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Wyniki wyszukiwania dla: NEAR-INFRARED SPECTROSCOPY
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Application of Infrared Thermography to Non-Contact Testing of Varistors
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Determination of the active ingredient in pharmaceutical gel formulation by NIR spectroscopy
PublikacjaPharmaceuticals of their intended must be thoroughly controlled. The traditional analytical methods are very costly and time consuming. NIR spectroscopy allows to analyze pharmaceutical materials very quickly and with very low costs. First pharmaceutical applications of the NIR spectroscopy appeared with some incuriosity in the late 1960s. Application of NIR in the contemporary pharmaceutical industry is very large. The most common...
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Photoelectron spectroscopy of brominated derivative of pyrimidine: 2-bromopyrimidine
PublikacjaIn this study the brominated derivative of pyrimidine, 2-bromopyrimidine, was investigated by photoelectron spectroscopy. Outer valence photoelectron spectra recorded at 21.22, 45 and 100 eV photon energy for this compound are presented. The recorded spectra have a higher resolution than that previously reported in the literature. The bromine 3d and 3p edge photoelectron spectra have also been recorded in a photon impact experiment...
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Application of dynamic impedance spectroscopy to scanning probe microscopy.
PublikacjaDynamic impedance spectroscopy, designed for measuring nonstationary systems, was used in combination with scanning probe microscopy. Using this approach, impedance mapping could be carried-out simultaneously with topography scanning. Therefore, correlation of electrical properties with particular phases of an examined sample was possible. The sample used in this study was spheroidal graphite cast iron with clearly defined phases...
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INTERNATIONAL JOURNAL OF INFRARED AND MILLIMETER WAVES
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Fast High-Impedance Spectroscopy Method Using SINC Signal Excitation
PublikacjaIn this paper the method of fast impedance spectroscopy of technical objects with high impedance (|Zx| > 1 Gohm) is evaluated by means of simulation and practical experiment. The method is based on excitation of an object with a sinc signal and sampling response signals proportional to current flowing through and voltage across the measured impedance. The object impedance spectrum is obtained with use of continuous Fourier transform...
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Fiber fluorescent spectroscopy
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Diagnostics of high-voltage varistor quality using resonant ultrasound spectroscopy
PublikacjaResonant spectroscopy is an effective nondestructive testing method focused on defects detection in tested objects. Resonance spectrum contains an information about the mechanical properties and particularly about the structural homogeneity of the whole object. A swept frequency method has been used to measure the selected resonant frequencies range. The system for measurement of resonant ultrasound spectroscopy of high-voltage...
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Concentration and sources of polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs) in surface soil near a municipal solid waste (MSW) landfill
PublikacjaDue to a continuous demand of land for infrastructural and residential development there is a public concern about the condition of surface soil near municipal solid waste landfills. A total of 12 surface (0–20 cm) soil samples from a territory near a landfill were collected and the concentration of 16 PAHs and 7 PCB congeners were investigated in these samples. Limits of detection were in the range of 0.038–1.2 μg/kg for PAHs...
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Electrochemical Evaluation of Sustainable Corrosion Inhibitors via Dynamic Electrochemical Impedance Spectroscopy
PublikacjaFinding suitable measurement methods for the effective management of electrochemical problems is of paramount importance, particularly for improving efficiency in corrosion protection. The need for accurate measurement techniques specific to nonstationary conditions has long been recognized, and promising approaches have emerged. This chapter introduces dynamic electrochemical impedance spectroscopy as a novel advancement in electrochemistry...
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On stress singularity near the tip of a crack with surface stresses
PublikacjaIn the framework of the simplified linear Gurtin–Murdoch surface elasticity we discuss a singularity of stresses and displacements in the vicinity of a mode III crack. We show that inhomogeneity in surface elastic properties may significantly affect the solution and to change the order of singularity. We also demonstrate that implicitly or explicitly assumed symmetry of the problem may also lead to changes in solutions. Considering...
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A Framework of A Ship Domain-Based Near-Miss Detection Method Using Mamdani Neuro-Fuzzy Classification
PublikacjaSafety analysis of navigation over a given area may cover application of various risk measures for ship collisions. One of them is percentage of the so called near- miss situations (potential collision situations). In this article a method of automatic detection of such situations based on the data from Automatic Identification System (AIS), is proposed. The method utilizes input parameters such as: collision risk measure based...
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Excited states of isoxazole molecules studied by electron energy-loss spectroscopy
PublikacjaElectron energy-loss spectra were measured in isoxazole in the excitation energy range 3.5−10 eV to investigate the valence excited states. Spectra recorded at different scattering conditions enabled the identification of the singlet and triplet states and the determination of their vertical excitation energies. The two lowest energy triplet bands, ππ* 13A' and ππ* 23A' at 4.20 and 5.30 eV, respectively show vibrational progressions....
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Evaluation of the fast impedance spectroscopy method in the laboratory measurement system
PublikacjaIn this paper the method for fast impedancespectroscopy of technical objects with very high impedance(|Zx| ≥ 1 GΩ) is evaluated by means of simulation and practicalexperiment. The method is based on excitation of an object, witha square pulse and measurements of voltage and currentresponses with DAQ card. The object impedance spectrum isobtained with use of continuous Fourier transform. Someimprovements of the method concerned...
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Determination of Hydroxy Groups in the Modified Epoxy Oligomers Using IR-Spectroscopy
PublikacjaThe use of IR-spectroscopy has been proposed to determine the content of hydroxy groups in the modified functional oligomers based on bisphenol A diglycidyl ether. Apart from hydroxy groups the investigated oligomers contain epoxy or peroxy, carboxy or acrylic groups.
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Privacy-Preserving, Scalable Blockchain-Based Solution for Monitoring Industrial Infrastructure in the Near Real-Time
PublikacjaThis paper proposes an improved monitoring and measuring system dedicated to industrial infrastructure. Our model achieves security of data by incorporating cryptographical methods and near real-time access by the use of virtual tree structure over records. The currently available blockchain networks are not very well adapted to tasks related to the continuous monitoring of the parameters of industrial installations. In the database...
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A ship domain-based model of collision risk for near-miss detection and Collision Alert Systems
PublikacjaThe paper presents a new model of ship collision risk, which utilises a ship domain concept and the related domain-based collision risk parameters. An encounter is here described by five variables representing: degree of domain violation (DDV), relative speed of the two vessels, combination of the vessels’ courses, arena violations and encounter complexity. As for the first three variables, their values can be directly computed...
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Dipole-driven dynamics for near-threshold electron/positron interactions with pyrimidinic DNA bases: a path to compound formations
PublikacjaCalculations are reported for electron and positron scattering from isolated cytosine and thymine, where the two pyrimidinic single-ring DNA bases, in the gas-phase at energies near the elastic threshold, they reveal the special features of the dipole-driven scattering states. All molecules examined exhibit, in fact, supercritical (>1.67 D) permanent dipoles which can therefore also support, below threshold, excited bound compound...
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Investigation of H2:CH4 plasma composition by means of spatially resolved optical spectroscopy
PublikacjaThe system based on spatially resolved optical emission spectroscopy dedicated for in situ diagnostics of plasma assisted CVD processes is presented in this paper. Measurement system coupled with chemical vapour deposition chamber by dedicated fiber-optic paths enables investigation of spatial distribution of species densities (Hx, H+, CH, CH+) during chemical vapour deposition process. Experiments were performed for a various...
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Modeling of TEC Variations Based on Signals from Near Zenith GNSS Satellite Observed by Dense Regional Network
PublikacjaCurrently the substantial successes in high-resolution ionospheric mapping is declared in many publications. Nevertheless, up to now there are no examples of dynamic visualization of TEC disturbances on regional scale with as high resolution as tropospheric models. Over the years, ionosphere has been modeling basing on the simple assumption, that it is a thin layer, which surrounds the Earth at some arbitrary height. However, the...
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Journal of Ancient Near Eastern Religions
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Journal of Balkan and Near Eastern Studies
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Selected perowskite type LSFO thin films for the infrared detectors
PublikacjaPrzedstawiono technologię wytwarzania cienkich warstw ceramicznych tlenków lantanowo-strontowo-żelazowych (LSFO). Zaprezentowano konstrukcję bolometrycznych detektorów podczerwieni wykonanych z opracowanych warstw. Przedstawiono charakterystyki prądowo-napięciowe wybranych detektorów, wyniki pomiaru ich szumów i termicznej stałej czasowej. Przedstawione detektory były w stanie wykryć obiekt o temperaturze 38 stopni Celcjusza znajdujący...
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Active Dynamic Infrared Thermal Imaging in Burn Depth Evaluation
PublikacjaThe aim of this study was to find the relationship between active dynamic thermography (ADT) with cold excitation and burn depth. This new modality of evaluation of burns seems to be an attractive proposal for quantitative classification, allowing proper choice of burn wound treatment: conservative or surgical, especially compared with static thermography. The work was an in vivo experiment on domestic pigs, and a small number...
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Ionic hydration behavior derived from infrared spectra in HDO
PublikacjaNa podstawie widm HDO w zakresie podczerwieni scharakteryzowano hydratacjejonów o różnym charakterze. Zastosowana analiza danych widmowych opierała się na metodzie widm różnicowych. Wyniki prowadzą do wniosku, że kationy i aniony wywierają jakościowo bardzo różny wpływ na strukturę wody. Energia wiązań wodorowych cząsteczek wody oddziaływającej z anionem zmienia się proporcjonalnie z siłą polaryzującą anionów. W przeciwieństwie...
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INFRARED PHYSICS & TECHNOLOGY
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X-ray Photoelectron Spectroscopy of Carboxylic Acids as Corrosion Inhibitors of Aluminium Alloys
PublikacjaThe datasets, titled X-ray Photoelectron Spectroscopy studies of citric acid adsorption on aluminium alloy 5754 in alkaline media and X-ray Photoelectron Spectroscopy studies of various carboxylic acids adsorption on aluminium alloys in alkaline media, contain XPS studies of the corrosion inhibitory action of selected dicarboxylic acids towards commercially available aluminium alloy 5754 in alkaline media at pH=11. These datasets...
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Characterization of nano-silica vegetable grease with diffusing wave spectroscopy DWS and Raman spectroscopy
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Utilizing pulse dynamics for non-invasive Raman spectroscopy of blood analytes
PublikacjaNon-invasive measurement methods offer great benefits in the field of medical diagnostics with molecular-specific techniques such as Raman spectroscopy which is increasingly being used for quantitative measurements of tissue biochemistry in vivo. However, some important challenges still remain for label-free optical spectroscopy to be incorporated into the clinical laboratory for routine testing. In particular, non-analyte-specific...
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DETERMINATION OF SP3 FRACTION IN ta-C COATING USING XPS AND RAMAN SPECTROSCOPY
PublikacjaThe paper presents results of studies on the structure of tetrahedral amorphous carbon films (ta-C) with a thickness in the range from 20 to 280 nm, deposited using pulsed vacuum arc technique with an electromagnetic Venetian blind plasma filter. The results of the phase structure analysis, obtained using visible Raman spectroscopy and UV Raman spectroscopy methods, showed a strong dependence of the results on the presence, on...
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Near-Field Wireless Sensing of Plastics and Papers Using Frugal Peel-Off Passive Tag
PublikacjaThis article presents a novel frugal approach of testing plastics and papers using a near-field microwave sensing technique with a peel-off tag. The proposed sensing technique involves two electrical entities: the sensor, which may be regarded as a reader, and a disposable tag. The reader is a modified design of a gap-coupled microstrip line (GCML) sensor, while the passive tag is a standard double-ring complementary split-ring...
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Characterization of metabolites in different kiwifruit varieties by NMR and fluorescence spectroscopy
PublikacjaIt is known from our previous studies that kiwifruits, which are used in common human diet, have preventive properties of coronary artery disease. This study describes a combination of 1H NMR spectroscopy, multivariate data analyses and fluorescence measurements in differentiating of some kiwifruit varieties, their quenching and antioxidant properties. A total of 41 metabolites were identified by comparing with literature data...
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Local impedance spectroscopy of membranes
PublikacjaCelem niniejszej publikacji jest zaprezentowanie zastosowania techniki Lokalnej Elektrochemicznej Spektroskopii Impedancyjnej (LEIS) do uzyskania lokalnej charakterystyki membran. Membranę wykonaną z polichlorku winylu (PCV), plastyfikowaną sebacynianem bis(2etyloheksylu) i domieszkowaną boranem tetradodecyloamoniowym zbadano pod kątem równomiernego rozkładu przewodnictwa na powierzchni badanej próbki. Lokalne pomiary impedancyjne,...
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Local impedance spectroscopy of membranes
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Advances in Atomic and Molecular Spectroscopy
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The Microwave Sources for EPR Spectroscopy
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The gyrotron source for the EPR spectroscopy
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Correction methods in impedance spectroscopy
PublikacjaW pracy przedstawiono trzy grupy metod, ktÓre mogą być zastosowane do korekcji danych pomiarowych uzyskanych za pomoca spektroskopii impedancyjnej.
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Remote Monitoring System for Impedance Spectroscopy using Wireless Sensor Network
PublikacjaThe architecture of a miniaturized impedanceanalyser with wireless communication module for remoteImpedance Spectroscopy (IS) of anticorrosion coatings ondifficult-to-reach objects (e.g. on the steel construction ofthe bridge) is described in this paper. Some practical aspectsof implementation of a Wireless Sensor Network (WSN) arealso discussed. A low scale, middle range, WSN networkcomposed of a Base Station (BS) with a Personal...
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Sub-terahertz Near-field Dielectric Sensor in CMOS Technology
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Dynamics near nonhyperbolic fixed points or nontransverse homoclinic points
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Urinary mercury in adults in Poland living near a chloralkali plant
PublikacjaW pracy przedstawiono wyniki badań prowadzonych w ramach projektu Unii Europejskiej nt European Mercury Emission from Chloralkali Informacja o zawartości rtęci w moczu została opracowana i przedyskutowana na podstawie chemicznej analizy próbek świeżego moczu pobranych od 75 osób zamieszkałych w rejonie zakładu i 100 osób z rejonu referencyjnego oraz odpowiedzi na pytania w specjalnie przygotowanym kwestionariuszu. Stwierdzono,...
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Localization of ferromagnetic objects via magnetometric method near equator
PublikacjaIstnieje wiele metod wykrywania ukrytych w ziemi obiektów. Metody te można podzielić na pasywne i aktywne. Do metod pasywnych należy metoda magnetometryczna. Obiekt ferromagnetyczny zaburza w swoim otoczeniu równomierność pola magnetycznego. Korzystając z metody magnetometrycznej można to zaburzenie zmierzyć i wykryć obiekt. W pracy przedstawiono nową metodę lokalizacji obiektów ferromagnetycznych metodą magnetometryczną znajdujących...
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Computer-aided analysis of thermal convection near electric devices
PublikacjaObciążalność długotrwała urządzeń elektrycznych zależy od intensywności oddawania ciepła przez te urządzenia do otoczenia. Dla zwiększenia obciążalności długotrwałej urządzeń stosuje się konwekcję wymuszoną np. z wykorzystaniem wentylatorów. Wszechstronne obserwacje i analiza procesów konwekcji naturalnej wskazują, że jej intensyfikację można uzyskać dzięki umieszczaniu w pobliżu urządzenia oddającego ciepło elementów tworzących...
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Leszek Ziemczonek dr
OsobyUniversity education 1973-1978 – Nicolaus Copernicus University in Toruń, University of Gdańsk in Gdańsk, Mathematical Physics, M. Sc. 1979 – Diploma of Postgraduate Studies, Pedagogics 1989 – Institute of Physics, Polish Academy of Sciences in Warsaw, Theoretical Physics, Ph. D. 2010-2012 – Diploma of Postgraduate Studies, Mathematics Training: · 09.1983 – Trieste (Italy) – International Centre for Theoretical Physics...
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Electron impact fragmentation of pyrrole molecules studied by fluorescence emission spectroscopy
PublikacjaThe fluorescence emission spectroscopy using electron impact excitation technique was employed to study fragmentation processes of the gas phase pyrrole molecules. The following excited fragmentation species were observed by detection of their fluorescence decay: the atomic hydrogen H(n), n = 4-7 and the diatomic CH(A2Δ), CN(B2Σ+), NH(A3Π) and C2(d3Πg) fragments. These atomic and molecular products differ from those previously...
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Unraveling Luminescent Energy Transfer Pathways: Futuristic Approach of Miniature Shortwave Infrared Light-Emitting Diode Design
Dane BadawczePhosphor-converted shortwave infrared phosphor light-emitting diodes (pc-SWIR LEDs, 900–1700 nm) are promising next-generation portable light sources for spectroscopy, security, optical communication, and medical applications. A typical design strategy involves energy transfer from Cr3+ to Ni2+, and thus, energy transfer from Cr3+–Cr3+ pairs to Ni2+...
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Detection of Denatonium Benzoate (Bitrex) Remnants in Noncommercial Alcoholic Beverages by Raman Spectroscopy
PublikacjaIllegal alcoholic beverages are often introduced into market using cheap technical alcohol, which is contaminated by denatonium benzoate (Bitrex) of very small concentration. Bitrex is the most bitter chemical compound and has to be removed before alcohol consumption. The home-made methods utilize sodium hypochlorite to disintegrate particles of denatonium benzoate in alcohol and to remove bitter taste before trading. In this experimental...
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Local electrochemical impedance spectroscopy in dynamic mode of galvanic coupling
PublikacjaA novel method that combines local electrochemical impedance spectroscopy and mapping in dynamicmode is proposed. Method was validated over two galvanic couplings, namely zinc/copper and cad-mium/copper. Impedance spectrum response for all measuring points was obtained by means ofsimultaneous implementation of selected range of frequencies. Proposed method allows the measure-ment in a more time-efficient manner, at the same time...
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Ultrastructural analysis of the submandibular sialoliths: Raman spectroscopy and electron back-scatter studies
PublikacjaThe aim of work was the epidemiological analysis of the occurrence of sialolithiasis of the submandibular gland in adults and the evaluation of the ultrastructure of salivary stones. The study sample consisted of 44 sialoliths. Analysis of the structure and chemical composition of sialoliths was performed using a Scanning Electron Microscope and Raman Spectroscopy. Comparing our results with the literature we can say that the epidemiology...