne. Podczas dalszego wykorzystania asfaltu, na etapie jego ekspedycji oraz budowy dróg, z gorącej masy...
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Main strategies, analytical trends and challenges in LC-MS and ambient mass spectrometry-based metabolomics
PublikacjaA plethora of analytical LC-MS-based methods have been successfully applied to analyses of complex samples of various origin for metabolomics investigations. Over the last ten years, the substantial evolution of ambient mass spectrometry (AMS) techniques has highlighted their tremendous potential in metabolomic studies due to the minimal sample pretreatment requirement and the ability to analyse samples in their native state. This...
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Chemical, Aroma and Pro-Health Characteristics of Kaffir Lime Juice—The Approach Using Optimized HS-SPME-GC-TOFMS, MP-OES, 3D-FL and Physiochemical Analysis
PublikacjaThe study aimed to provide the chemical, aroma and prohealth characteristics of the kaffir lime juice. A procedure using solid-phase microextraction with gas chromatography (SPME-GC-TOFMS) was optimized and validated for the determination of terpenes of kaffir lime. Main physicochemical parameters: pH, vitamin C, citric acid and °Brix were evaluated. Micro- and macro elements were determined using microwave plasma optic emission...
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DNA methylation analysis with methylation‐sensitive high‐resolution melting (MS‐HRM) reveals gene panel for glioma characteristics
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Application and optimization of headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography - flame-ionization detector (GC-FID) to determine products of the petroleum industry in aqueous samples
PublikacjaA simple and solvent-free analytical method has been optimized for the determination of hydrocarbons (C6 - C20) from products of the petroleum industry in aqueous samples. Extraction and analysis was carried out using headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled with flame-ionization detector (GC-FID). A ZB-5 capillary column (30 m × 0.25 mm inner diameter, 0.25 µm film thickness) was used for...
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Zastosowanie techniki LC-MS/MS oraz biotestów w analityce próbek środowiskowych w celu oznaczenia ich potencjału endokrynnego i zawartości wybranych związków endokrynnych
PublikacjaWyniki wielu badań prowadzonych w przeciągu ostatnich lat mogą stanowić podstawę do stwierdzenia, że zanieczyszczenia emitowane do środowiska ze źródeł antropogennych mogą stanowić kolejny rodzaj zagrożenia, z którego nie zdawano sobie sprawy wcześniej. Zanieczyszczeniami takimi są substancje z grupy EDC definiowane jako jakikolwiek czynnik, który wpływa na syntezę, wydalanie, transport, wiązanie, działanie lub wydalanie hormonów...
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Process Control and Investigation of Oxidation Kinetics of Postoxidative Effluents Using Gas Chromatography with Pulsed Flame Photometric Detection (GC-PFPD)
PublikacjaThis article presents the results of investigations on the use of headspace analysis and gas chromatography with pulsed flame photometric detection (HSA-GC-PFPD) to evaluate the effectiveness of oxidation of postoxidative effluents from the production of bitumens. Samples of effluents from the bitumen oxidation unit were used in the experiments. In addition, the kinetics of effluent oxidation was also investigated. The content...
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Local ordering of nano-structured Pt probed by multiple-scattering XAFS
PublikacjaW pracy przedstawiono wyniki analizy MS EXAFS krystalicznej platyny i nanostruktur platyny (klastry o rozmiarach od 1nm do 7nm). Rezultaty analizy masowej platyny (uwzględniające rozkłady dwu i trój-ciałowe) są zgodne z wcześniejszymi danymi strukturalnymi i wibracyjnymi i stały się podstawą do realistycznej analizy EXAFS nanocząstek Pt realizownej w połączeniu z wynikami pomiarów TEM, SEM i XRD. Badaniom poddano nanocząstki Pt...
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Comparison of Quality Evaluation of Agricultural Distillates Using Prototype of Electronic Nose and Fast/Flash GC
PublikacjaThe paper presents the results of investigation on quality evaluation of agricultural distillates using a prototype of electronic nose instrument and a commercial electronic nose of Fast/Flash GC type – HERACLES II. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co.. In case of the prototype volatile fraction of the agricultural distillate was prepared via barbotage process. HERACLES II analysed the...
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Simple SIR models with Markovian control
PublikacjaWe consider a random dynamical system, where the deterministic dynamics are driven by a finite-state space Markov chain. We provide a comprehensive introduction to the required mathematical apparatus and then turn to a special focus on the susceptible-infected-recovered epidemiological model with random steering. Through simulations we visualize the behaviour of the system and the effect of the high-frequency limit of the driving...
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New data acquisition system for birch sap concentrate production using the reverse osmosis technology
PublikacjaThe work presents a simple electronic device that helps to monitor the basic parameters of the reverse osmosis (RO) system during the concentration of birch tree sap. The construction costs are low (around 150 Euro) but the functionality of the device is high. It has an in-build two channel conductometer and can measure the volumetric flow rate of two streams of liquids. The collected data are transmitted wirelessly via Bluetooth...
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Contact angle of the ferronanofluid and influence of the magnetic field on the drying droplet
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Concentration of Potentially Bioactive Compounds in Italian Extra Virgin Olive Oils from Various Sources by Using LC-MS and Multivariate Data Analysis
PublikacjaHigh quality extra virgin olive oils represent an optimal source of nutraceuticals. The European Union (EU) is the world’s leading olive oil producer, with the Mediterranean region as the main contributor. This makes the EU the greatest exporter and consumer of olive oil in the world. However, small olive oil producers also contribute to olive oil production. Beneficial effects on human health of extra virgin olive oil are well...
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Fidelity thresholds in single copy entanglement distillation
PublikacjaRozważono różne aspekty destylacji zaszumionego splątania oraz pewne stowarzyszone efekty w kwantowej korekcji błędów. W szczególności pokazano, że w przypadku gdy dozwolona jest komunikacja klasyczna w jedną stronę oraz współdzielony stan kwantowy dxd nie jest czysty, to istnieje próg dla optymalnego ułamka F stanu, który może być otrzymany w procesie destylacji na jednej kopii. Wynika z tego, że aby otrzymać (probabilistycznie)...
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Calcium sulphate scaling in membrane distillation process
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Separation of saline oily wastewater by membrane distillation
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Fouling in direct contact membrane distillation process
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Chemical pretreatment of feed water for membrane distillation
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The assessment of microorganism growth in the membrane distillation system
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The long-term studies of osmotic membrane distillation
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Osmotic MD and other membrane distillation variants
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Membrane cleaning and pretreatments in membrane distillation – a review
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Long-term performance of membrane distillation process
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Effectiveness of Water Desalination by Membrane Distillation Process
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Concentration of FeSO4 spent solutions by membrane distillation
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublikacjaOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Quantification and distribution of 4-fluoroisobutyryl fentanyl (4-FiBF) in postmortem biological samples using UHPLC–QqQ-MS/MS
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Elucidation of transformation pathway of ketoprofen, ibuprofen, and furosemide in surface water and their occurrence in the aqueous environment using UHPLC-QTOF-MS
PublikacjaThe identification and determination of transformation products (TPs) of pharmaceuticals is essential nowadays, in order to track their fate in the aqueous environment and, thus, to estimate the actual pollution. However, this is a challenging task due to the necessity to apply high-resolution instruments enable to detect known and unknown compounds. This work presents the use of liquid chromatography quadrupole time-of-flight...
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A novel method of Mycobacterium tuberculosis complex strain differentiation using polymorphic GC-rich gene sequences.
PublikacjaTuberculosis is one of the leading infectious diseases. In this work, a new genotyping method of Mycobacterium tuberculosis (Mtb) complex strain is presented. 27 Mtb genomes were analyzed for the presence of length polymorphism within polymorphic GC-rich gene sequences. Four genes, Rv3345c, Rv3507, Rv0747 and Rv3511, showing variation in length depending on the Mtb strain were selected for designing primer sequences flanking variable...
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The Use of Liquid Crystal Thermography an Image Processing in Heat and Fluid-Flow Research
PublikacjaLiquid crystal thermography (LCT) have been used in many technical, industrial and biomedical applications [1]. During over 20 years it has been successfully applied in Department of Energy and Industrial Apparatus at Gdansk University of Technology for visualization of steady-state and transient temperature fields. In order to demonstrate feasibility of LCT techniques in practical heat transfer contexts, the authors have performed...
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TIME-OF-FLIGHT DIFFERENTIAL ELECTRON SCATTERING FROM MOLECULAR TARGETS: BENCHMARK CROSS SECTIONS
PublikacjaWe report time-of-flight differential cross section (DCS) measurements for the electron impact excitation transition in H2. In this work, agreement between available theory and experiment is excellent overall, and marks a transition in electron molecule scattering where differential scattering of excitation is found to be in such precise agreement. We also prove that the newly built apparatus can be used for accurate measurement...
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. II. Technika PTR – MS – ciekawe rozwiązanie metodyczne w zakresie spektrometrii mas
PublikacjaTechnika spektrometrii mas stanowi niezwykle istotne narzędzie badawcze, umożliwiające uzyskanie wielu cennych informacji, dotyczących składu chemicznego wielu próbek rzeczywistych pochodzenia biologicznego, farmaceutycznego i spożywczego. Spektrometr mas zazwyczaj pełni role detektora w przypadku stosowania połączenia z urządzeniami chromatograficznymi (GC, LC). Dzięki zastosowaniu pewnych modyfikacji aparaturowych i metodycznych,...
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Ekspertyza techniczna dot. stref zakotwień kabli sprężających – obiekt MS-6 w ciągu S7
PublikacjaOpracowanie zawiera wyniki badań i symylacji MES na temat stref zakotwień wewnętrznych kabli sprężenia podłużnego oraz wskazuje na przyczyny przemieszczenia biernych bloków kotwiących wewnętrznych kabli sprężenia podłużnego przęsła 7-8 mostu MS-6 zlokalizowanego w drogi krajowej S-7 na odcinku Miłomłyn – Olsztynek.
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Late cultivars of cabbage can better cope with cadmium- involved stress than early one
PublikacjaThe usefulness of white cabbage (Brassica oleracea ssp. capitata L. f. alba) for phytoremediation of heavy metals (cadmium and zine) due to the rapid growth and a large biomass of its heads has been already described (Bączek-Kwinta et al., 2011. Kusznierewicz et al., 2012). As the photosynthetic apparatus supplies the whole plant with sugars necessary for various physiological processes and, in consequence, results in the yield,...
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Chosen aspects of muscle biomechanics
PublikacjaConsidering a striated skeletal muscle as a different properties mechanical system, one can understand series of important phenomena happening in a real muscle phenomenon of muscle: 1) force delivery to skeletal apparatus through tendons; 2) changing of exerted muscle belly mass distribution with regards to skeletal apparatus; 3) beginning drop of muscle force. A disregard of first phenomenon causes an impossibility to explain...
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DESIGN LOGICAL LINGUISTIC MODELS TO CALCULATE NECESSITY IN TRUCKS DURING AGRICULTURAL CARGOES LOGISTICS USING FUZZY LOGIC
Publikacja: The study is aimed to develop the logic-linguistic models to design a number of rules for the correct calculation of the vehicles needed, taking into account the technical, technological, and weather and climate conditions of the harvesting and transport complex. The article has shown that the construction of the design of logic-linguistic models was not performed earlier to solve the problem of the agro-industrial production...
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The use of HPLC-Q-TOF-MS for comprehensive screening of drugs and psychoactive substances in hair samples and several “legal highs” products
PublikacjaNon-targeted screening of drugs present in herbal products, known as “legal high” drugs and in hair as a biological matrix commonly used in toxicological investigations was accomplished with the use of high pressure liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (HPLC-Q-TOF-MS). In total, 25 and 14 therapeutical drugs and psychoactive substances/metabolites were detected in investigated hair samples...
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Quantification of DNA Modifications Using Two-Dimensional Ultraperformance Liquid Chromatography Tandem Mass Spectrometry (2D-UPLC-MS/MS)
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Cavitation Erosion of Nodular Cast Iron - Microstructural Effects
PublikacjaThe paper deals with susceptibility of nodular cast iron with ferritic-pearlitic matrix on cavitation erosion. Cavitation tests were carried out with the use of a cavitation erosion vibratory apparatus employing a vibration exciter operated at frequency of 20 kHz. The study allowed to determine the sequence of subsequent stages in which microstructure of cast iron in superficial regions is subject to degradation. The first features...
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Photoelectron spectroscopy of brominated derivative of pyrimidine: 2-bromopyrimidine
PublikacjaIn this study the brominated derivative of pyrimidine, 2-bromopyrimidine, was investigated by photoelectron spectroscopy. Outer valence photoelectron spectra recorded at 21.22, 45 and 100 eV photon energy for this compound are presented. The recorded spectra have a higher resolution than that previously reported in the literature. The bromine 3d and 3p edge photoelectron spectra have also been recorded in a photon impact experiment...
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Degradation of Polypropylene Membranes Applied in Membrane Distillation Crystallizer
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Application of vacuum membrane distillation for concentration of organic solutions‡
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