wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: BIOSOLID SAMPLES
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DETERMINATION OF SURFACTANTS IN ENVIRONMENTAL SAMPLES - PART I. CATIONIC COMPOUNDS = Oznaczanie Surfaktantów W Próbkach Środowiskowych. Część I. Związki Kationowe
PublikacjaCompounds from the group of cationic surfactants are widely applied in household, industrial, cleaning, disinfectant, cosmetic and pharmaceutical products as their specific properties (antimicrobial, emulsifying, anticorrosion, softening). After use, cationic surfactants are disposed to wastewater-treatment plants and finally with effluent water to surface waters due to their incomplete degradation. Moreover, they can freely circulate...
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Optimization of vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction for quantification of niclosamide in real samples
PublikacjaIn this manuscript, a green and fast vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction (VA-HMDES-DLPME) method was developed for the selective extraction and determination of niclosamide in read samples, including rice, medicine tablets, and water samples. Here, hydrophobic magnetic deep eutectic solvents were used as the extracting solvent without requiring any centrifugation...
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Self-adjusting sub-sample delay estimator based on fractional delaying Hilbert transform filter
PublikacjaZaprezentowano nowe rozwiązanie samo-nastrajalnego estymatora opóźnienia sygnału sinusoidalnego, działającego w czasie dyskretnym. Zastosowano filtr Hilberta o skończonej odpowiedzi ipulsowej (FIR od ang. finite impulse response) zagregowany z filtrem ułamkowo-opóźniającym. Zilustrowano performancję estymatora, również w obecności szumu. Przeanalizowano jego złożoność numeryczną.
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Evaluation of sample injection precision in respect to sensitivity in capillary electrophoresis using various injection modes
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The Indirect Relationship Between Spiritual Experiences and Subjective Wellbeing Through Hope? A Sample of Chilean Students
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Seeking genetic signature of radiosensitivity - a novel method for data analysis in case of small sample sizes
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Evaluation of the impact of geometry and plastic deformation on the stray magnetic field around the bone shaped sample
PublikacjaInfluence of two factors: the variable cross-section and the localized plastic deformation, which affect the stray magnetic field profile of a ferromagnetic sample have been studied. Evaluation of an effect size is based on the analysis of the stray magnetic field component which is tangential to the longest dimension of a sample. However, in order to describe the nature of the stray magnetic field, the normal component (perpendicular...
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Monitoring of volatile organic compounds (VOCs) in atmospheric air. Part II. Sample collection and preparation
PublikacjaThe paper reviews literature information on air sampling techniques commonly used for monitoring volatile organic compounds (VOCs) levels in atmospheric air. It describes containers for collecting samples of atmospheric air, such as vacuum canisters and bags made from synthetic materials. It discusses dynamic, passive and denudational techniques for sampling analytes from air combining isolation with preliminary enrichment, and...
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Determination of environmental pollutants in soil and sediments - some aspects of sample clean-up and GC analysis
PublikacjaPrzedstawiono wstępne wyniki badań nowej procedury analitycznej przeznaczonej do badań próbek i osadów dennych na zawartość związków organicznych (WWAPCB). Procedura składa się z następujących etapów: - ekstrakcji analitów z wykorzystaniem techniki ASE, - oczyszczania ekstraktów (kolumienki), - chromatograficznego rozdzielania i oznaczania analitów.
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Deep eutectic solvents in analytical sample preconcentration Part B: Solid-phase (micro)extraction
PublikacjaOne of the key challenges of modern analytical chemistry is the monitoring of trace amounts of contaminants using sensitive and selective instrumental techniques. Due to the variety and complexity of some samples, it is often necessary to properly prepare a sample and to perform a preconcentration of trace amounts of analytes. In line with the principles of Green Analytical Chemistry (GAC), it is important for an analytical procedure...
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Imaging of biological samples: crassula arborescens
Dane BadawczeOne of the tasks of modern botany is to describe the relationship between climatic conditions and other environmental factors and the anatomical structure and adaptation of species present in given geographic areas. The work [1] focuses on anatomical and morphological studies of leaves of plants from the coarse family. Species tested belong to leaf...
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Acid site concentrations of the MXenes samples
Dane BadawczeData contains the pH of 0.01M NaOH solution, before and after mixing with the MXenes samples.
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Application of the chromatographic retention index system for the estimation of the calibration constants of permeation passive samplers with polydimethylsiloxane membranes
PublikacjaThe paper presents the results of research on the calibration of permeation passive samplers equipped with polydimethylsiloxane (PDMS) membranes using the physico-chemical properties of the analytes. Strong correlations were found between the calibration constants of the samplers and the linear temperature-programmed retention indices of the analytes determined on columns coated with pure PDMS (r2 = 0.914). These correlations...
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Design of a simple modular active power electronic transformer
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The photophysics of β-homo-tyrosine and its simple derivatives
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An efficient algorithm for mobile guarded guards in simple grids
PublikacjaW pracy rozważono problem strzeżenia ortogonalnych krat dwuwymiarowych przez mobilne straże strzeżone. Podano algorytmy wielomianowe m.in. dla przypadku krat prostych i dla przypadku krat bez przeszkód w kierunku poziomym (pionowym).
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Simple and accurate field interpolation in finite difference methods
PublikacjaW artykule wprowadzono nową metodę interpolacji pól w metodzie różnic skończonych. Metoda jest prosta i daje wyniki bardziej dokładne niż w przypadku interpolacji liniowej. Proponowana metoda interpolacji może zostać użyta do poprawienia dokładności takich metod, jak subgridding.
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Simple design criteria and efficiency of hydrodynamic vortex separators
PublikacjaVortex separators are locally applied for waste water treatment in different systems - from storm waste water sewerage to water treatment in fish ponds. However, the methods for separator design presented in the literature are questionable. The paper presents two simple and functional criteria that were employed to construct a laboratory test stand. The test results gave positive feed back on the efficiency of vortex separators.
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Study of Icosahedral Clusters in Close-packed Simple Liquids
PublikacjaThe local structure of liquid copper was determined using Steinhardt order parameters, with particular attention paid to icosahedral clusters. The positions of atoms were obtained from three sets of molecular dynamics simulations, with the forces obtained from: the Sutton-Chen (SC) potential, the Naval Research Laboratory total energy tight-binding (NRL-TB) method and the divide-and-conquer learn-on-the-fly (DCLOTF) method, respectively....
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Medley filters - simple tools for efficient signal smoothing
PublikacjaMedley filters are defined as convex combinations of elementary smoothing filters (averaging, median) with different smoothing bandwidths. It is shown that when adaptive weights of such a mixture are evaluated using the recently proposed Bayesian rules, one obtains a tool which often outperforms the state-of-the-art wavelet-based smoothing algorithms. Additionally, unlike wavelet-based procedures, medley filters can easily cope...
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A simple method for prediction of hydrodynamics forces on a pod propulsor
PublikacjaReferat przedstawia prostą metodę teoretyczną wyznaczania sił hydrodynamicznych na pędniku podowym przy różnych współczynnikach posuwu i kątach dryfu. Metoda jest oparta na elementarnej teorii płatów nośnych i na teorii pędnika idealnego. metoda ta jest podstawą dla programu komputerowego pozwalającego wyznaczać napór, siłę boczną i moment dla pędnika o znanej geometrii i znanych parametrach pracy. Rezultaty obliczeń są porównane...
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Reliability of imperfect structures (simple non-linear models)
PublikacjaPrzyjęto proste modele prętów umożliwiających analizę układów o niestatecznych i statecznych punktach bifurkacji. Wykorzystano symulacyjną metodę wyznaczania niezawodności. Zastosowano metodę Monte Carlo i równania 3 poziomu dokładności. Uzyskano rozkłady prawdopodobieństwa obciążenia granicznego nieliniowych modeli konstrukcji z losowymi imperfekcjami. Wykazano, że histogramy siły granicznej modelu statecznego i niestatecznego...
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A Simple Neural Network for Collision Detection of Collaborative Robots
PublikacjaDue to the epidemic threat, more and more companies decide to automate their production lines. Given the lack of adequate security or space, in most cases, such companies cannot use classic production robots. The solution to this problem is the use of collaborative robots (cobots). However, the required equipment (force sensors) or alternative methods of detecting a threat to humans are usually quite expensive. The article presents...
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Detecting Apples in the Wild: Potential for Harvest Quantity Estimation
PublikacjaKnowing the exact number of fruits and trees helps farmers to make better decisions in their orchard production management. The current practice of crop estimation practice often involves manual counting of fruits (before harvesting), which is an extremely time-consuming and costly process. Additionally, this is not practicable for large orchards. Thanks to the changes that have taken place in recent years in the field of image...
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Simple sufficient condition for subspace to be completely or genuinely entangled
PublikacjaWe introduce a simple sufficient criterion, which allows one to tell whether a subspace of a bipartite or multipartite Hilbert space is entangled. The main ingredient of our criterion is a bound on the minimal entanglement of a subspace in terms of entanglement of vectors spanning that subspace expressed for geometrical measures of entanglement. The criterion is applicable to both completely and genuinely entangled subspaces. We...
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Hydration of Simple Model Peptides in Aqueous Osmolyte Solutions
PublikacjaThe biology and chemistry of proteins and peptides are inextricably linked with water as the solvent. The reason for the high stability of some proteins or uncontrolled aggregation of others may be hidden in the properties of their hydration water. In this study, we investigated the effect of stabilizing osmolyte–TMAO (trimethylamine N-oxide) and destabilizing osmolyte–urea on hydration shells of two short peptides, NAGMA (N-acetyl-glycine-methylamide)...
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A Geometrically Simple Compact Wideband Circularly Polarized Antenna
PublikacjaA compact broadband wide-slot circular polarization (CP) antenna is proposed. An inverted L-shape parasitic strip at the open end of a microstrip line extension and a slot modification is applied to attain wideband CP. The advantage of this technique is simplicity which makes it readily re-designable for different frequency bands. To demonstrate the concept, three designs working at different frequencies are obtained. The redesign...
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Simple observer for induction motor speed sensorless control
PublikacjaPrzedstawiono układ sterowania polowo zorientowanego silnikiem asynchronicznym klatkowym pozwalający na pracę w szerokim zakresie prędkości obrotowych bez użycia czujnika prędkości. Zaproponowano estymator zmiennych o prostej strukturze charakteryzujący się znaczna odpornością na zmiany parametrów silnika. Zależności obserwatora oparte są na równaniach obwodu napięciowego silnika. Pokazano wyniki badań eksperymentalnych.
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FE-simulations of a direct and a true simple shear test
PublikacjaPorównano dwa aparaty ścinania: aparat bezpośredniego ścinania i aparat prostego ścinania. Analizy pola naprężeń i odkształceń dokonano stosując metodę elementów skończonych i mikropolarne prawo hypoplastyczne. Analiza ta pokazała, że pole naprężeń i odkształceń jest niejednorodne w obu aparatach, szczególnie w aparacie bezpośredniego ścinania.
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A Novel Electrochemical Sensor Based on Graphene Oxide Nanosheets and Ionic Liquid Binder for Differential Pulse Voltammetric Determination of Droxidopa in Pharmaceutical and Urine Samples
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Particle swarm optimization–artificial neural network modeling and optimization of leachable zinc from flour samples by miniaturized homogenous liquid–liquid microextraction
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Synthesis of UiO-66-OH zirconium metal-organic framework and its application for selective extraction and trace determination of thorium in water samples by spectrophotometry
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Highly Sensitive Determination of Bisphenol A in Bottled Water Samples by HPLC after Its Extraction by a Novel Th-MOF Pipette-Tip Micro-SPE
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Monitoring of occupational exposure to volatile organohalogen solvents (VOXs) in human urine samples of dry-cleaner workers by TLHS-DAI-GC-ECD procedure
PublikacjaChlorinated hydrocarbon solvents are often used for dry-cleaning clothes in the laundry industry. The object of this study was to monitor the occupational exposure of dry-clean employees coming into contact with VOXs. 25 workers collected their urine samples before the work shift, after 4 hours of work and after the work shift. The analyses of urine samples and solvents used in dry-cleaning were performed using TLHS-DAI-GC-ECD....
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples
PublikacjaCelem prowadzonych badań było opracowanie metodyki oznaczania krótkołańcuchowych kwasów alkanomonokarboksylowych (KKA), opartej na ich izolowaniu i wzbogacaniu za pomocą techniki HS-SPME, a następnie oznaczaniu za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Do ekstrakcji zastosowano włókno pokryte polarną fazą stacjonarną opartą na glikolu polietylenowym (PEG). Dla celów porównawczych zastosowano również...
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Determination of organotin compounds in biological samples using accelerated solvent extraction, sodium tetraethylborate ethylation, and multicapillary gas chromatography flame photometric detection.
PublikacjaPrzedstawiono metodę oznaczania związków cynoorganicznych w próbkach biologicznych. Procedura oparta jest na wykorzystaniu ekstrakcji pod zwiększoną temperaturą i ciśnieniem (ASE) do izolacji związków cynoorganicznych z próbek wątroby morświnów odłowionych w Morzu Bałtyckim. Walidacji metody dokonano na podstawie analizy materiału odniesienia NIES No 11.
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Application of chemometric modeling for ionic liquid-based ultrasonic-assisted dispersive liquid-liquid microextraction: Analysis of fosetyl-aluminum in fruit and vegetable samples
PublikacjaThis manuscript presents a new method for selective extraction and determination of fosetyl-aluminum in fruits and vegetable samples based on ultrasonic-assisted dispersive liquid-liquid microextraction method using ionic liquids (IL-UA-DLLME). A UV-Visible spectrophotometer was used for detection and quantification. Plants used for sample collection were grown under controlled conditions in a greenhouse. Central composite design...
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Green capsule phase microextraction employing hydrophobic monolithic sol-gel octadecyl siloxane platforms for the monitoring of organophosphorus pesticides in environmental water samples
PublikacjaIn this study, a novel, facile and green capsule phase microextraction (CPME) method is presented for the extraction and preconcentration of organophosphorus pesticides (i.e., chlorpyrifos, disulfoton, ethoprophos, fenchlorphos, prothiofos, and parathion-methyl) from environmental water samples. Monolithic sol-gel octadecyl siloxane (sol-gel C18) sorbent encapsulated within porous polypropylene capsules was synthesized, characterized,...
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Solid-Contact Ion-Selective Electrodes with Highly SelectiveThioamide Derivatives of p-tert-Butylcalix[4]arene for theDetermination of Lead(II) in Environmental Samples
PublikacjaThioamide derivatives of p-tert-butylcalix[4]arene were used as ionophores in the development of solid-contact ion-selective electrodes based on conducting polymer poly(3,4-ethylenedioxythiophene)/polystyrene sulfonate (PEDOT/PSS) which was synthesized by electrodeposition on the glassy carbon electrodes. The typical ion-selective membranes with optionally two different plasticizers [bis(2-ethylhexyl)sebacate (DOS) and 2-nitrophenyl...
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Determination of modifier contents in polymer-modified bitumens and in samples collected from the roads using high performance gel permeation/size exclusion chromatography
PublikacjaThis paper describes application of high performance gel permeation/size exclusion chromatography (HP-GPC/SEC) for the determination of content of polymer modifiers in modified road bitumens. The obtained results were compared with the measurements based on the procedure recommended by the American Association of State Highway and Transportation Officials, which employs Fourier transform mid-infrared spectroscopy (mid-IR FTIR)....
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Application potential of dummy molecularly imprinted polymers as solidphase extraction sorbents for determination of low-mass polybrominated diphenyl ethers in soil and sediment samples
PublikacjaDespite the introduction of restrictive regulations in the USA and the European Union, polybrominated diphenyl ethers (PBDEs) are still found in various types of environmental and biological samples at significant concentration levels. The presence of these persistent organic pollutants in the environment raises important issues because of their negative impact on immunological and neurological systems, and on the hormonal balances...
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Application of analytical procedure based on accelerated solvent extraction and ion chromatography technique for determination of thiocyanate and other inorganic ions in human placenta samples
PublikacjaExposure of a pregnant woman during pregnancy is a special case of exposure to toxic substances. Samples of placenta collected for the studies had been prepared with the technique of accelerated solvent extraction and later analyzed for the presence of thiocyanate ion and other inorganic ions, with the use of the technique of ion chromatography. The concentration of thiocyanate ion in placenta samples collected from active smokers...
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Portable computer diagnostics system PSD - the measurement potentiality and application examples
PublikacjaOpisano system diagnostyczny do pomiarów statycznych i dynamicznych wszelkiego typu maszyn stosowanych w przemyśle drzewnym. ocena stanu maszyny może byc dokonywana na podstawie wyników pomiaru bicia osiowego i promieniowego wrzecion, pił tarczowych, przemieszczeń poprzecznych piły tasmowej itp.. System jest wyposażony w specjalne oprogramowanie i pozwala m. in. na przeprowadzanie szczegółowych analiz tj. wykonywanie FFT lub filtrowanie...
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Mitochondrial DNA of Anisakis simplex S.S. as a Potential Tool for Differentiating Populations
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GREEN AREAS IN THE NEW CONCEPTS OF DEVELOPMENT OF CITIES AND METROPOLIS ON SELECTED EXAMPLES
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Examples of a use of the optimal control at energy performance index in mechatronic approach
PublikacjaW pracy zaprezentowano przykłady zastosowania sterowania optymalnego przy energetycznym wskaźniku jakości w rozwiązaniach mechatronicznych. Rozważano układy mechaniczne modelowane dyskretnie. Metody sterowania optymalnego znalazły zastosowanie w robotyce (kołowe roboty mobilne jako układy silnie nieliniowe) oraz obróbce szybkościowej przedmiotów podatnych frezem kulistym.
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New Challenges in Management and Economics in 21st century. Selected studies and examples
PublikacjaIn Chapter 1 authors describe the method used to assess the level of readiness of an organization to introduce the Lean Six Sigma concept supporting the Quality 4.0 assumptions, which is gaining more and more interest not only in large organizations, but also in the SME sector. Its use will be illustrated by the example of a small service company. Chapter 2 presents the characteristics of blockchain technology applications in the...
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Isotropic damage in viscoplastic flow conditions, fem applications with practical examples
PublikacjaW pracy omówiono niektóre zagadnienia zniszczenia w warunkach płynięcia lepkoplastycznego. Podano podstawowe prawa konstytutywne jakie mogą tu być zastosowane oraz sposoby identyfikacji parametrów materiałowych. Pokazano przykład zastosowania.
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Pedestrian and bicycle bridges as examples of safe collision-free road crossings
PublikacjaPedestrians are most at risk when they are crossing the road. This represents a significant proportion of all fatalities among pedestrians, amounting respectively to 50% in non-built-up areas and 75% in built-up areas. The most frequent reason for this accident is failure to give way. What is most terrible is that 30% of pedestrian accidents occurred at marked pedestrian crossings. Therefore, an important part of pedestrian safety...
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Informal practices in urban planning and governance. Examples from Polish cities
PublikacjaPlanning has a formal, legally defined component and an informal component developed in response to deficiencies in the planning system. Informal practices can contribute to the development of tools that would improve urban governance, especially in areas related to space. This article presents an overview of informal practices that have taken place in Polish cities and towns in recent years and offers an assessment of their impact...