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Method of selecting the LS-SVM algorithm parameters in gas detection process
PublikacjaIn this paper we showed the method of resistive gas sensors data processing. The UV irradiation and temperature modulation was applied to improve gas sensors’ selectivity and sensitivity. Noise voltage across the sensor’s terminals (proportional to its resistance fluctuations) was recorded to estimate power spectral density. This function was an input data vector for LS-SVM (least squares – support vector machine) algorithm, which...
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Investigation of solid polymer electrolyte gas sensor with different electrochemical techniques
PublikacjaIn this work solid polymer electrolyte (SPE) amperometric sulphur dioxide sensor is investigated. Nafion was used as a membrane electrode and 1M sulphuric acid as an internal electrolyte. Sensor response to sulphur dioxide was measured. Besides traditional constant voltage amperometry also different electrochemical techniques were used. Results obtained by these methods are compared.
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A commercial gas boiler fitted with the ORC module as perspective solution for households
PublikacjaIn this paper the applicability of the commercial gas boiler (De Dietrich DTG X23N) coupled with the laboratory prototype micro ORC setup was experimentally studied. The main objective was to determine the working fluid capability to obtain required temperatures of vapour prior to the turbine, attainable heat rates and efficiencies of the whole system. The boiler thermal power was 25 kW. Tests were carried out with a single stage...
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublikacjaAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Standard gas mixtures- indispensable reference materials in the analysis of gaseous media
PublikacjaIn recent years the need for the quality control and assurance of analytical measurement results has been particularly strongly emphasised. Certified reference materials play an invaluable role in this process. The article characterises the basic types of reference materials, focusing in particular on those in the gaseous state. It also reviews the literature on the techniques of preparing standard gas mixtures over the last ten...
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On the Nonlinear Effects of Magnetoacoustic Perturbations in a Perfectly Conducting Viscous and Thermoconducting Gas
PublikacjaNonlinear effects of planar and quasi-planar magnetosound perturbations are discussed. The plasma is as- sumed to be a Newtonian thermoconducting gas with infinite electrical conductivity permeated by a magnetic field orthogonal to the trajectories of gas particles. Generation of the non-wave modes (magnetoacoustic heating and streaming) in the field of periodic and aperiodic magnetoacoustic perturbations is discussed. The results...
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Analysis of odor interactions in ternary gas mixtures using electronic nose
PublikacjaIn recent years there has been a noticeable increase in interest in the use of electronic noses in analytical chemistry. These devices perform a holistic analysis of the gas mixtures composition, without the separation and identification of its individual components. For this reason e-noses are increasingly replacing the conventional olfactometers, due to the significantly shorter analysis time and possible automation. In the work...
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Degradation of protective coatings in steel chimneys of flue gas desulfurisation system
PublikacjaThis paper presents problems associated with corrosion of steel stacks and changes in philosophy of corrosion protection when implemented into flue gas desulphurization systems. In-situ tests were taken by means of electrochemical impedance spectroscopy at the stack which discharges flue gas before wet lime/limestone desulphurization. A very quick electrolyte absorption by the spherical infill vinylester coating was found using...
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Standard gas mixtures – indispensable reference materials in the analysis of gaseous media
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Effects of a rotating magnetic field on gas-liquid mass transfer coefficient
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Dissociative electron attachment to gas phase thiothymine: experimental and theoretical approaches
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Non-Wave Variations in Temperature Caused by Sound in a Chemically Reacting Gas
PublikacjaA weakly nonlinear generation of non-acoustic modes in the field of sound in a gas is considered. An exotericchemical reaction of A->B type, which takes place in a gas, may be reversible or not. Two types of sound areconsidered, low-frequency and high-frequency as compared with the characteristic time of a chemical reaction.For both these cases, the governing equations of non-acoustic modes are derived and conclusions of the efficiencyof...
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Standard gas mixtures- indispensable reference materials in the analysis of gaseous media
PublikacjaIn recent years the need for the quality control and assurance of analytical measurement results has been particularly strongly emphasised. Certified reference materials play an invaluable role in this process. The article characterises the basic types of reference materials, focusing in particular on those in the gaseous state. It also reviews the literature on the techniques of preparing standard gas mixtures over the last ten...
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Control of mass concentration of reagents by sound in a gas with nonequilibrium chemical reactions
PublikacjaThe weakly nonlinear dynamics of a chemically reacting gas is studied. Nonlinear interaction of acoustic and nonacoustic types of motion are considered. We decompose the base equations using the relationships of the gas-dynamic perturbations specific for every type of motion. The governing equation for the mass fraction of a reagent influenced by dominating sound is derived and discussed. The conclusions concern the equilibrium...
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Operational causes of fatigue failures within the passages of gas turbine engines
PublikacjaThe short profile of a fatigue wear process of gas turbine engine's constructional elements has been introduced in the article. The primary causes of a fatigue cracks formation within the mechanical system as well as within the passages of the engine have been showed. Especial attention was devoted to the low-cycle fatigue, what is associated with unsteady thermal-flow processes being worked out in the passages.The selected damages...
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Non-matrix reference materials-the challenges in the preparation of standard gas mixtures
PublikacjaIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials.
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Non-matrix reference matrials- chalanges in the preparation of standard gas mixtures
PublikacjaIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials. In addition, a review of literature on techniques of preparation of gaseous standard materials, published...
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Liquid circulation in the agitated airlift reactor with the high gas disengagement zone
PublikacjaPrzedstawiono doświadczalne zależności stopnia zatrzymania gazu i prędkości cyrkulacji cieczy od prędkości przepływu gazu i częstości obrotów mieszadła. Obserwowano wzrost prędkości cyrkulacji cieczy ze wzrostem wysokości strefy napowietrzania. Dla niskich częstości obrotów mieszadła prędkość cyrkulacji cieczy wzrastała wraz ze wzrostem prędkości przepływu gazu, natomiast dla wysokich cząstości obrotów mieszadła prędkość cyrkulacji...
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Weakly nonlinear dynamics of short acoustic waves in exponentially stratified gas
PublikacjaRozpatruje się dynamika krótkich (w porównywaniu z charakterystyczną skalą zmiany gęstości gazu atmosferycznego) fal akustycznych. Wyprowadzone nowe równanie ewolucyjne, które uwzględnia dyspersję i nieliniowy charakter propagacji tych fal. Porównuje sie liniowa i nieliniowa dynamika. Ilustracje propagacji, numeryczne wyliczione na podstawie nowych wzorów, są przedstawione. Indexed and abstracted (from vol. 32(1) 2007) in Science...
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Nonlinear Interaction of Modes in a Planar Flow of a Gas with Viscous and Thermal Attenuation
PublikacjaThe nonlinear interaction of wave and non-wave modes in a gas planar flow are considered. Attention is mainly paid to the case when one sound mode is dominant and excites the counter-propagating sound mode and the entropy mode. The modes are determined by links between perturbations of pressure, density, and fluid velocity. This definition follows from the linear conservation equations in the differential form and thermodynamic...
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Concentration levels of selected analytes in the gas phase of an e-cigarette aerosol
PublikacjaThe aerosols generated from e-cigarettes are composed of liquid and gas phases resulting from vapourized e-liquid. The apportioning of substances from e-liquid into the liquid and gas phases during e-cigarette use has not been extensively studied. Partitioning of e-liquid components between the gas and the liquid phase of the aerosol influences the substances inhaled and exhaled by the users, leading to second-hand exposure. It...
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Special Issue on “Advanced Liquid Waste and Gas Waste Treatment Processes”
PublikacjaThe editorial contains a short review of the content of the Special Issue on waste gas and liquid streams treatment strategies.
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From flow to jamming: Lattice Gas Automaton simulations in granular materials
PublikacjaWe introduce the first extension of a Lattice Gas Automaton (LGA) model to accurately replicate observed emergent phenomena in granular materials with a special focus on previously unexplored jamming transitions by incorporating gravitational effects, energy dissipation in particle collisions, and wall friction. We successfully reproduce flow rate evolution, density wave formation, and jamming transition observed in experiments....
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublikacjaThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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New approaches for improving selectivity and sensitivity of resistive gas sensors: a review
PublikacjaPurpose – This paper aims to present the methods of improving selectivity and sensitivity of resistance gas sensors. Design/methodology/approach – This paper compares various methods of improving gas sensing by temperature modulation, UV irradiation or fluctuation-enhanced sensing. The authors analyze low-frequency resistance fluctuations in commercial Taguchi gas sensors and the recently developed tungsten trioxide (WO3) gas-sensing...
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New approaches for improving selectivity and sensitivity of resistive gas sensors: A review
PublikacjaResistive gas sensors are very popular and reliable but suffer from low selectivity and sensitivity. Various methods have been suggested to improve both features without increasing the number of sensors in gas detection systems. Fluctuation enhanced gas sensing was proposed to improve gas detection efficiency by analyzing low-frequency resistance fluctuations, and noise parameters can be more informative than the single DC resistance...
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Process control of air stream deodorization from vapors of VOCs using a gas sensor matrix conducted in the biotrickling filter (BTF)
PublikacjaThis article presents the validity, advisability and purposefulness of using a gas sensor matrix to monitor air deodorization processes carried out in a peat-perlite-polyurethane foam-packed biotrickling filter. The aim of the conducted research was to control the effectiveness of air stream purification from vapors of hydrophobic compounds, i.e., n-hexane and cyclohexane. The effectiveness of hydrophobic n-hexane and cyclohexane...
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Recent Trends in the Application of Chromatographic Techniques in the Analysis of Luteolin and Its Derivatives
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Analysis of Isocratic-Chromatographic-Retention Data using Bayesian Multilevel Modeling
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Maximum A Posteriori Bayesian Estimation of Chromatographic Parameters by Limited Number of Experiments
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Green sample preparation techniques for chromatographic determination of small organic compounds
PublikacjaAccurate monitoring of the state of the environment requires the introduction of additional isolation and/or preconcentration step prior to the chromatographic determination. In this work the information about novel methodological and instrumental solutions in relation to different variants of microextraction techniques are presented. Attention is focused on analytical procedure and suitable analytical tools for extraction of the...
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Dynamic Headspace Sampling as an Initial Step for Sample Preparation in Chromatographic Analysis
PublikacjaThis work represents a brief summary of the use of dynamic headspace (DHS) as a technique for sample preparation in chromatographic analysis. Despite numerous developments in the area of analyte isolation and enrichment, DHS remains one of the fundamental methods used with GC. In our opinion, interest in this technique will not diminish significantly because it conforms to stipulations of green analytical chemistry. Moreover, DHS...
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Analysis of volatile fraction selected hybrid fruits using chromatographic techniques
PublikacjaAt present, "healthy eating" is gaining in popularity. Many people associate this term with eating plenty of vegetables and fruits. The basic elements influencing the selection of fruit are their appearance and smell. Of course, their origin and impact on human health are also very important. In recent years, exotic fruits have become increasingly accessible, making them gaining popularity, even among Poles. You can also meet plants...
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Modeling of chromatographic lipophilicity of food synthetic dyes estimated on different columns
PublikacjaBadano parametry retencyjne wybranych syntetycznych barwników żywności z wykorzystaniem techniki RP-HPLC z wykorzystaniem kolumn z chemicznie modyfikowanym wypełnieniem typu C-8, C-16, C-18 oraz CN.Uzyskane wyniki mogą być podstawą do stwierdzenia, że badane związki charakteryzują się podobnymi parametrami retencyjnymi w stosunku do kolumn z fazą stacjonarną typu C-8, C-16 oraz C-18.
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Determination of estrogenic endocrine disruptors in environmental samples - a review of chromatographic methods
PublikacjaWśród związków endokrynnych to estrogeny zarówno naturalne jak i syntetyczne zostały wskazane i opisane jako związki niosące ze sobą największy potencjał aktywności estrogennej. Wysoki potencjał estrogenny jaki posiadają związki z grupy hormonów płciowych potwierdziły badania przeprowadzone zarówno in vitro jak i in vivo. W dużej części (50-95%) próbek ścieków pochodzących z oczyszczalni ścieków zostały wykryte związki z grupy...
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Challenges in preparing honey samples for chromatographic determination of contaminants and trace residues
PublikacjaThe determination of contaminations and residues in honey is of growing concern over past few years, especially that these compounds can not only diminish beneficial properties of honey but more importantly, if present in significant amounts, can pose serious threat to human health. Since honey is characterized by complex composition of the matrix sample, it is often necessary to apply clean-up step, in order to eliminate interfering...
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Recent theoretical and practical applications of micellar liquid chromatography (MLC) in pharmaceutical and biomedical analysis
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Improved chromatography separation for polybrominated diphenyl ether congeners quantification in the food of animal origin
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Can Immobilized Artificial Membrane Chromatography Support the Characterization of Antimicrobial Peptide Origin Derivatives?
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pH Gradient as a Tool for the Separation of Ionizable Analytes in Reversed-Phase High-Performance Chromatography
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Troubleshooting of the determination of bisphenol A at ultra-trace levels by liquid chromatography and tandem mass spectrometry
PublikacjaDetermination of trace amounts of bisphenol A (BPA) may cause problems mainly related to the presence of BPA in solvents (even in LC-MS grade), laboratory vessels, and plastic equipment used for sample preparation. Variable and sometimes significant amounts of BPA present in the background cause problems in obtaining good repeatability of measurements at the ultra-trace levels. Such observations (i.e., poor repeatability of results)...
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Metody detekcji stosowane w chromatografii wykluczania (ang. Size Exclusion Chromatography - SEC)
PublikacjaW pracy przedstawiono oraz scharakteryzowano metody detekcji powszechnie wykorzystywane w chromatografii wykluczania (ang. Size Exclusion Chromatography, SEC), dawniej określanej termi¬nem chromatografia żelowa (ang. GelPermeation Chromatography, GPC). Chromatografia wykluczania umożliwia ustalanie masy cząsteczkowej, a także określanie rozkładu masy cząsteczkowej rzeczywistych mieszanin. W tej odmianie chromatografii cieczowej...
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Determination of cyanide ion in urine samples using ion chromatography with pulsed amperometric detection.
PublikacjaCyanides are widely applied in industrial activity, including gold and silver mining and the production of organic chemicals. HCN is also formed directly from fossil fuel combustion sources from gasoline and diesel vehicles. In natural environment, in plants seeds for example an apple seed, it exists as a cyanogenic glycosides. The amount of cyanide ions originating from food products is however rather small. Larger concentrations...
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Polyfunctional chemically bonded stationary phase for reversed phase high-performance liquid chromatography
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Liquid chromatography tandem mass spectrometry study of urinary nucleosides as potential cancer markers
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Suppression of deleterious effects of free silanols in liquid chromatography by imidazolium tetrafluoroborate ionic liquids
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Comparative study of surface topography of high performance liquid chromatography columns in terms of hydrophobicity
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Separation of anthocyanins from black carrot, chokeberry, blackcurrant, and elderberry with the use of preparative chromatography
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Characterization of In Vitro and In Vivo Metabolism of Antazoline Using Liquid Chromatography-Tandem Mass Spectrometry
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Comparison of Ion Chromatography and Isotachophoresis for the Determination of selected Anions in Atmospheric Wet Deposition Samples
PublikacjaW pracy przedstawiono porównanie wyników oznaczenia zawartości wybranych anionów w próbkach opadów atmoferycznych z zastosowaniem technik izotachoforezy i chromatografii jonowej. Na podstawie otrzymanych wyników można stwierdzić, że technika chromatografii jonowej charakteryzuje się niższymi wartościami granic wykrywalności i oznaczalności, szerokim zakresem pomiarowym i możliwością oznaczania analitów w próbkach o róznym składzie...