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Wyniki wyszukiwania dla: HIGH TEMPERATURE PROTECTIVE COATINGS
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Effect of environmental temperature variations on protective properties of organic coatings
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Effect of environmental temperature variations on protective properties of organic coatings
PublikacjaW oparciu o model rozwoju naprężeń oraz niszczenia kumulatywnego przedyskutowano wpływ zmiennych temperatur środowiska na mechaniczną spójność i własności ochronne systemów powłokowych. Badano wpływ cykli temperaturowych pomiędzy 20 i 55 st. C oraz między -20 i 20 st. C na trwałość różnych powłokowych systemów malarskich na stali. Stosując technikę spektroskopii impedancyjnej monitorowano zmiany parametrów powłok poddanych cyklom...
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High temperature corrosion of evaporator tubes with thermal sprayed coatings
PublikacjaDegradation examinations of outer surface of low-emission steam boiler evaporator tubes are presented in the paper. Metallographic evaluation of scale morphology, its micro sites chemical composition analysis and distribution of elements on cross sections have been performed. Water-wall tubes were exposed in steam boiler for up to two years period. Common tubes made of 16Mo3 steel suffered sulphide and molten salts corrosions....
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Coatings for improvement of high temperature corrosion resistance of porous alloys
PublikacjaPorowate stopy metaliczne są potencjalnymi podłożami nośnymi dla tlenkowych ogniw paliwo. Ich stosowanie obniża cenę ogniw paliwowych, co zaowocuje ich szybszą komercjalizacą. Jednak są one podatne na korozję w wysokich temperaturach. Dotychczas brak jest metod, które mogą poprawić rezystancję korozyjną porotawych stopów w wysokich temperaturach porowatych stopy do zastosowań SOFC. W tym artykule zaproponowano sposób na poprawę...
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Low temperature processed MnCo2O4 and MnCo1.8Fe0.2O4 as effective protective coatings for solid oxide fuel cell interconnects at 750 °C
PublikacjaIn this study two materials, MnCo2O4 and MnCo1.8Fe0.2O4 are studied as potential protective coatings for Solid Oxide Fuel Cell interconnects working at 750 °C. First powder fabrication by a modified Pechini method is described followed by a description of the coating procedure. The protective action of the coating applied on Crofer 22 APU is evaluated by following the area specific resistance (ASR) of the scale/coating for 5500...
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Low temperature deposition of dense MnCo 2 O 4 protective coatings for steel interconnects of solid oxide cells
PublikacjaIn this work manganese cobalt spinel (MnCo2O4) coatings were deposited on steel substrates by spray pyrolysis at 390 °C. This is at much lower temperatures than previously reported (typically in excess of 900 °C). It was possible to produce coatings with well controlled thickness (2-5-10 μm). The as-deposited coatings were evaluated for their microstructural changes and electrical conductivity up to 800 °C. Results confirm the...
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Thermal Barrier Coatings for High-Temperature Performance of Nickel-Based Superalloys: A Synthetic Review
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High-temperature oxidation of the Crofer 22 H ferritic steel with Mn1.45Co1.45Fe0.1O4 and Mn1.5Co1.5O4 spinel coatings under thermal cycling conditions and its properties
PublikacjaThe aim of the presented study was to deposit protective-conducting Mn1.45Co1.45Fe0.1O4 and Mn1.5Co1.5O4 spinel coatings on the Crofer 22 H ferritic steel by means of electrophoresis and to evaluate their physicochemical properties after high-temperature oxidation under thermal cycling conditions. When the Crofer 22 H steel – whether uncoated or coated with the two spinels – was oxidized in 48-h cycles involving a temperature of...
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Influence of yttria surface modification on high temperature corrosion of porous Ni22Cr alloy
PublikacjaProtective coatings for porous alloys for high temperature use are relatively new materials. Their main drawback is high temperature corrosion. In this work protective coatings based the on Y-precursor infiltrated into the sintered Ni22Cr alloys are studied at 700°C. Effects of the amount of the protective phase on the resulting corrosion properties are evaluated in air and humidified hydrogen. Weight gain of the samples, their...
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The protective properties of graphene oxide coatings functionalized with phosphorus atoms.
PublikacjaRecently, electrophoretically deposited graphene oxide coatings are commonly applied as an anti-corrosion layer. However, improper adjustment of electrophoretic deposition (EPD) parameters as well as the hydrophilic nature of graphene oxide contribute to the formation of defects in the coatings and the increase in the wetting properties, respectively, and thus lead to a reduction of protective properties. The growth of wetting...
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Protective coatings for stainless steel for SOFC applications
PublikacjaW pracy przedstawiono badania związane z warstwami antykorozyjnymi stali nierdzewnych stosowanych w tlenkowych ogniwach paliwowych. Warstwy przygotowana z użyciem prekursorów polimerowych na bazie Y i Co. Użyta stal to Crofer 22 APU.
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Ceria Based Protective Coatings for Steel Interconnects Prepared by Spray Pyrolysis
PublikacjaStainless steels can be used in solid oxide fuel/electrolysis stacks as interconnects. For successful long term operation they require protective coatings, that lower the corrosion rate and block chemical reactions between the interconnect and adjacent layers of the oxygen or the hydrogen electrode. One of the promising coating materials for the hydrogen side is ceria. Using standard sintering techniques, ceria sinters at around...
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Protective properties of the chromium - titanium carbonitryde composite coatings.
PublikacjaZbadano właściwości ochronne warstw chromowych zawierających dodatki węglika tytanu poprawiającego właściwości mechaniczne warstw. badania ditycżą roztworów kwasu siarkowego. Badania przeprpwadzono metodą spektroskopii impedamncyjnej. Wykazano ze właściwosci ochronne warswt są lepsze dzięki sdyspergowanym cząstkowm węglika tytanu.
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Antimicrobial properties of protective coatings produced by plasma spraying technique
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Cyclic mechanical stress impact on protective properties of organic coatings
PublikacjaCelem pracy jest zaprezentowanie wyników badań wpływu cyklicznych naprężeń mechanicznych na układy powłoka/metal. Powtarzające się naprężenia mechaniczne zostały zidentyfikowane jako czynnik w znaczącym stopniu przyczyniający się do degradacji powłok. Próbki składające się z powłoki epoksydowej nałożonej na stal St3SAl poddano serii 21000 cykli naprężenie-odpuszczenie. Badania przeprowadzono w zakresie odkształceń elastycznych...
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Nanocrystalline diamond sheets as protective coatings for fiber-optic measurement head
PublikacjaFiber-optic sensors find numerous applications in science and industry, but their full potential is limited because of the risk of damaging the measurement head, in particular, due to the vulnerability of unprotected tips of the fiber to mechanical damage and aggressive chemical agents. In this paper, we report the first use of a new nanocrystalline diamond structure in a fiber-optic measurement head as a protective coating of...
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CuMn1.7Fe0.3O4 – RE2O3 (RE=Y, Gd) bilayers as protective interconnect coatings for Solid Oxide Cells
PublikacjaEfficient replacement of materials based on critical elements such as cobalt is one of the greatest challenges facing the field of solid oxide cells. New generation materials, free of cobalt show potential to replace conventional materials. However, these materials are characterized by poor ability to block chromium diffusion. This article described the study of CuMn1.7Fe0.3O4 (CMFO) spinel combined with single metal oxide (Y2O3...
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Recent advances on spinel-based protective coatings for solid oxide cell metallic interconnects produced by electrophoretic deposition
PublikacjaThe application of ceramic protective coatings to the metallic interconnects in solid oxide cells (SOCs) is a viable and effective method to limit interconnect degradation issues. This featured letter provides a critical overview of the main outcomes of current research on the use of the electrophoretic deposition (EPD) technique to produce protective coatings for SOC metallic interconnects, specifically focusing on different approaches...
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The Microclimate in Protective Fire Fighter Footwear: Foot Temperature and Air Temperature and Relative Humidity
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Degradation of protective coatings in steel chimneys of flue gas desulfurisation system
PublikacjaThis paper presents problems associated with corrosion of steel stacks and changes in philosophy of corrosion protection when implemented into flue gas desulphurization systems. In-situ tests were taken by means of electrochemical impedance spectroscopy at the stack which discharges flue gas before wet lime/limestone desulphurization. A very quick electrolyte absorption by the spherical infill vinylester coating was found using...
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Impact of low-temperature sintering on the Fe-based amorphous coatings
PublikacjaBulk metallic glasses (BMGs) have gained a lot of attention in recent years due to their outstanding properties such as high hardness and excellent wear and corrosion resistance. However, they are restricted in industrial applications due to their extreme brittleness. Iron based amorphous coatings from BMGs are the best solution to use them by overcoming the problem of extreme brittleness. The coatings can be sprayed by various...
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Use of impedance spectroscopy to evaluate the durability of protective coatings after thermal shock
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Experimental review of the performances of protective coatings for interconnects in solid oxide fuel cells
PublikacjaFerritic stainless steel interconnects are used in solid oxide fuel cells; however, coatings are required to improve their performance. Although several types of coatings have been proposed, they have been scarcely investigated under similar conditions. This study compares the characteristics of uncoated Crofer 22 APU and eight different coatings on Crofer 22 APU for up to 3000 h at 800 ◦C. The coatings were deposited at various...
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Water uptake in protective organic coatings and its reflection in measured coating impedance
PublikacjaWater uptake in commercially available epoxy coating on mild steel using impedance spectroscopy and gravimetry was studied. The water content in the coating was determined using the Brasher-Kingsbury equation and various methods of coating capacitance calculation used in the literature. The obtained results were compared with reference gravimetric data. An overestimation of values obtained from impedance data in relation to gravimetric...
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Local properties of organic coatings close to glass transition temperature
PublikacjaAcrylic coating applied on copper substrate has been investigated at different temperatures starting from the ambient one up to the level above the glass transition temperature. Its local topographic and electric properties have been examined with the atomic force microscopy (AFM) based approach including dc current mapping and local impedance spectroscopy. The local findings have been compared with the information from global...
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Non-destructive inspection of anti-corrosion protective coatings using optical coherent tomography
PublikacjaW artykule przedstawiono zastosowanie optycznej tomografii koherentnej (OCT) do badania antykorozyjnych powłok ochronnych. Omówiono właściwości optycznej interferometrii niskokoherentnej jako zastosowanej metody pomiarowej, opisano budowę pomiarowego systemu OCT, zbudowanego w Katedrze Metrologii i Optoelektroniki WETI PG. Przy pomocy zrealizowanego systemu przebadano grupę powierzchni metalicznych pokrytych różnymi powłokami antykorozyjnymi....
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Nickel-nanodiamond coatings electrodeposited from tartrate electrolyte at ambient temperature
PublikacjaIn this study, nanocrystalline Ni and Ni-diamond coatings were obtained by electrodeposition from tartrate electrolyte at ambient temperature aiming at improving corrosion and wear properties of the material. The created surfaces were investigated with regard to microhardness, adhesion, wear- and corrosion-resistance. The various methods such as atomic force microscopy, scanning electron microscopy, electrochemical impedance spectroscopy...
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Protective and Suppressing Electromagnetic Interference Properties of Epoxy Coatings Containing Nano-Sized NiZn Ferrites
PublikacjaNano-crystalline ferrites with the chemical formula NixZn(1−x)Fe2O4, where x = 0, 0.2, 0.4, 0.6, 0.8, 1.0, were synthesized using a co-precipitation method. The obtained ferrites were investigated by X-ray diffraction (XRD). The corrosion inhibiting behavior of nano-sized ferrites was tested using carbon steel samples and 10% aqueous ferrite extracts. Results were compared with previous data obtained for micro-sized ceramic ferrites....
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Preparation of MnCo2O4 and Mn1.7CuFe0.3O4 single-layer, and novel MnCo2O4/ Mn1.7CuFe0.3O4 dual-layer spinel protective coatings on complex-shaped metallic interconnects by EPD method
PublikacjaCeramic protective coatings applied to metallic interconnects play a vital role in solid oxide cells (SOCs) preventing interconnect degradation. In this study, uniform, dense, and crack-free single-layer coatings of MnCo2O4, Mn1.7CuFe0.3O4, and dual-layer coatings of MnCo2O4/ Mn1.7CuFe0.3O4 spinel are deposited onto complex-shaped metallic interconnect using electrophoretic deposition (EPD) method. The porosity of sintered MnCo2O4...
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Influence of CeO2 and TiO2 Particles on Physicochemical Properties of Composite Nickel Coatings Electrodeposited at Ambient Temperature
PublikacjaThe Ni-TiO2 and Ni-CeO2 composite coatings with varying hydrophilic/hydrophobic characteristics were fabricated by the electrodeposition method from a tartrate electrolyte at ambient temperature. To meet the requirements of tight regulation by the European Chemicals Agency classifying H3BO3 as a substance of very high concern, Rochelle salt was utilized as a buffer solution instead. The novelty of this study was to implement a...
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Effect of the let-through energy of overcurrent protective devices on the temperature of conductors during short-circuits
PublikacjaThe scope of the verification of low-voltage systems covers the earth fault loop impedance measurement. This measurement is usually performed with the use of low-value current meters, which force a current many times lower than the one occurring during a real short-circuit. Therefore, the international standard recommends consideration of the increase of resistance of conductors with the increase of temperature, which may occur...
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Analysis of the Possibility of Using New Types of Protective Coatings and Abrasion-Resistant Linings under the Operating Conditions of the Spiral Classifier at KGHM Polska Miedź S.A. Ore Concentration Plant
PublikacjaA study was carried out to select the appropriate coatings for corrosion protection of the spiral classifier working at KGHM Polska Miedź S.A. Ore Concentration Plant. The abrasion resistance of selected protective coatings and wear-resistant linings was investigated using a DT-523 rotary abrasion tester with Taber CS-10 rubber abrasive discs. The average weight loss of the coatings after a cycle of 2000 revolutions was determined....
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Results of acoustic emission tests of corrosion protection degree of ship steel tanks covered by means of protective coatings (Phase I)
PublikacjaThis paper presents methods and results of the 1st series of tests of acoustic emission (AE) signals, aimed at assessing degree of corrosion protection of a tank made of hull structural steel, protected by means of a protective coating combined from polyurethane layer and concrete filler. The tests were carried outin compliance with a method specially elaborated for application to the work in question. In the method were used requirements...
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Influence of Low-Temperature Plasma Treatment on The Liquid Filtration Efficiency of Melt-Blown PP Nonwovens in The Conditions of Simulated Use of Respiratory Protective Equipment
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Review of the Application of Graphene-Based Coatings as Anticorrosion Layers
PublikacjaDue to the excellent properties of graphene, including flexibility that allows it to adjust to the curvature of the substrate surface, chemical inertness, and impermeability, graphene is used as an anticorrosion layer. In this review, we present the current state-of-the-art in the application of graphene in the field of protective coatings. This review provides detailed discussions about the protective properties of graphene coatings...
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RESEARCH ON ORGANIC COATINGS DESIGNED FOR UNDERWATER APPLICATIONS
PublikacjaUnderwater steel structures require periodic maintenance. In the case of vessels, anti-corrosion works are carried out in the shipyard, where very good conditions for applying organic protective coatings can be provided. Very good surface preparation can be obtained by the use of abrasive blasting. The well-prepared metal surface is free from impurities (particularly inorganic salts). Suitable conditions for the application and...
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Evaluation of organic coating systems for corrosion protection of industrial equipment using impedance spectroscopy
PublikacjaThe high economic impact of corrosion can be reduced by enhanced corrosion management and prevention based on appropriate means. This applies in particular to the protection of structures with organic protective coatings. Steel is subject to corrosion that reduces its service life and leads to destruction in most severe cases. The application of paints to metallic objects for corrosion control has been known for a long time and...
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Ferromagnetic nanoparticles imaging by means of Magnetic Force Microscopy
Dane BadawczeFerromagnetic nanoparticles can be used as building blocks for advanced thin film magnets, and can also be used in data storage and biomedical technologies. Nano-crystalline ferrites with the chemical formula NixZn (1 - x) Fe2O4, where x = 0, 0.2, 0.4, 0.6, 0.8, 1.0 show anti-corrosion properties and suppress electromagnetic interference, in the case...
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Study of anticorrosion and microwave absprption properties of NiZn ferrite pigments
PublikacjaPurpose - The purpose of this paper is to report the electrochemical verification of anticorrosive properties of NiZn ferrites as pigments in protective coatings and evaluation of their microwave absorbing properties. Design/methodology/approach - Ferrites, represented by formula NixZn(1-x)Fe2O4, where x=0, 0.2, 0.4, 0.6, 0.8, 1.0, were synthesized using a ceramic method. The samples of ferrites were examined by X-ray diffraction...
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Applying of Doped Graphene Oxide Coatings for Corrosion Prevention
PublikacjaINTRODUCTION Graphene is a carbonaceous material characterized by extraordinary properties (high electron mobility, high surface area, high mechanical strength of 1100 GPa, very dense network hindering the passage of even the smallest helium atoms) [1]. Therefore, it found many applications, also as an anti-corrosive layer [2]. Electrophoretic Deposition (EPD) is one of the methods to deposit coatings. However, due to slight solubility...
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Gelatin-chitosan interactions in edible films and coatings doped with plant extracts for biopreservation of fresh tuna fish products: A review
PublikacjaThe preservation of tuna fish products, which are extremely perishable seafood items, is a substantial challenge due to their instantaneous spoilage caused by microbial development and oxidative degradation. The current review explores the potential of employing chitosan-gelatin-based edible films and coatings, which are enriched with plant extracts, as a sustainable method to prolong the shelf life of tuna fish products. The article...
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Protective properties of Al2O3 + TiO2 coating produced by the electrostatic spray deposition method
PublikacjaMechanical resistance of Al2O3 + TiO2 nanocomposite ceramic coating deposited by electrostatic spray deposition method onto X10CrAlSi18 steel to thermal and slurry tests was investigated. The coating was produced from colloidal suspension of TiO2 nanoparticles dispersed in 3 wt% solution of Al2(NO3)3, as Al2O3 precursor, in ethanol. TiO2 nanoparticles of two sizes, 15 nm and 32 nm, were used in the experiments. After deposition,...
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Assesment of (Mn,Co)3O4powders for possible coating material for SOFC/SOEC interconnects
PublikacjaIn this work (Mn,Co)3O4 spinel powders with different Mn:Co ratio (1:1 and 1:2) and from different commercial suppliers are evaluated for possible powder for production of interconnect coatings. Sinterability of the powders is evaluated on pressed pellets sintered in oxidizing and in reducing/oxidizing atmospheres. For selected powder, coatings are then prepared by the electrophoretic deposition method on Crofer 22 APU stainless...
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Impedance evaluation of coatings from biobased material
PublikacjaThe authors propose a modification of sodium caseinate edible coating for foodstuff protection. The aim was to improve the film’s barrier properties. It was achieved by the addition of propolis, which is a natural, environmentally friendly product known from its intrinsic sealing action. In the next step, propolis-admixed sodium caseinate films were exposed to elevated temperature for 10 min. This approach was meant to improve...
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Functionalization of graphene oxide coatings with phosphorus atoms and their corrosion resistance in sodium chloride environment
PublikacjaIn this work, we compared corrosion resistance of graphene oxide, and phosphorus functionalized reduced graphene oxide coatings obtained as a result of electrophoretic deposition on the copper substrate. Doping graphene oxide with phosphorus atoms was performed by a hydrothermal method in the presence of different amounts of phosphoric acid. Structural studies confirmed the insertion of phosphorus atoms into the graphene oxide...
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Strontium-based nanosized phosphates as anticorrosive fi llers of epoxy and polyurethane coating compositions
PublikacjaAnticorrosive epoxy and polyurethane coatings were compounded using zinc-free nanosized phosphates of strontium (SP) or strontium and aluminum (SAP). For comparison, a nanosized calcium aluminum ammonium phosphate (CAP) and a microsized zinc phosphate (ZP) were tested. Results of salts spray and cyclic corrosion tests revealed better anticorrosive properties of the SAP-based coatings...
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Effect of Functionalization of Reduced Graphene Oxide Coatings with Nitrogen and Sulfur Groups on Their Anti-Corrosion Properties
PublikacjaElectrophoretic production of anticorrosion carbonaceous coatings on copper could be successfully performed by anodic oxidation of negatively charged graphene platelets suspended in an aqueous solution. The various platelets were synthesized by Hummer’s method followed by a hydrothermal reduction in the presence of NH4SCN which was expected to substitute some parts of graphene structure with nitrogen and sulfur groups. X-ray photoelectron...
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AFM-assisted investigation of conformal coatings in electronics
PublikacjaPurpose – This paper aims to presents a new method of investigation of local properties of conformal coatings utilized in microelectronics. Design/methodology/approach – It is based on atomic force microscopy (AFM) technique supplemented with the ability of local electrical measurements, which apart from topography acquisition allows recording of local impedance spectra, impedance imaging and dc current mapping. Potentialities...
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Selection of Organic Coating Systems for Corrosion Protection of Industrial Equipment
PublikacjaThe most important element of corrosion protection in industrial conditions is the protective coating system. However, selecting the right coating can often be a real problem due to the sheer number of coating manufacturers and their products on the market. A quantitative approach based on the data mining technique used to analyze the obtained multi-site exposure data has been proposed. This was demonstrated by the example of the...
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Robert Bogdanowicz dr hab. inż.
OsobyRobert Bogdanowicz received his Ph.D. degree with honours in Electronics from the Gdansk University of Technology. He worked as a post-doc researcher in Ernst-Moritz-Arndt-Universität Greifswald Institut für Physik. He has initiated optical emission imaging of muti-magnetron pulsed plasma and contributed to the development of antibacterial implant coatings deposited by high-power impulse magnetron sputtering. He moved back to...