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Wyniki wyszukiwania dla: SOLID-PHASE SYNTHESIS
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Investigation of sour substances by a set of all-solid-state membrane electrodes
PublikacjaTestowano elektrody typu all solid state (ASS) w roztworach elektrolitów zawierających substancje o smaku kwaśnym. Elektrody typu ASS zawierają dwa typy membran. Badano wpływ grubości membrany oraz stosunku związek lipofilowy/ chlorek poliwinilu na odpowiedzi elektrod. Stwierdzono, że grubość elektro aktywnego polimeru, nie ma wpływu na czułość i stabilność elektrod w przeciwieństwie do grubości membrany składającej się ze związku...
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Convenient and efficient synthesis of functionalized unsymmetrical Z-alkenyl disulfanes
PublikacjaWe developed a simple and efficient method for the synthesis of functionalized unsymmetrical Z-alkenyl disulfanes under mild conditions in moderate to good yields. The designed method is based on the reaction of Z-alkenyl thiotosylates with thiols in the presence of base. The developed method allows the preparation of unsymmetrical Z-alkenyl disulfanes bearing additional hydroxy, carboxy, or amino functionalities.
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Radioisotope measurements of the liquid-gas flow in the horizontal pipeline using phase method
PublikacjaThe paper presents application of the gamma-absorption method to a two-phase liquid-gas flow investigation in a horizontal pipeline. The water-air mixture was examined by a set of two Am-241 radioactive sources and two NaI(Tl) scintillation probes. For analysis of the electrical signals obtained from detectors the cross-spectral density function (CSDF) was applied. Results of the gas phase average velocity measurements for CSDF...
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Noncryogenic Synthesis of Functionalized 2-Methoxypyridines by Halogen-Magnesium Exchange Using Lithium Dibutyl(isopropyl)magnesate(1-) and Lithium Chloride
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Synthesis and properties of new 'N,'N-phenyltetrazole podand
PublikacjaThe synthesis of a new chromogenic N,N-phenyltetrazole receptor is reported here. The cationbinding properties of this receptor in solution were investigated by naked-eye colour change, electrochemical methods and UV-Vis spectroscopy in various solvents (CH3CN, dimethylsulphoxide (DMSO), DMSO/H2O, CH3CN/H2O and CH3CN/MeOH). In addition, the receptor was used as a sensing material in ion-selective membrane electrodes. The selectivity...
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A Review on Deactivation and Regeneration of Catalysts for Dimethyl Ether Synthesis
Publikacjahe deactivation of catalysts and their regeneration are two very important challenges that need to be addressed for many industrial processes. The most quoted reasons for the deterioration of dimethyl ether synthesis (DME) concern the sintering and the hydrothermal leaching of copper particles, their migration to acid sites, the partial formation of copper and zinc hydroxycarbonates, the formation of carbon deposits, and surface...
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THE INFLUENCE OF PHASE SHIFTERS ON THE VOLTAGE STABILITY OF CONNECTED POWER SYSTEMS
PublikacjaThe paper presents the results of simulation tests of connected power systems in which phase shifters were installed on cross-border links. The analysis was carried out in terms of assessing the impact of shifters on node voltage stability. Individual systems were characterized by different balance of active power: deficit or excess. The evaluation of voltage stability was based on the dU/dQ and dU/dP criteria.
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Interconnection of the Customer-Side Resources Using Single Phase VAPF
PublikacjaThe paper introduces method for utilization of the customer-side generated energy using single phase voltage active power filter. Structure and control method of the power electronics converter has been described and some simulation results are shown to prove usefulness of this arrangements. Proposed application realizes the following functions: power quality improvement, uninterruptible supplying and energy costs reduction.
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Design and synthesis of TiO2/Ti3C2 composites for highly efficient photocatalytic removal of acetaminophen: The relationships between synthesis parameters, physicochemical properties, and photocatalytic activity
PublikacjaIn this study, we report the potential of TiO2/Ti3C2 composite fabricated by oxidation of MXene for degradation of persistent organic pollutants. The effect of the synthesis conditions (time, temperature, and reaction environment) on the morphology, physicochemical properties, and photocatalytic activity was investigated. It was found that acetaminophen degradation was positively correlated with TiO2 content in the composite structure. Furthermore,...
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Potentiometric Solid-Contact Ion-Selective Electrode for Determination of Thiocyanate in Human Saliva
PublikacjaA new solid-contact potentiometric ion-selective electrode for the determination of SCN− (SCN-ISE) has been described. Synthesized phosphonium derivative of calix[4]arene was used as a charged ionophore. The research included selection of the ion-selective membrane composition, determination of the ISEs metrological parameters and SCN-ISE application for thiocyanate determination in human saliva. Preparation of the ISEs included...
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Cation-ordered perovskite-type anode and cathode materials for solid oxide fuel cells
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Poly(3-octylthiophene) as solid contact for ion-selective electrodes: contradictions and possibilities
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New Architecture of Solid-State High-Voltage Pulse Generators
PublikacjaThe application of the nanosecond pulsed electric field (nsPEF) for biomedical treatments has gained more interest in recent decades due to the development of pulsed power technologies which provides the ability to control the electric field dose applied during tests. In this context, the proposed paper describes a new architecture of solid-state high-voltage pulse generators (SSHVPG) designed to generate fully customised sequences...
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The unstable thermoelectric effect in non-stoichiometric Cu2Se during the non-equilibrium phase transition
PublikacjaThe superionic α ↔ β phase transition in Cu1.96Se thermoelectric material is investigated by means of thermal analysis (DSC) and measurements of Seebeck coefficient and electrical conductivity. Results of the DSC measurements with 1–10 K/min heating and cooling rates show that the material is close to the equilibrium phase composition during the transformation. However, the kinetic limitation of the process exists, which is indicated...
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Thermodynamic Characteristics of Phenacetin in Solid State and Saturated Solutions in Several Neat and Binary Solvents
PublikacjaThe thermodynamic properties of phenacetin in solid state and in saturated conditions in neat and binary solvents were characterized based on differential scanning calorimetry and spectroscopic solubility measurements. The temperature-related heat capacity values measured for both the solid and melt states were provided and used for precise determination of the values for ideal solubility, fusion thermodynamic functions, and...
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Design advantages and analysis of a novel five-phase doubly-fed induction generator
PublikacjaPurpose – The purpose of this paper is to provide an analysis of the performance of a new five-phase doubly fed induction generator (DFIG). Design/methodology/approach – This paper presents the results of a research work related to fivephase DFIG framing, including the development of an analytical model, FEM analysis as well as the results of laboratory tests of the prototype. The proposed behavioral level analytical model is based...
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Synthesis and characterization of novel aliphatic polyurethanes for tissue engineering applications
PublikacjaSummarizing, in this thesis was described the synthesis of novel PUR system, which was obtained by using aliphatic diisocyanate (HDI), amorphous macrodiol (PEBA) and chain extender (BDO). This PUR system was established as suitable for TE purpose and successfully modified with AA, which as expected improved its biocompatibility. According to this, AA-modified HDI-based PURs is the PUR system ready for further studies including...
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Synthesis and properties of the double perovskites La2NiVO6, La2CoVO6, and La2CoTiO6
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Synthesis of Combretastatin A-4 Analogs and their Biological Activities
PublikacjaCombretastatin A-4 (CA-4) is a natural product, which consists of two phenyl rings, linked by an ethylene bridge. CA-4, inhibitor of polymerization of tubulin to microtubules, possesses a strong antitumor and anti-vascular properties both in vitro and in vivo. Previous studies showed that disodium phosphate salt of CA-4, a water-soluble prodrug is well tolerated at therapeutically useful doses. However, it should be noted that...
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Dead-Time Effect Compensation Based on Additional Phase Current Measurements
PublikacjaThis paper proposes a new method of dead-time effect compensation. The proposed solution is based on additional phase current measurements realized by analog-to-digital converters. These measurements are carried out at the time instants specified by a pulsewidth-modulation (PWM) strategy. This makes it possible to estimate inverter currents at the commutation instants and, finally, to estimate the voltage error caused by dead time. This...
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Developments in the synthesis and biological activity of Glycyl-L-Histydyl-L-Lysine derivatives
PublikacjaWe emphasize on the methods of the synthesis described in the literature and present the aspects of Gly-His-Lys structure modifications that played a key role in scientific research.
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DIFFRACTION PHASE MICROSCOPY FOR OBSERVATION ON RED BLOOD CELLS FLUCTUATION
PublikacjaNowadays there is quite huge need for more and more precise and effective fast diagnostics methods in hematology diseases. One of the most important blood components are erythrocytes – RBCs (Red Blood Cells). Due to their size they are easy to observe using microscopy. It is commonly known that the shape and lifetime of RBCs allows for early disease identification. Authors present special measurement system for RBCs fluctuations observation...
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Study of Phase and Chemical Composition of Bi1-xNdxFeO3 Powders Derived by Pressureless Sintering
PublikacjaIn the present paper studies on Bi1xNdxFeO3 for x =0.1-0.4 are reported. The mixed oxide method followed with pressureless sintering was employed for ceramics fabrication. Thermal behavior of stoichiometric mixtures of simple oxide powders, viz. Bi2O3, Nd2O3 and Fe2O3 was studied by simultaneous thermal analysis. It was found that with an increase in neodymium content the weight loss increased from 0.75% to 3.16% for x =0.1 and...
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Micellar Route of the Synthesis of Alkyl Xylosides: An Unexpected Effect of Amphiphilic Imidazolium Ionic Liquids
PublikacjaThis manuscript presents results from the investigation on the synthesis of alkyl xylosides by the novel, very efficient and promising protocol of the Fischer synthesis from unprotected xylose and aliphatic alcohol. The use of 1-alkyl-3-methylimidazolium hydrogen sulfate ionic liquids as the catalysts with dual functionality (surfactant + acid catalyst) and micellar reaction system are the main novelty of described method. It has...
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Numerical single-phase modeling of turbulent flow and heat transfer of nanofluids
PublikacjaIn this work, Nusselt number and friction factor are calculated numerically for turbulent pipe flow (6 000< Re < 12 000) with constant heat flux boundary condition using nanofluids. The nanofluid is modelled with the single-phase approach and the simulation results are compared with published experimental data.
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Single-phase power electronics transformer with active functions for smart grid
PublikacjaThis paper presents the control of one cell of a modular single-phase power electronics transformer with active functions for meeting the smart grid concept. In this way, the converter could be used not only as a conventional transformer but also for grid such as reactive power, harmonic elimination and energy storage. The topology of the cell is composed by a bidirectional converter with three stages: a half bridge in the input...
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Determination of leakage inductances of multi-winding and single-phase transformer
PublikacjaThis paper presents the method for determination of leakage inductances of single-phase and multi-winding transformer. The matrix of leakage inductances takes into account leakage self and also leakage mutual magnetic couplings. It is assumed that there is a flux common to all windings and several leakage fluxes referred to a particular winding. The flux linkages of each coil needed fo calculation of leakage inductances was computed...
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Inhibitors of angiogenesis in cancer therapy – synthesis and biological activity
PublikacjaAngiogenesis is the process of formation of new capillaries from preexisting blood vessels. Angiogenesis is involved in normal physiological processes, and plays an important role in tumor invasion and development of metastases. Vascular endothelial growth factor (VEGF) plays a key role in angiogenesis. VEGF is a mitogen for vascular endothelial cells and stimulates their proliferation. By inhibiting the biological activity of...
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Two-phase flow in heterogeneous porous media with non-wetting phase trapping
PublikacjaThis article presents amathematical model describing flowof two fluid phases in a heterogeneous porous medium. Zaproponowano model matematyczny przepływu dwufazowego w drobnoziarnistym ośrodku porowatym zawierającym inkluzje gruboziarniste. Inkluzje charakteryzują się niższą wartością ciśnienia wejścia dla płynu niezwilżającego (np. powietrze, ropa naftowa) niż materiał podstawowy. Podczas nawadniania takiego ośrodka dochodzi do...
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Is the Solid Electrolyte Interphase an Extra-Charge Reservoir in Li-Ion Batteries?
PublikacjaAdvanced metal oxide electrodes in Li-ion batteries usually show reversible capacities exceeding the theoretically expected ones. Despite many studies and tentative interpretations, the origin of this extra-capacity is not assessed yet. Lithium storage can be increased through different chemical processes developing in the electrodes during charging cycles. The solid electrolyte interface (SEI), formed already during the first...
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublikacjaThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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Effect of interconnect coating procedure on solid oxide fuel cell performance
PublikacjaChromium (Cr) species vaporizing from chromia-forming alloy interconnects is known as a source of degradation in solid oxide fuel cell (SOFC) stacks called “cathode poisoning”. (Mn,Co)3O4 spinel coatings offer good protection against Cr evaporation during operation. In this study, Crofer 22 APU steel interconnects were electrophoretically deposited in different mediums to obtain high packing of green coating layer. The optimized...
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Comparative Study of Taste Substance Sensing by Liquid Membrane Oscillator and Electrochemical Systems With All-Solid-State Electrodes
PublikacjaIn food industry, different types of sensors are used for characterizing and quantifying taste substances. Therefore, it is important to establish the principal advantages and disadvantages of these sensors for optimal application. In this paper, two possible systems are compared for sensing the four fundamental tastes: sour (citric acid), salty (sodium chloride), sweet (sucrose), and bitter (caffeine or quinine hydrochloride). One...
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The new method of ZnIn2S4 synthesis on the titania nanotubes substrate with enhanced stability and photoelectrochemical performance
PublikacjaThe new method of ZnIn2S4 synthesis on the titania nanotubes substrate with enhanced stability and photoelectrochemical performance
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Sensorless Disturbance Detection for Five Phase Induction Motor with Third Harmonic Injection
PublikacjaThe paper presents a sensorless disturbance detection procedure that was done on a five phase induction motor with third harmonic injection. A test bench was developed where a three phase machine serves as disturbance generator of different frequencies. The control of the machines is based on multi scalar variables that ensures an independent control of the motor EMF and the rotor flux. For disturbance identification a speed observer...
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Numerical Simulations of Seepage in Dikes Using unsaturated and Two-Phase Flow Models
PublikacjaModeling of water flow in variably saturated porous media, including flood dikes, is often based on the Richards equation, which neglects the flow of pore air, assuming that it remains at constant atmospheric pressure. However, there is also evidence that the air flow can be important, especially when the connectivity between the pore air and atmospheric air is lost. In such cases a full two-phase air-water flow model should be...
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Phase change thermal energy storage – the experience of the materials preparation for the specific applications.
PublikacjaThermal energy storage and temperature stabilization is very important in many engineering applications. There are three kinds of thermal energy storage: sensible heat, latent heat and reversible chemical reaction heat. Phase change materials (PCM) absorb, store and release large amounts of energy in the form of latent heat, at constant temperature, called the transition temperature. Many innovative applications could be found...
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Radar Signal Parameters Estimation Using Phase Accelerogram in the Time-Frequency Domain
PublikacjaRadar signal parameter estimation, in the context of the reconstruction of the received signal in a passive radar utilizing other radars as a source of illumination, is one of the fundamental steps in the signal processing chain in such a device. The task is also a crucial one in electronic reconnaissance systems, e.g. ELINT (Electronic Intelligence) systems. In order to obtain accurate results it is important to measure, estimate...
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Observation on red blood cells fluctuations by diffraction phase microscopy
PublikacjaNowadays there is quite huge need for more and more precise and effective fast diagnostics methods in hematology diseases. One of the most important blood components are erythrocytes – Red Blood Cells (RBCs). Due to their size they are easy to observe using microscopy. It is commonly known that the shape and lifetime of RBCs allows for early disease identification. Authors present special measurement system for RBCs fluctuations...
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Testing Stability of Digital Filters Using Multimodal Particle Swarm Optimization with Phase Analysis
PublikacjaIn this paper, a novel meta-heuristic method for evaluation of digital filter stability is presented. The proposed method is very general because it allows one to evaluate stability of systems whose characteristic equations are not based on polynomials. The method combines an efficient evolutionary algorithm represented by the particle swarm optimization and the phase analysis of a complex function in the characteristic equation....
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On the synthesis of coupled-lossy resonator filters with unloaded quality factor control
PublikacjaA technique for fast synthesis of coupling matrix low-pass prototypes of generalized Chebyshev bandpass filters with lossy resonators is presented in this paper. The coupling matrix is found by solving a nonlinear least squares problem based on zeros and poles of filter's transfer functions. Additional constraints are introduced that allow one to control the level of unloaded quality factor of resonators.
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Five-phase squirrel-cage motor. Construction and drive properties
PublikacjaThis paper presents the simulation and experimental results of a five-phase squirrel-cage induction motor. The new machine has been designed to operate in a drive system with third harmonic rotor flux injection in order to improve the motor torque utilization. The motor structure, the mathematical model as well as the laboratory prototype have been described. The motor speed-torque characteristics and transients are elaborated...
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Rock salt ordered-type double perovskite anode materials for solid oxide fuel cells
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Low-Cost Unattended Design of Miniaturized 4 × 4 Butler Matrices with Nonstandard Phase Differences
PublikacjaDesign of Butler matrices dedicated to Internet of Things and 5th generation (5G) mobile systems—where small size and high performance are of primary concern—is a challenging task that often exceeds capabilities of conventional techniques. Lack of appropriate, unified design approaches is a serious bottleneck for the development of Butler structures for contemporary applications. In this work, a low-cost bottom-up procedure for...
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Comparison of Transmission Capacities of Two Regulation Systems: Lateral and in-phase Control Transformers
PublikacjaThis paper presents a comparison of regulation capabilities of lateral and in-phase control transformers in a selected node of a power system. Their regulation capabilities are presented, as well as cross-system exchange options.
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Synthesis and physical properties of the 10.6 K ferromagnet NdIr3
PublikacjaThe magnetic, transport, and thermodynamic properties of NdIr3 are reported. Its PuNi3-type crystal structure (space group R−3m), with lattice parameters a= 5.3262(1)Å and c=26.2218(3)Å, was confirmed by powder x-ray diffraction. Our measurements indicate that NdIr3 exhibits a previously unreported paramagnetic to ferromagnetic phase transition below TC=10.6 K(determined by using the Arrott plot). The magnetic susceptibility obeys...
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A miniaturized solid-contact potentiometric multisensor platform for determination of ionic profiles in human saliva
PublikacjaThis paper describes a miniaturized multisensor platform (MP-ISES) consisting of electrodes: a reference one (RE) and ion-selective electrodes (ISEs) for monitoring Na+, K+, Ca2+, Mg2+, Cl−, and SCN− ions and pH in human saliva. Gold electrode surface was modified by deposition of two layers: electrosynthesized PEDOT:PSS forming an intermediate layer, and ion-selective membrane. The developed ISEs were characterized by a wide linear...
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3-phase medium frequency transformer for a 100kW 1.2kV 20kHz Dual Active Bridge converter
PublikacjaThe article presents a three-phase Medium Frequency Transformer being a part of a 100kW 1.2kV 20kHz Dual Active Bridge DC-DC converter. The transformer design is detailed focusing on winding and core power loss calculation. The high power three-phase MFT prototype is presented. The experimental results include the transformer impedance characteristics, no load test and three-phase DAB full load test waveforms
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Rhodotorulic Acid and its Derivatives: Synthesis, Properties, and Applications
PublikacjaSiderophores are low molecular weight compounds produced by microorganisms to scavenge iron in iron-deficient environments. Rhodotorulic acid, a natural hydroxamate siderophore, plays a vital role in iron acquisition for fungi and bacteria. As the simplest natural hydroxamate siderophore, it exhibits a high affinity for ferric ions, enabling it to form stable complexes that facilitate iron uptake and transport within microorganisms....
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Representation of magnetic hysteresis in single-phase transformer for circuit simulations
PublikacjaThe paper presents a mathematical model for the hysteresis phenomenon in a multi-winding single-phase core type transformer. In the circuit transformer model, it is assumed that there is a flux common Φ to all windings as nonlinear and hysteretic function of the total currents Θ (Ampere turns) of all windings. To simulate magnetic behaviour of the iron core the feedback scalar Preisach model of hysteresis is developed. The Preisach...