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Wyniki wyszukiwania dla: MCD
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Microcrystalline diamond film evaluation by spectroscopic optical coherence tomography
PublikacjaThis study has focused on the microcrystalline diamond film (MCD) thickness evaluation. For this purpose, optical coherence tomography (OCT) enhanced by spectroscopic analysis has been used as a method of choice. The average thickness of the tested layer was about 1.5 µm, which is below the standard 2-point OCT resolution. In this case, the usefulness of the spectroscopic analysis was confirmed for the evaluation of the thickness...
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INFLUENCE OF A VERTEX REMOVING ON THE CONNECTED DOMINATION NUMBER – APPLICATION TO AD-HOC WIRELESS NETWORKS
PublikacjaA minimum connected dominating set (MCDS) can be used as virtual backbone in ad-hoc wireless networks for efficient routing and broadcasting tasks. To find the MCDS is an NP- complete problem even in unit disk graphs. Many suboptimal algorithms are reported in the literature to find the MCDS using local information instead to use global network knowledge, achieving an important reduction in complexity. Since a wireless network...
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Freshwater Ulva (Chlorophyta) as a bioaccumulator of selected heavy metals (Cd, Ni and Pb) and alkaline earth metals (Ca and Mg)
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Binuclear Co(II), Zn(II) and Cd(II) tri-tert-butoxysilanethiolates. Synthesis, crystal structure and spectroscopic studies.
PublikacjaA series of Co(II), Zn(II) and Cd(II) complexes have been synthesized in reaction of respective metal tri-tert-butoxysilanethiolates with pyrazine 1 and 2 and 1,2-bis(2-pyridyl)ethylene 3–5. All compounds have been characterized by single-crystal X-ray structure determination, elemental analysis, FT-IR and thermogravimetry. Obtained complexes are bimetallic with the formula of [M{SSi(OtBu)3}2(μ-L)]2 and metal ions bridged by N,N′-spacer....
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Interaction of cisplatin and two potential antitumoral platinum(ii) complexes with a model lipid membrane: a combined NMR and MD study
PublikacjaIn this study, the interaction of cisplatin (1) and two potential antitumoral Pt(II) complexes (2 and 3) with a model DMPC bilayer was investigated by multinuclear NMR spectroscopy and MD simulations in order to understand its implication for the different antitumoral properties shown by the three complexes. In particular, 31P, 13C and 2H solid state NMR experiments were performed to obtain information on the phase structure, phase...
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Structural, spectral and magnetic properties of Ni(II), Co(II) and Cd(II) compounds with imidazole derivatives and silanethiolate ligands
PublikacjaA series of new metal heteroleptic complexes have been obtained in simple reactions of 1-(3-aminopropyl)-imidazole (api) and 1,4-bis(imidazol-1-yl)-butane (bbi) ligands with metal silanethiolates or acetylacetonates. The obtained complexes are the coordination polymers [Ni{SSi(tBuO)3}2(μ-api)]n1, [Co{SSi(tBuO)3}2(μ-api)]n2, [Cd{SSi(tBuO)3}2(μ-api)·2CH3OH]n3, [Cd{SSi(tBuO)3}2(μ-bbi)·CHCl3]n4 and the dimer [Co{SSi(tBuO)3}2(μ-bbi)·3CH3OH]25....
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Enrichment of Bi-Be-Mo-Cd-Pb-Nb-Ga, REEs and Y in the Permian coals of the Huainan Coalfield, Anhui, China
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Optimization and Modeling of Cr (VI) Removal from Tannery Wastewater onto Activated Carbon Prepared from Coffee Husk and Sulfuric Acid (H2SO4) as Activating Agent by Using Central Composite Design (CCD)
PublikacjaThe primary goal of this research is to lower the hexavalent chromium (Cr (VI)) concentration that has occurred from the growth of the tannery industry. As a result, the potential for heavy metal concentration is increasing day by day. Industrial effluent containing Cr (VI) contributes significantly to water pollution. Chromium hexavalent ion (Cr (VI)) in wastewater is extremely hazardous to the environment. It is critical to address...
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Arginine-, d-arginine-vasopressin, and their inverso analogues in micellar and liposomic models of cell membrane: CD, NMR, and molecular dynamics studies
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Facilitated transport of Zn(II), Cd(II) and Pb(II) across polymer inclusion membranes doped with imidazole azocrown ethers
PublikacjaZbadano transport jonów Pb(II), Cd(II) i Zn(II) przez polimerowe membrany inkluzyjne (PIM) przy użyciu imidazolowych azokoron. Badanie prowadzono dla wodnych roztworów azotanów metali o c(Me)=0,001M i pH=5,0. Polimerowe membrany inkluzyjne otrzymywano z trójoctanu celulozy (nośnik), plastyfikatora i jonoforu (jeden z imidazolowych eterów koronowych z ugrupowaniem azowym). Badane azokorony różniły sięmiejscem podstawienia imidazolu...
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Efficiency of ozonation process with calcium peroxide in removing heavy metals (Pb, Cu, Zn, Ni, Cd) from aqueous solutions
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Experimental investigations on the mechanical properties and damage detection of carbon nanotubes modified crumb rubber concrete
PublikacjaThis study presents a modified crumb rubber (MCR) concrete design mix reinforced with multi-walled carbon nanotubes (MWCNTs), mechanical characterization, and cracking monitoring using the acoustic emission (AE) technique. The results showed that the bridging effect of MWCNTs and MCR in the concrete mix mitigated the shortcomings of MWCNT-MCR concrete and improved the flexural and compressive strengths by 18.3% and 26.5%, respectively,...
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Niejednorodność podbudowy z mieszanki moneralno-cementowo emulsyjnej
PublikacjaW ostatnich latach wzrosła popularność podbudów z mieszanek mineralno-cementowo-emulsyjnych (MCE) ze względu na możliwość ponownego wykorzystania mieszanek mineralno-bitumicznych pochodzących z istniejących nawierzchni. Badania przeprowadzone w trakcie wykonywania podbudów wykazują, że materiał ten jest niejednorodny. Ma to dość duże znaczenie zarówno dla jakości wykonanej warstwy jak i dla określenia trwałości całej konstrukcji...
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Rapid and Green Separation of Mono- and Diesters of Monochloropropanediols by Ultrahigh Performance Supercritical Fluid Chromatography–Mass Spectrometry Using Neat Carbon Dioxide as a Mobile Phase
PublikacjaThis study demonstrates the effect of column selectivity and density of supercritical carbon dioxide (SC-CO2) on the separation of monochloropropanediol (MCPD) esters, known as food toxicants, using SC-CO2 without addition of cosolvent in ultrahigh performance supercritical fluid chromatography–mass spectrometry (UHPSFC-MS). This study shows that over 20 2-monochloropropanediol (2-MCPD) and 3-monochloropropanediol (3-MCPD) mono-...
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Sensitive Determination of Cd in Small-Volume Samples by Miniaturized Liquid Drop Anode Atmospheric Pressure Glow Discharge Optical Emission Spectrometry
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Wykorzystanie kapusty białej (brassica oleracea var. capitata) do fitoekstrakcji metali ciężkich (zn, cd, cu, pb) z gleby*
PublikacjaGatunki roślin z rodziny Brassicaceae uważane są za przydatne w fitoremediacjimetali ciężkich z gleby. Przeprowadzone badania mają na celu potwierdzenie zasadności wykorzystaniakapusty białej, odmiany 'Kamienna Głowa' do fitoekstrakcji Zn, Cd, Cu, Pb. Poziomwybranych metali badano w glebie oraz liściach i głąbach kapusty uprawianej na tych glebach,pochodzących z upraw wazonowych (Kraków) oraz polowych (Czapielsk). Zawartość metaliciężkich...
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Corncob-supported calcium oxide nanoparticles from hen eggshells for cadmium (Cd-II) removal from aqueous solutions; Synthesis and characterization
PublikacjaThis study investigated the efficient removal of cadmium ions from aqueous solutions using calcium oxide nanoparticles (CaO NPs) synthesized from waste hen eggshells using a Sol-gel method and supported on corncob bio-adsorbent. The synthesized CaO NPs were characterized using FT-IR, XRD, specific surface area, and TGA. Batch adsorption experiments were conducted to examine the influence of process parameters such as adsorbent...
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Reply to “Enrichment of Bi-Be-Mo-Cd-Pb-Nb-Ga, REEs and Y in the Permian coals of the Huainan Coalfield, Anhui, China: Discussion”
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Estry kwasów tłuszczowych i monochloropropanodioli w tłuszczach spożywczych oraz produktach spożywczych bogatych w tłuszcze - problemy i wyzwania
PublikacjaMonochloropropanodiole (3-monochloropropanodiol, 3-MCPD; 2-monochloropropanodiol, 2-MCPD) są zaliczane do zanieczyszczeń żywności powstających w wyniku procesów termicznego jej przetwarzania. Obecność tych ksenobiotyków w żywności została stwierdzona już w 1978 r. w sosach sojowych i produktach pokrewnych. Wzmożone zainteresowanie tymi związkami, które ma miejsce od 2004 r. jest związane ze stwierdzeniem znacznych ilości 3-MCPD...
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Structure, morphology and mechanical behaviour of novel bio-based polyurethane composites with microcrystalline cellulose
PublikacjaThe aim of this work was to obtain bio-based polyurethane composites using biocomponents such as, bio-glycol, modified natural oil-based polyol, and microcrystalline cellulose (MCC). The prepolymer method was used to prepare the bio-based polyurethane matrix. Prepolymer synthesised from 4,4’-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 75% wt. commercial polyether and 25% wt. hydroxylated soybean oils (H3)...
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Chemometrics and Statistics | Multicriteria Decision Making
PublikacjaThis contribution describes the application of Multicriteria Decision Making tools in analytical chemistry. The general scheme of MCDM is presented to show its general steps. The most frequently applied in analytical sciences MCDM techniques – AHP, ELECTRE, PROMETHEE and TOPSIS – are briefly described and their advantages and disadvantages are discussed. The applications in analytical chemistry are selection of an appropriate...
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Opinia dotycząca zastosowania mieszanki MCE w trakcie remontu istniejących dróg DK 7 oraz DK 8 w ramach realizacji kontraktu "Kontynuacja projektowania i budowa odcinka drogi ekspresowej S8 od rejonu węzła OPACZ do węzła PASZKÓW"
PublikacjaW ramach realizacji kontraktu "Kontynuacja projektowania i budowa odcinka drogi ekspresowej S8 od rejonu węzła OPACZ do węzła PASZKÓW" firma TPA, działając na zlecenie firmy URS Sp. z o.o. przedstawiła propozycję remontu fragmentów istniejących nawierzchni dróg krajowych nr 7 i nr 8 z wykorzystaniem technologii MCE. Takie rozwiązanie jest zgodne z zapisami Specyfikacji Istotnych Warunków Zamówienia dla tego zadania ale pojawił...
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Model-Driven Testing of Real-Time Embedded Systems - From Object Oriented towards Function Oriented Development
PublikacjaMBD
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A comparative study of sequential extraction methods for identification of trace elements fractions (Cr, Ni, Pb, Cd) in urban soils from several parks
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Bioaccumulation of alkaline soil metals (Ca, Mg) and heavy metals (Cd, Ni, Pb) patterns expressed by freshwater species of Ulva (Wielkopolska, Poland)
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Facilitated transport of Zn(II), Cd(II) and Pb(II) ions trough polymer inclusion membranes with calix[4]-crown-6 derivaties
PublikacjaBadano transport mieszaniny równomolowych ilości jonów Zn(II), Cd(II) i Pb(II)z wodnej fazy azotanowej (cMe=0,001M) przez polimerowe membrany inkluzyjne(PIM) zawierające pochodne kaliks[4]korony-6 jako nośniki jonów. Badany był wpływ różnych podstawników na wydajność procesu. Selektywność transportu przez membrany zawierające jonofory 4 i 5 malała w kolejności Pb(II), Zn(II), Cd(II), natomiast z jonoforem 3 Pb(II), Zn(II)Cd(II)....
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Studies on removal of Zn(II), Cd(II) and Pb(II) ions in polymer inclusion membrane transport with calix[4]-crown-6 derivatives
PublikacjaZbadano selektywność procesu wydzielania jonów cynku(II), kadmu(II) i ołowiu(II) z wodnych roztworów azotanowych zawierających równomolową mieszaninę tych trzech metali (cMe= 0,01 M) w procesie transportu przez polimerowe membrany inkluzyjne (PIM) przy użyciu w roli przenośników jonów pochodnych kaliks[4]-korony-6. Membrany typu PIM syntezowano z trójoctanu celulozy (nośnik), eteru o?nitrofenylopentylowego (pastyfikator) i pochodnych...
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Exploring novel Cd(ii) complexes with 5-methyl-4-imidazolecarboxaldehyde: synthesis, structure, computational insights, and affinity to DNA through switchSense methodology
PublikacjaA series of four Cd(II) complexes with 5-methyl-4-imidazolecarboxaldehyde (L) with different inorganic anions within or outside the coordination sphere of general formula: [CdCl2 L2 ] (1), [CdBr2 L 2] (2), [CdI2L 2] (3), and [CdL4 ](PF6 )2 ·3H2 O (4) was synthesized through one-step and two-step reactions, respectively. All complexes were obtained as colorless crystals without the need for recrystallization and exhibited solubi- lity...
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To Work or Not to Work… in a Multicultural Team?
PublikacjaThe main goal of the article is to present research findings regarding student’s attitude to working in a multicultural team (MCT). Research participants of different cultural background completed the research survey. Their willingness to work in MCT was measured together with factors that influence it. These include factors related to both team members and the task structure. Research findings indicate that the respondents preferred...
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Influence of Cd(II), Cr(VI) and Fe(III) on early steps of deetiolation process in wheat: fluorescence spectral changes of protochlorophyllide and newly formed chlorophyllide
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Coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol – Crystal structures and formation constants in aqueous solution
PublikacjaStability constants were determined for a series of coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol in aqueous solution. The tendency of histaminol to form chelate complexes has been confirmed by the isolation of several complex species in the monocrystalline form and determination of their molecular structures.
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Bamboo-biochar and hydrothermally treated-coal mediated geochemical speciation, transformation and uptake of Cd, Cr, and Pb in a polymetal(iod)s-contaminated mine soil
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Trihalometany (THM)
PublikacjaOpisano powstawanie trohalometanów w trakcie chlorowania wody do picia orazdwie metody ich oznaczania z wykorzystaniem ekstrakcji ciecz-ciecz i ozna-czaniem techniką GC-ECD oraz metodą bezpośredniego dozowania próbki wody dokapilarnej kolumny chromatograficznej połączonej z detektorem wychwytu elek-tronów (DAI-GC-ECD).
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Zastosowanie modułu symulacji dynamicznej programu Autodesk Inventor do badań właściwości dynamicznych odbieraków prądu
PublikacjaW pracy przedstawiono wybrane zagadnienia komputerowego modelowania 3D podzespołów kolejowego odbieraka prądu typu 160 EC oraz jego złożenie jako integralnej konstrukcji w programie Autodesk Inventor. Omówiono sposób implementacji modelu 3D odbieraka w Module Symulacji Dynamicznej (MSD). W symulacji komputerowej badano proces unoszenia się odbieraka pod wpływem zadanego momentu obrotowego. Pokazano wybrane wyniki symulacji dynamicznej...
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Road texture influence on tyre rolling resistance
PublikacjaTyre performance, one of the critical factors for vehicle users, is strongly related to theroad surface characteristics, most notably to the pavement texture. Phenomena that occur at the tyre/road interface affect tyre friction (skid resistance), rolling resistance, tyre wear and tyre/road noise. This article deals with relationship between surface texture and rolling resistance of light and heavy vehicle tyres. Mean profile depth...
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Flowing Liquid Anode Atmospheric Pressure Glow Discharge as an Excitation Source for Optical Emission Spectrometry with the Improved Detectability of Ag, Cd, Hg, Pb, Tl, and Zn
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Information Retrieval with the Use of Music Clustering by Directions Algorithm
PublikacjaThis paper introduces the Music Clustering by Directions (MCBD) algorithm. The algorithm is designed to support users of query by humming systems in formulating queries. This kind of systems makes it possible to retrieve songs and tunes on the basis of a melody recorded by the user. The Music Clustering by Directions algorithm is a kind of an interactive query expansion method. On the basis of query, the algorithm provides suggestions...
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Evaluation of Professional Demands and Financial Reward Through the Perception of Police Managers
PublikacjaThe aim of the study was to examine the relationship between job demands and salary in the subjective perception of mid-level police managers. An occupational stress model in which effort spent on job demands are not balanced by the received reward, was adopted. The study comprised 51 police officers (4 women). The partial least squares method was used for the analysis, and the SmartPLS 2.0 program was applied. The income and...
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How can analysts use multicriteria decision analysis?
PublikacjaProper decision making in multifacitated situation is very challenging task. It is especially difficult if there are many alternatives and criteria that are often contradictory. Analytical chemistry and related sciences involve many situations where decisions on complex problems are made. The support tools may be the use of MCDA (Multi-criteria Decision Analysis) algorithms. They formalize the decision process, make it transparent...
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3-monochloro-1,2-propandiol w produktach żywnościowych
Publikacja3-monochloro-1,2-propandiol (3-MCPD) jest związkiem należącym do grupy zanieczyszczeń żywności zwanych chloropropanolami. Powstaje on w produktach żywnościowych poddanych działaniu podwyższonej temperatury. Po raz pierwszy jako zanieczyszczenie żywności został zidentyfikowany w 1978 roku w roślinnych hydrolizatach białkowych i produktach pochodnych takich jak sosy sojowe. Później jego obecność wykryto w wielu popularnych produktach...
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Bio polyetherurethane composites with high content of natural ingredients: hydroxylated soybean oil based polyol, bio glycol and microcrystalline cellulose
PublikacjaIn our study, we focused on obtaining bio-polyurethane composites using bio-components such as bio glycol, modified natural oil-based polyol, and microcrystalline cellulose (MCC). The pre-polymer method was used to prepare the bio polyurethane matrix. Prepolymer was synthesized using 4,4’-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 50 wt.% of commercial polyether and 50 wt.% of hydroxylated soybean oil (H3)....
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Snapshot of micro-animals and associated biotic and abiotic environmental variables on the edge of the south-west Greenland ice sheet
PublikacjaMicroinvertebrates play a role as top consumers on glaciers. In this study we tested what kind of cryoconite material the animals inhabit (mud vs granules) on the edge of the Greenland ice sheet (GrIS) in the south-west. We also tested the links between the densities of micro-fauna in cryoconite material and selected biotic (algae, cyanobacteria, bacterial abundances) and abiotic (water depth, pH, ion content, radionuclides) factors....
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Udział podmiotów gospodarczych determinantą transformacji współczesnego miasta w kierunku inteligentnego miasta
PublikacjaWraz ze wzrostem populacji, miasta dotykają złożone problemy. Skalę problemu ilustrują liczby: w 2008 r. na terenach zurbanizowanych żyło ponad 50% światowej populacji, czyli około 3,3 mld ludzi, zaś do 2030 r. prognozuje się wzrost liczby ich mieszkańców do ok. 5 mld. Jedną z koncepcji poprawy warunków życia jest koncepcja smarc city (SC) - inteligentnego miasta.
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Multicriteria decision analysis in ranking of analytical procedures for aldrin determination in water
PublikacjaThe study presents the possibility of multi-criteria decision analysis (MCDA) application when choosing analytical procedures with low environmental impact. A type of MCDA, Preference Ranking Organization Method for Enrichment Evaluations (PROMETHEE), was chosen as versatile tool that meets all the analytical chemists – decision makers requirements. Twenty five analytical procedures for aldrin determination in water samples (as...
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Derecho Evolving from a Mesocyclone—A Study of 11 August 2017 Severe Weather Outbreak in Poland: Event Analysis and High-Resolution Simulation
PublikacjaThis study documents atmospheric conditions, development, and evolution of a severe weather outbreak that occurred on 11 August 2017 in Poland. The emphasis is on analyzing system morphology and highlighting the importance of a mesovortex in producing the most significant wind damages. A derecho-producing mesoscale convective system (MCS) had a remarkable intensity and was one of the most impactful convective storms in the history...
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Mission impossible for cellular internalization: When porphyrin alliance with UiO-66-NH2 MOF gives the cell lines a ride
PublikacjaIs it possible to accelerate cell internalization by hybridization of nanomaterials? Herein we support the realization of using metal-organic frameworks (MOFs) with the assistance of rigid porphyrin structure (H2TMP) aimed at drug loading, drug release, relative cell viability, and targeted in vitro drug delivery. There are several MOFs, i.e., UiO-66-NH2 (125 ± 12.5 nm), UiO-66-NH2 @H2TMP (160 ± 14 nm), UiO-66-NH2 @H2TMP@DOX, and...
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New clicked full agonists of the estrogen receptor β
PublikacjaA click chemistry approach was used to synthesize a series of 1,4-diaryl-substituted 1,2,3-triazoles designed to behave as estrogen receptor (ER) ligands. We studied their affinities for both receptors α and β, their agonist activities in a cell-based luciferase reporter assay and their effect on the proliferation of the hormone-dependent MCF-7 cell line. We found two compounds (3a and 3c) that behave as selective full agonists...
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The use of Response Surface Methodology for reliability estimation of aluminum silo subjected to wind load
PublikacjaAn axisymmetric aluminum silo model with a single, standardized geometric imperfection of its lateral surface is considered. The silo is wind – loaded only. The paper is focused on the critical, or limit value of wind pressure, both producing a loss of stability of the silo. This value is affected by vertical coordinate (position) of the imperfection and the angular relation between the imperfection and the wind direction. Reliability...
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Single and Series of Multi-valued Decision Diagrams in Representation of Structure Function
PublikacjaStructure function, which defines dependency of performance of the system on performance of its components, is a key part of system description in reliability analysis. In this paper, we compare two approaches for representation of the structure function. The first one is based on use of a single Multi-valued Decision Diagram (MDD) and the second on use of a series of MDDs. The obtained results indicate that the series of MDDs...
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A novel hybrid adaptive framework for support vector machine-based reliability analysis: A comparative study
PublikacjaThis study presents an innovative hybrid Adaptive Support Vector Machine - Monte Carlo Simulation (ASVM-MCS) framework for reliability analysis in complex engineering structures. These structures often involve highly nonlinear implicit functions, making traditional gradient-based first or second order reliability algorithms and Monte Carlo Simulation (MCS) time-consuming. The application of surrogate models has proven effective...