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Wyniki wyszukiwania dla: DI-SPME

  • Mikroekstrakcja z wykorzystaniem cieczy jonowych - przygotowanie próbek do chromatograficznego oznaczania krótkołańcuchowych kwasów karboksylowych

    Polimerowe ciecze jonowe, ze względu na wyjątkowe właściwości chemiczne i fizyczne mogą znaleźć zastosowanie w wielu technikach analitycznych. Na szczególną uwagę zasługują techniki ekstrakcyjne ograniczające zużycie rozpuszczalników organicznych. Ze względu na możliwości sterowania właściwościami cieczy jonowych poprzez odpowiedni dobór kationu i anionu, można z powodzeniem stosować je jako selektywne pokrycia włókien do SPME,...

  • MEMS Gyro in the Context of Inertial Positionning

    Publikacja

    - Rok 2017

    The article undertake some vital aspect in geodesy, namely an inertial positioning problem using MEMS. Although MEMS inertial sensors offer affordable, appropriately scaled units, and though their inherent measurement noise can be relatively easily mitigated, there are still parameters due to they are not currently capable of meeting all requirements for the accurate and precise inertial positioning. The article presents crucial...

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  • Porous Phantoms Mimicking Tissues—Investigation of Optical Parameters Stability Over Time

    Publikacja

    - Materials - Rok 2021

    Optical phantoms are used to validate optical measurement methods. The stability of their optical parameters over time allows them to be used and stored over long-term periods, while maintaining their optical parameters. The aim of the presented research was to investigate the stability of fabricated porous phantoms, which can be used as a lung phantom in optical system. Measurements were performed in multiple series with an interval...

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  • Web Services Integration with Regard to the Metrics of Data Believability

    Publikacja

    - Rok 2012

    The paper is concerned with estimating the believability of data acquired from web services. In the paper, a new method for believability estimation is introduced. The method is designed for integrating web services. The believability estimation is based on the following metrics: quantity, reputation, approval, independence, traceability, maturity, authority and objectivity. In the method, data trustworthiness is determined by...

  • Integrity level verification for safety-related functions

    This article describes methods for safety integrity level (SIL) verification of safety-related functions with regard to probabilistic criteria given international standards IEC 61508 and IEC 61511. These functions are to be realized using the electrical, electronic and programmable electronic (E/E/PE) systems or safety instrumented systems (SIS). Some methods are proposed for quantitative probabilistic modelling taking into account...

  • Comparing Arbitrary Unrooted Phylogenetic Trees Using Generalized Matching Split Distance

    Publikacja

    In the paper, we describe a method for comparing arbitrary, not necessary fully resolved, unrooted phylogenetic trees. Proposed method is based on finding a minimum weight matching in bipartite graphs and can be regarded as a generalization of well-known Robinson-Foulds distance. We present some properties and advantages of the new distance. We also investigate some properties of presented distance in a common biological problem...

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  • generation of the vorticity mode by sound in a bingham plastic

    This study investigates interaction between acoustic and non-acoustic modes, such as vorticity mode,in some class of a non-newtonian fluid called Bingham plastic. The instantaneous equations describinginteraction between different modes are derived. The attention is paid to the nonlinear effects in the fieldof intense sound. The resulting equations which describe dynamics of both sound and the vorticity modeapply to both periodic...

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  • Transition curve with smoothed curvature at its ends for railway roads

    In the paper, in view of a railway ballasted track, a new concept of transition curve of linear form of curvature along its length and smoothed extreme regions is presented. For this purpose use has been made of an original, universal method for identifying transition curves by means of differential equations. Some general curvature equations for three regions investigated have been determined to be followed by appropriate parametric...

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  • A new division of bacterial UvrA homologues

    The UvrA protein is a DNA-binding and damage-recognition enzyme which participates in the prokaryotic type nucleotide excision repair (NER) pathway. It has recently been noted that some bacterial genomes comprise additional uvrA genes which encode five distinct types of UvrA homologue. We investigated the sequences of over 2400 bacterial genomes and found 130 examples of bacteria containing uvrA 2 genes. The sequence analyses conducted...

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  • Testing Watermark Robustness against Application of Audio Restoration Algorithms

    Publikacja

    The purpose of this study was to test to what extent watermarks embedded in distorted audio signals are immune to audio restoration algorithm performing. Several restoration routines such as noise reduction, spectrum expansion, clipping or clicks reduction were applied in the online website system. The online service was extended with some copyright protection mechanisms proposed by the authors. They contain low-level music features...

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  • Environmental Impacts of Renewable Energy Technologies

    Publikacja

    Nowadays, fossil fuels are the main sources energy from which electricity is obtained. But these sources will not last forever, so in due course renewable energies will have to replace them in this role. All energy sources have some impact on our environment. Fossil fuels — coal, oil, and natural gas — do substantially more harm than renewable energy sources by most measures, including air and water pollution, damage to public...

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  • Deep compaction control of sandy soils

    Vibroflotation, vibratory compaction, micro-blasting or heavy tamping are typical improvement methods for the cohesionless deposits of high thickness. The complex mechanism of deep soil compaction is related to void ratio decrease with grain rearrangements, lateral stress increase, prestressing effect of certain number of load cycles, water pressure dissipation, aging and other effects. Calibration chamber based interpretation...

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  • Human Factors and Functional Safety Analysis in Designing the Control Rooms of Industrial Hazardous Plants

    Publikacja

    - Rok 2014

    In this work some aspects of human factors and functional safety analysis in designing the control rooms of industrial hazardous plants are presented. The “defence in depth” (D-in-D) concept is outlined. Some designing issues of the alarm system (AS) with regard to human factors to be supported using the human reliability analysis (HRA) are discussed. The AS and decision support system (DSS), when properly designed, would contribute...

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  • A comparative analysis of phenotypic and genotypic methods for the determination of the biofilm-forming abilities of Staphylococcus epidermidis

    Publikacja
    • R. Los
    • R. Sawicki
    • M. Juda
    • M. Stankevic
    • P. Rybojad
    • M. Sawicki
    • A. Malm
    • G. Ginalska

    - FEMS MICROBIOLOGY LETTERS - Rok 2010

    The collection of 146 Staphylococcus epidermidis strains isolated from the nasopharynx of lung cancer patients has been studied for the ability of slime secretion and biofilm formation using the Congo red agar (CRA) test and the microtiter plate (MtP) method, respectively. The prevalence of the icaAD and the aap genes was also analyzed. Some isolates (35.6%) were biofilm positive by the MtP method, while 58.9% of isolates exhibited...

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  • A comparative analysis of phenotypic and genotypic methods for the determination of the biofilm-forming abilities of Staphylococcus epidermidis

    Publikacja
    • R. Los
    • R. Sawicki
    • M. Juda
    • M. Stankevic
    • P. Rybojad
    • M. Sawicki
    • A. Malm
    • G. Ginalska

    - FEMS MICROBIOLOGY LETTERS - Rok 2010

    The collection of 146 Staphylococcus epidermidis strains isolated from the nasopharynx of lung cancer patients has been studied for the ability of slime secretion and biofilm formation using the Congo red agar (CRA) test and the microtiter plate (MtP) method, respectively. The prevalence of the icaAD and the aap genes was also analyzed. Some isolates (35.6%) were biofilm positive by the MtP method, while 58.9% of isolates exhibited...

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  • Study of the Anti-Staphylococcal Potential of Honeys Produced in Northern Poland

    Publikacja

    - MOLECULES - Rok 2018

    The antimicrobial activity of 144 samples of honeys including 95 products from apiaries located in Northern Poland was evaluated. The antibacterial activity of those natural products, their thermal stability, and activity in the presence of catalase was investigated by microdilution assays in titration plates. The MTT assay was performed for the determination of anti-biofilm activity. Spectrophotometric assays were used for the...

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  • Succinite, Baltic Amber: A Chemical Masterpiece of Nature

    Succinite, Baltic amber, is one of the most appreciated fossil resins. Its beauty has fascinated people since prehistoric times. It is a substance, and also gemstone, whose uniqueness is due to its compelling, though still not fully understood, physicochemical nature. In this article, some facts about the physical and chemical properties of succinite in order to find an answer for questions about the unique properties of this resin,...

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  • Statistics with R A Handbook for Statistical Analysis with R and R-Studio

    Publikacja

    - Rok 2022

    If you are to perform any kind of data (statistical) analysis and use tools in the data science ecosystem, you may have seen a variety of tutorials, handbooks online (I’m not mentioning traditional bibles of statistics). Unfortunately most of them is written intentionally for specific purposes and/or target group of people and does not include many aspects, data types, difficult aspects, usually hiding them trying to solve theoretical...

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  • Comparison of various flow maldistribution quantification methods in mini heat exchangers

    Publikacja

    The aim of study is to compare various flow maldistribution quantification methods, using velocity, mass flow rate, pressure, and temperature. An experimentally validated numerical study has been prepared and a heat exchanger with 34 semi-circular channels with a diameter of 3.1 mm has been tested. The minichannels were heated from the bottom with a heat flux of 50, 60, 70, and 80 kW/m2. The cases for various inlet velocities of...

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  • Investigation of use of hydrophilic/hydrophobic NADESs for selective extraction of As(III) and Sb(III) ions in vegetable samples: Air assisted liquid phase microextraction and chemometric optimization

    Publikacja
    • A. Elik
    • B. Doğan
    • A. Demirbas
    • H. Haq
    • K. Sanaullah
    • N. Altunay

    - FOOD CHEMISTRY - Rok 2024

    In this paper, a green, cost-effective sample preparation method based on air assisted liquid phase microextraction (AA-LPME) was developed for the simultaneous extraction of As(III) and Sb(III) ions from vegetable samples using hydrophilic/hydrophobic natural deep eutectic solvents (NADESs). Central composite design was used for the optimization of extraction factors including NADES volume, extraction cycle, pH, and curcumin concentration....

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  • Photocatalytic hydrogen evolution by co-catalyst-free TiO2/C bulk heterostructures synthesized under mild conditions

    Publikacja
    • C. Imparato
    • G. Iervolino
    • M. Fantauzzi
    • C. Koral
    • W. Macyk
    • M. Kobielusz
    • G. D'Errico
    • I. Rea
    • R. Di
    • L. De... i 4 innych

    - RSC Advances - Rok 2020

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  • ‘Green’ multi - residue methods for the determination of high importance currently used pesticides in environmental samples

    Publikacja

    The purpose of the research has been to develop and apply ‘green’ analytical methodologies to control and monitor the level of currently used pesticides from different chemical groups in aqueous samples. For extraction of analytes solid - phase microextraction (SPME) and dispersive liquid - liquid microextraction (DLLME) have been applied and compared. For SPME, commonly used materials for coating fibers include: polydimethylsiloxane...

  • Metoda opracowania uniwersalnej osnowy na bazie krzemionki do unieruchomienia cieczy jonowych jako materiałów sorpcyjnych w technice mikroekstrakcji do fazy stacjonarnej

    Publikacja

    - Rok 2022

    Rozprawa doktorska stanowi opis badań prowadzonych w trakcie czterech lat (2018-2022) studiów doktoranckich. Rezultaty prac badawczych zostały opublikowane w postaci pięciu oryginalnych artykułów, stanowiących podstawę tej rozprawy. Tematyka badań dotyczy wykorzystania cieczy jonowych w technice mikroekstrakcji do fazy stacjonarnej (ang. SPME). Głównym celem prowadzonych prac badawczych było: (a) otrzymanie nowej, porowatej sorpcyjnej...

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  • Układy napędowe pojazdów elektrycznych

    W artykule omówiono nowe technologie stosowane w układach napędowych pojazdów elektrycznych. Praca zawiera zależności teorii ruchu pojazdu, nowe rozwiązania w konstrukcji silników trakcyjnych. Przedstawiono również zagadnienia układów zasilania bateryjnego i magazynów energii z superkondensatorami. Pokazano metody sterowania zapewniające optymalizacje rozdziału energii pomiędzy akumulatorami a magazynem energii. Zaprezentowano...

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  • Quasi-Static Response

    Publikacja
    • J. Underwood
    • E. Alley
    • J. Andric
    • D. Boote
    • Z. Gao
    • A. Van Hoeve
    • J. Jelovica
    • Y. Kawamura
    • Y. Kim
    • J. Liu... i 5 innych

    - Rok 2022

    Concern for the quasi-static response of ship and offshore structures, as required for safety and serviceability assessments. Attention shall be given to uncertainty quantification of quasi-static load and response analysis approaches, and their limitations, including exact and approximate methods for derivation of different acceptance criteria.

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  • Modern trends in solid phase extraction: New sorbent media

    Based on the recently published literature, this review provides an update of the most important features and application of formats and devices employed in solid phase extraction (SPE). Special attention was paid on new trapping media proposed in SPE prior the chromatography analysis, based on the use of nanostructured materials, including carbon nanomaterials, electrospun nanofibers, dendrimes and magnetic nanoparticles, molecular...

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  • Miniaturized Solid Phase Extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 1

    Publikacja

    - TRAC-TRENDS IN ANALYTICAL CHEMISTRY - Rok 2023

    Solid Phase Extraction (SPE) has been practiced in a modern form for more than half a century. It was constantly developing, driven by the analysts needs. These needs are coming from the importance to select an appropriate analytical method, which should have satisfactory accuracy, precision and sensitivity. In the case of sorbent-based microextraction techniques, the choice of miniaturized variants that meet these requirements...

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  • Shape Memory Materials from Rubbers

    Publikacja
    • A. Reghunadhan
    • P. Jibin
    • V. Kaliyathan
    • P. Velayudhan
    • M. Strankowski
    • S. Thomas

    - Materials - Rok 2021

    Smart materials are much discussed in the current research scenario. The shape memory effect is one of the most fascinating occurrences in smart materials, both in terms of the phenomenon and its applications. Many metal alloys and polymers exhibit the shape memory effect (SME). Shape memory properties of elastomers, such as rubbers, polyurethanes, and other elastomers, are discussed in depth in this paper. The theory, factors...

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  • Ontology management in the multi-agent system for the it evaluation

    Publikacja

    The team of researchers at the Gdańsk University of Technology is currently developing a model of the multi-agent system (MAS_IT) that would aid the IT managers to find the most appropriate technology to the goals assumed. The knowledge is to be provided by experts and stored in the facts and rules bases. The responsibility of the verification process-on the input and query stages-is given to the ontology, making it to some extend...

  • Multiresolution analysis and adaptive estimation on a sphere using stereographic wavelets

    We construct an adaptive estimator of a density function on d dimensional unit sphere Sd (d ≥ 2), using a new type of spherical frames. The frames, or as we call them, stereografic wavelets are obtained by transforming a wavelet system, namely Daubechies, using some stereographic operators. We prove that our estimator achieves an optimal rate of convergence on some Besov type class of functions by adapting to unknown smoothness....

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  • Determining required safety integrity level

    One of the most important stage of technical system functional safety analysis is defining the safety-related functions as well as determining safety integrity level (SIL) for each defined function. A properly carried out hazard identyfication process is the necessary condition for correct definition of the safety-related functions. Determining the safety integrity level (SIL) is based on risk assessment taking into account risk...

  • Construction of phylogenetic trees with topological constraints

    This paper proposes a method of reconstruction of phylogenetic trees based on heuristic search with topological constraints. Using topological constraints it is possible to reduce the set of solutions as well as to enforce that the result is consistent with a given hypothesis about the evolution process within some group of species. Along with this work a number of algorithms used for phylogenetic analysis were implemented. Those...

  • On the interspike-intervals of periodically-driven integrate-and-fire models

    We analyze properties of the firing map, which iterations give information about consecutive spikes, for periodically driven linear integrate-and-fire models. By considering locally integrable (thus in general not continuous) input functions, we generalize some results of other authors. In particular, we prove theorems concerning continuous dependence of the firing map on the input in suitable function spaces. Using mathematical...

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  • CAPABILITY OF IDENTIFYING AND PREDICTING THE TECHNICAL CONDITION OF PLATE HEAT EXCHANGERS IN OPERATION

    Publikacja

    The paper presents a test stand for plate heat exchangers, allowing to identify the technical condition and to predict durability of the heat exchangers used aboard the sea-going ships: ”Oceanograf”, ”Władysław Orkan”and a passenger-car ferry, under the condition that they are of the same type and manufactured by the same company. In the first part three different installations with plate heat exchangers in the engine rooms...

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  • On the convergence of a nonlinear finite-difference discretization of the generalized Burgers–Fisher equation

    Publikacja

    In this note, we establish analytically the convergence of a nonlinear finite-difference discretization of the generalized Burgers-Fisher equation. The existence and uniqueness of positive, bounded and monotone solutions for this scheme was recently established in [J. Diff. Eq. Appl. 19, 1907{1920 (2014)]. In the present work, we prove additionally that the method is convergent of order one in time, and of order two in space. Some...

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  • Towards the boundary between easy and hard control problems in multicast Clos networks

    In this article we study 3-stage Clos networks with multicast calls in general and 2-cast calls, in particular. We investigate various sizes of input and output switches and discuss some routing problems involved in blocking states. To express our results in a formal way we introduce a model of hypergraph edge-coloring. A new class of bipartite hypergraphs corresponding to Clos networks is studied. We identify some polynomially...

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  • Velocity measurement using the fdoa method in ground-based radio navigation system

    Velocity is one of the main navigation parameters of the moving objects. However some systems of position estimation using radio wave measurements cannot provide velocity data due to limitation of their performance. In this paper a velocity measurement method for DS-CDMA radio navigation system is proposed, which doesn’t require full synchronization of reference stations carrier frequencies. The article presents basics of FDOA...

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  • Swarm Algorithms in Modern Engineering Optimization Problems

    Publikacja

    Complexity of today engineering problems is constantly increasing. Scientists no longer are facing issues, for which simple, mathematical programming methods are sufficient. Issues like autonomic vehicle navigation or classification are considered to be challenging, and although there exist valid means to solve them, in some cases there still is some place for improvement. With emergence of a new type of optimization techniques...

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  • Unity-Gain Zero-Offset CMOS Buffer with Improved Feedforward Path

    Publikacja

    A voltage unity-gain zero-offset CMOS amplifier with reduced gain error and increased PSRR (power supply rejection ratio) is proposed. The amplifier uses two feed mechanisms, negative feedback and supporting positive feedforward, to achieve low deviation from unit gain over the entire input range. The circuit, designed in a standard 180-nanometer 1.8-voltage CMOS process, is compared with two known buffers of similar topology,...

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  • Comparison of luminescence (TL and OSL) dating results from selected loess profiles in SE Poland and the NW Ukraine

    Publikacja
    • S. Fedorowicz
    • M. Łańczot
    • A. Muc

    - Rok 2005

    Five periglacial loess profiles, three from Poland and two from the Ukraine, were selected from dating luminescence methods (TL and OSL). In regional terms, they include loess of the Carpathin, peri-Carpathian and Podalia facies. 89 samples were collected for dating purposes from five profiles. Of these samples, 19 were OSL-dated. The function of TL and OSL date distribution for the same samples was presented on one chart. The...

  • Chladni and circular saw disc vibrations visualisation

    Publikacja

    - Rok 2011

    In this paper are described some methods for saw disc vibration monitoring in march of time (chronology). Ernst Chaldni, the father of sound visualisation and his patternsis are mentioned. In the last partof article are introduced results received with authors measuring systems.

  • Hybrid System for Ship-Aided Design Automation

    Publikacja

    - Rok 2011

    A hybrid support system for ship design based on the methodology of CBR with some artificial intelligence tools such as expert system Exsys Developer along with fuzzy logic, relational Access database and artificial neural network with backward propagation of errors.

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  • Niobiany ziem rzadkich - właściwości i zastosowania

    Publikacja

    Rare earth niobates are a very interesting group of materials. These compound have different properties which could be changes in a wide range by appropriate doping. X-Ray diffraction examinations for some compounds of RE3NbO7 group were shown

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  • Application of nanofluids in selected thermal technologies

    Publikacja

    - Rok 2015

    Some peculiarities regarding convective heat transfer of nanofluids are presented. Particularly, results of the fundamental research concerning pool boiling and single phase convection of nanofluids as well as data obtained for selected heat exchangers operated with nanofluids are discussed.

  • Optimization of Automata

    Publikacja

    - Rok 2014

    This book is conceived as an effort to gather all algorithms and methods developed by the author of the book that concern three aspects of optimization of automata: incrementality, hashing and compression. Some related algorithms and methods are given as well when they are needed to complete the picture.

  • CROWDFUNDING OF RESEARCH PROJECTS IN POLAND

    Publikacja

    Crowdfunding recently became a very popular way of funding, which allows funding almost everything, from minor personal projects to expensive commercial ones, as long as we can find investors. It may also be a new opportunity for entrepreneurial researchers, who may attract capital investment in companies that are promised to own developed technologies. Social financing of science is well suited to reduce some of the biggest problems...

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  • Open Access w naukach biomedycznych

    Publikacja

    Open Access (OA) Movement to nazwa ruchu społecznego, którego celem jest zminimalizowanie przeszkód w upowszechnianiu wyników badań naukowych, a także bardziej efektywne wykorzystywanie nakładów na naukę. Jego historia sięga lat sześćdziesiątych XX wieku, kiedy pojawiły się pierwsze formy sieci rozległych, ale zasadniczy rozwój nastąpił w latach dziewięćdziesiątych wraz z nadejściem tzw. ery cyfrowej. Pojawiła się wówczas koncepcja...

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  • Antimicrobial Activity of Honey

    Publikacja

    - Rok 2017

    Honey has had a valued place in traditional medicine for centuries. It was used to overcome liver, cardiovascular and gastrointestinal problems and for treatment of some types of infectious disease. Particularly, good results were achieved in the case of application of this product for therapy of infected, difficult to heal wounds. The high health-promoting properties of honey have been recently confirmed in many research investigations....

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  • Business continuity management framework for Industry 4.0 companies regarding dependability and security of the ICT and ICS/SCADA system

    Publikacja

    - Rok 2021

    This chapter addresses a business continuity management (BCM) framework for the Industry 4.0 companies including the organizational and technical solutions, regarding the dependability and security of the information and telecommunication technology (ICT), and the industrial control system (ICS) / supervisory control and data acquisition (SCADA) system. These technologies and systems play nowadays important roles in modern advanced...

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  • IoT protocols, architectures, and applications

    Publikacja
    • C. Buratti
    • E. G. Ström
    • L. Feltrin
    • L. Clavier
    • G. Gardašević
    • T. Blazek
    • L. Berbakov
    • T. C. Balan
    • L. Orozco-Barbosa
    • C. Anton-Haro... i 2 innych

    - Rok 2021

    The proliferation of embedded systems, wireless technologies, and Internet protocols have enabled the IoT to bridge the gap between the virtual and physical world enabling the monitoring and control of the environment by data processing systems. IoT refers to the inter-networking of everyday objects that are equipped with sensing, computation, and communication capabilities. These networks can collaboratively interact and perform...

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