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Wyniki wyszukiwania dla: wax crystals
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Analiza wad powierzchni gorącowalcowanych wyrobów stalowych = Hot rolled sections surface defects analysis
PublikacjaZanalizowano hutnicze wady powierzchni dwuteowników walcowanych na gorąco, głebokość zdefektowanych obszarów i zmiany mikrostruktury w tych obszarach.
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Wpływ warunków techniczno - eksploatacyjnych na występowanie i rozwój wad w szynach kolejowych
PublikacjaW artykule scharakteryzowano odcinek doświadczalny oraz przeanalizowano sześć wybranych przypadków wpływu warunków techniczno-eksploatacyjnych na występowanie i rozwój wad.
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Polynomial analysis as a new way of describing dynamic impedance spectra – Differential and relative impedance spectra
PublikacjaModel measurements of an equivalent electrical system were carried out using the technique of Dynamic Electrochemical Impedance Spectroscopy. The measurement took the form of potentiodynamic changes imposed on the tested system. Using the possibility of continuous impedance measurements, an attempt was made to develop an original and innovative method of analyzing impedance spectrograms, which is termed polynomial analysis. As...
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Dynamic Charging of Electric Buses as a Way to Reduce Investment Risks of Urban Transport System Electrification
PublikacjaNight charging and fast charging are currently the two most common systems for charging electric buses. Despite the fact that numerous trial installations were started, neither of these two systems has obtained unqualified approval of the users. The alternative is to charge vehicles in motion - dynamic charging which combines the advantages of trolleybus transport and of electric buses. One of the advantages is the reduction of...
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Report vconcerning corrosion reasons of s/y Lunar hull surface and possible way of repair
PublikacjaDokonano oceny korozji kadłuba jednostki pływającej, przyczyn powstania korozji oraz zaproponowano sposoby naprawy miejsc skorodowanych.
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A New Canon of the Modernist Villa of the 1930s - a Villa with a Semicircular Veranda. The Post-War Continuation of the Idea
PublikacjaThe articcle presents a new type of villa, which started to be popular in Gdynia in the 1930s. It was a villa with a semicircular veranda. Villas of that type were continously built also after the II World War
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Interplay between Aryl···Perfluoroaryl and Hydrogen Bonding Interactions in Cocrystals of Pentafluorophenol with Molecules of Trigonal Symmetry
PublikacjaCocrystals of seven star-shaped triaryl compounds with pentafluorophenol (pfp) were prepared and structurally characterized by the single-crystal X-ray diffraction method. Cocrystallization of pfp with planar (or almost planar) compounds gave six 3:1 molecular complexes with well-defined layered structures. The layers are composed of alternating pfp3 trimers, linked by hydrogen bonding, and triaryl molecules held together in planes...
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Self-assembly of secondary aryl amides in cocrystals with perfluoroaryl coformers: structural analysis and synthon preferences
PublikacjaCooperation of aryl⋯perfluoroaryl stacking interactions and hydrogen bonds was utilized in the construction of six novel cocrystals of aromatic cis-amides with pentafluorobenzoic acid (pfba) and pentafluorophenol (pfp). They were obtained by crystallization from solution and structurally characterized. In four instances, the components form heterotetrameric motifs, in which amide:amide homodimer interacts symmetrically on two sides...
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Personal income tax - tax scales in 1992–2019
Dane BadawczeThe tax rate is the ratio (usually expressed as a percentage) at which a business or person is taxed. There are several methods used to present a tax rate: statory, average, marginal, and effective. These rates can also be presented using different definitions applied to a tax base: inclusive and exclusive.
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Personal income tax - tax scales in 1992–2019
Dane BadawczePersonal income tax in Poland is regulated by the Act of July 26, 1991. In addition, the rights and obligations of the taxpayer of this tax result from a number of provisions of the Polish Constitution, many statutes and ratified international agreements and executive regulations. This research data contains information on the amount of tax in Poland...
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Application of the LPE-Grown LuAG: Ce Film/YAG Crystal Composite Thermoluminescence Detector for Distinguishing the Components of the Mixed Radiation Field
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(Cyclopentadienyl){(N,N-dimethylaminoethyl)cyclopentadienyl} complexes of zirconium: Crystal structure of [(η5-C5H5)(η5-C5H4CH2CH2NHMe2)ZrCl2]2[ZrCl6]
Publikacja(C5H5)ZrCl3 reaguje z [C5H4-CH2CH2NMe2]Li dając polimer koordynacyjny {(C5H5)(C5H4-CH2CH2NMe2)ZrCl2}n, który z kolei w reakcji z HCl daje żółtozielone kryształy [(η5-C5H5)(η5-C5H4CH2CH2NHMe2)ZrCl2]2[ZrCl6]. Ten ostatni związek został scharakteryzowany za pomocą widm NMR oraz przy użyciu rentgenowskiej analizy strukturalnej. Utworzenie w/w związku wskazuje na oderwanie grup C5H5 oraz C5H4-CH2CH2NMe2 od centrum metalicznego Zr(IV).
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Effect of Aromatic System Expansion on Crystal Structures of 1,2,5-Thia- and 1,2,5-Selenadiazoles and Their Quaternary Salts: Synthesis, Structure, and Spectroscopic Properties
PublikacjaRational manipulation of secondary bonding interactions is a crucial factor in the construction of new chalcogenadiazole-based materials. This article reports detailed experimental studies on phenanthro[9,10-c][1,2,5]chalcogenadiazolium and 2,1,3-benzochalcogenadiazolium salts and their precursors. The compounds were synthesized, characterized employing NMR and UV-Vis spectroscopy. TD-DFT calculations were also performed. The influence...
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Copper and copper-manganese 1D coordination polymers: Synthesis optimization, crystal structure and preliminary studies as catalysts for Baylis–Hillman reactions
PublikacjaThis work reports the influence of experimental parameters (pH and counter-ion) in the synthesis of the 1D coordination polymer [Cu(IDA)(H2O)2]n (IDA = iminodiacetate), named here Cu-IDA. Copper-manganese bimetallic coordination polymers were also obtained by isomorphic replacement into Cu-IDA structure, with different molar ratio of Cu2+ and Mn2+ ions, denoted here as Cu/Mn-IDA (0.9/0.1; 0.7/0.3 and 0.5/0.5). New coordination...
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Copper(I) halide cluster-based coordination polymers modulated by chiral ditopic dithiodianthranilide ligands: synthesis, crystal structure and photoluminescence
PublikacjaReaction of copper(I) halides with chiral dithiodianthranilidesmdtaandbdtaafforded polymeric complexeswhere polynuclear CuX clusters were linked together by ditopic bridging ligands into 1D chains or 2D layerstructures. In the case of racemic ligands double stranded chain polymers were formed where the Cu4X4(X = I or Br) cores are connected by enantiomeric pairs of the ditopic ligands. In contrast, a homochiralmdtaligand created...
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Novel 1,2,3-Triazole Derivatives as Mimics of Steroidal System—Synthesis, Crystal Structures Determination, Hirshfeld Surfaces Analysis and Molecular Docking
PublikacjaHerein, we present the synthesis and crystal structures determination of five 4-(1-phenyl-1H-1,2,3-triazol-4-yl)phenol derivatives containing halogen atoms, 6a–e, which may be used as an excellent mimic of steroids in the drug development process. Good quality crystals obtained for all of the synthesized compounds allowed the analysis of their molecular structures. Subsequently, the determined crystal structures were used to calculate...
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Black Devils in Normandy—Identification of an Unknown Soldier Found in the Polish War Cemetery of Urville-Langannerie (France)
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Precyzyjna lokalizacja i parametryzacja wad korozyjnych ścianek rurociągów stalowych przy wykorzystaniu tłoków inteligentnych
PublikacjaW artykule przedstawiono sposoby pozyskiwania danych o stanie technicznym dalekosiężnych rurociągów stalowych, w szczególności ropy surowej i paliw ropopochodnych. Scharakteryzowano kilka technik diagnostyki rur przy pomocy autonomicznych urządzeń pomiarowych typu ''tłok inteligentny'', z podziałem na typy wykrywanych obiektów: deformacja średnicy wewnętrznej, korozja i wady materiałowe, zmiany w trajektorii rurociągu. Przedstawiono...
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Occlusion phenomenon of redox probe by protein as a way of voltammetric detection of non-electroactive C-reactive protein
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Implementation of magnitude calculation of complex numbers using improved alpha max plus beta min algorithm
PublikacjaThe paper presents the hardware implementation of the improved alpha max plus beta min algorithm for calculating the magnitude of complex numbers. This version of the algorithm requires the general division which is performed using a noniterative multiplicative division algorithm. We analyze in detail the division algorithm, its error and the impact of finite word-length signal representations on the assumed total computation error....
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Mixing of excimer and exciplex emission: A new way to improve white light emitting organic electrophosphorescent diodes
PublikacjaW pracy opisano konstrukcję wydajnych diod elektrofosforescencyjnych emitujących światło białe. Emisja diod pochodzi od trypletowych monomerów PtL2Cl, trypletowych ekscymerów (PtL2Cl:PtL2Cl) i trypletowych ekscypleksów m-MTDATA (donor elektronu):PtL2Cl (akceptor elektronu), gdzie PtL2Cl oznacza organiczny kompleks platyny (II), a m-MTDATA - dendrymer aminowy. Kwantowa wydajność EL diody wynosi 6.5% fot./e. Współrzędne charakteryzujące...
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Praktyczna ocena zalet i wad stosowania osadów ściekowych do rekultywacji terenów zdegradowanych technicznie.
PublikacjaPrzedstawiono wyniki badań ukierunkowanych na ocenę skuteczności rekultywacji przeprowadzonej na dwóch obszarach zdegradowanych technicznie: składowisku odpadów paleniskowych oraz wyrobisku pożwirowym. Podstawowym celem zrealizowanych prac było określenie chemicznego oddziaływania ustabilizowanych osadów ściekowych na środowisko gruntowe. Udowodniono glebotwórcze właściwości osadów ściekowych, a jednocześnie celowość i zasadność...
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Transformation of the countryside into an open-air museum as a way to rescue its spatial layot and to improve the quality of life
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Evolution of magnetic and transport properties in (Cr1−xMnx)2AlC MAX-phase synthesized by arc melting technique
PublikacjaHerein we initiate a comeback to the arc melting technique to produce MAX-phase solid solutions. Bulk samples of (Cr1−xMnx)2AlC MAX-phase with X = 0, 0.025, 0.05 and 0.1 were synthesized and studied by means of X-ray diffractometry, scanning electron microscopy in combination with energy-dispersive X-ray spectroscopy. Samples were established to be homogeneous with an incorporation of Cr7C3, AlCr2 and Al2O3 secondary phases which...
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Methods of determination of C coefficient for period of rolling vessel in calm water for example of pax cargo ship
PublikacjaThis article presents a different approach to calculate the C coefficient needed to determine the period of own rolling vessel in calm water. The C coefficient is usually adopted as the approximate value from the available literature, usually depending on the type of vessel, and less dependent on the loading condition. In experimental studies of marine properties (seakeeping) often have a problem with the selection of the correct...
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Lax-Wendroff and McCormack Schemes for Numerical Simulation of Unsteady Gradually and Rapidly Varied Open Channel Flow
PublikacjaTwo explicit schemes of the finite difference method are presented and analyzed in the paper. The applicability of the Lax-Wendroff and McCormack schemes for modeling unsteady rapidly and gradually varied open channel flow is investigated. For simulation of the transcritical flow the original and improved McCormack scheme is used. The schemes are used for numerical solution of one dimensional Saint-Venant equations describing free...
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A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
PublikacjaPorous iron-based scaffolds were prepared by the simple replica method using polyurethane foam as a template and applying the sintering process in a tube furnace. Their surface morphology was characterized using scanning electron microscopy (SEM) and phase homogeneity was confirmed using X-ray diffraction (XRD). Corrosion behavior was determined using immersion and potentiodynamic polarization methods in phosphate buffered saline...
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Where the Second World War in Europe broke out: the land-scape history of Westerplatte, Gdańsk/Danzig
PublikacjaWesterplatte is known as the place where the Second World War in Europe broke out. However, its history covers many other events involving Polish, German, Russian and even French politics over the last three centuries - neglected by many papers published in the current discussion. Due to its location at the entrance to the main harbour on the Baltic Sea entrance, Wester-platte-Peninsula is cartographically the best-documented part...
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On my way to global science - 1933-2015 memoirs". A volume of memoirs by professor Wiesław Maria Grudzewski
PublikacjaI wish to express my graditude for the oportunity to read excellent on the life and academic work of Professor Grudzewski, and outstanding scientist and unquestioned authority on economic sciences in the area of management science. Professor Grudzewski had an influence on the events presented in his memoirs through his acquaintances and associates.
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Authentication of whisky due to its botanical origin and way of production by instrumental analysis and multivariate classification methods
PublikacjaHeadspacemass-spectrometry (HS-MS), mid infrared (MIR) and UV–vis spectroscopywere used to authenticate whisky samples from different origins and ways of production ((Irish, Spanish, Bourbon, TennesseeWhisky and Scotch). The collected spectra were processed with partial least-squares discriminant analysis (PLS-DA) to build the classification models. In all cases the five groups ofwhiskieswere distinguished, but the best resultswere...
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Selection of effective cocrystals former for dissolution rate improvement of active pharmaceutical ingredients based on lipoaffinity index
PublikacjaNew theoretical screening procedure was proposed for appropriate selection of potential cocrystal formers possessing the ability of enhancing dissolution rates of drugs. The procedure relies on the training set comprising 102 positive and 17 negative cases of cocrystals found in the literature. Despite the fact that the only available data were of qualitative character, performed statistical analysis using binary classification...
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Application of Multivariate Adaptive Regression Splines (MARSplines) Methodology for Screening of Dicarboxylic Acids Cocrystal Using 1D and 2D Molecular Descriptors
PublikacjaDicarboxylic acids (DiAs) are probably one of the most popular cocrystals formers. Due to the high hydrophilicity and non-toxicity, they are promising solubilizes of active pharmaceutical ingredients (APIs). Although DiAs appear to be highly capable of forming multicomponent crystals with various compounds, some systems reported in the literature are physical mixtures the solid state without forming stable intermolecular complex....
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A New Phenylalanine Derivative Acts as an Antagonist at the AMPA Receptor GluA2 and Introduces Partial Domain Closure: Synthesis, Resolution, Pharmacology, and Crystal Structure
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Uniformity of Thermoluminescence and Optically Stimulated Luminescence Signals Over the Length of Doped LiMgPO4 Crystal Rods Grown by Micro-Pulling-Down Method
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5- epi -Incensole: synthesis, X-ray crystal structure and absolute configuration by means of ECD and VCD studies in solution and solid state
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Crystal structure and initial characterization of a novel archaeal-like Holliday junction-resolving enzyme from Thermus thermophilus phage Tth15-6
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Crystal structures of (E)-3-(4-hydroxybenzylidene)chroman-4-one and (E)-3-(3-hydroxybenzylidene)-2-phenylchroman-4-one
PublikacjaThe synthesis and crystal structures of (E)-3-(4-hydroxybenzylidene)chroman-4-one, C16H12O3,I, and (E)-3-(3-hydroxybenzylidene)-2-phenylchroman-4-one,C22H16O3,II, are reported. These compounds are of interest with respect to biological activity. Both structures display intermolecular C—H---O and O—H---O hydrogen bonding, forming layers in the crystal lattice. The crystal structure of compound I is consolidated...
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Focused ion beam-based microfabrication of boron-doped diamond single-crystal tip cantilevers for electrical and mechanical scanning probe microscopy
PublikacjaIn this paper, the fabrication process and electromechanical properties of novel atomic force microscopy probes utilising single-crystal boron-doped diamond are presented. The developed probes integrate scanning tips made of chemical vapour deposition-grown, freestanding diamond foil. The fabrication procedure was performed using nanomanipulation techniques combined with scanning electron microscopy and focused ion beam technologies....
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The crystal structure of (1RS,4RS,5RS,6SR)-5-cyano-5-nitro-6-phenyl-bicyclo[2.2.1]hept-2-ene
PublikacjaStructure of nitronorbornene derivative C14H12N2O2 synthesized in the reaction of cyclopentadiene with E-2-phenyl-1-cyano-1-nitroethene was determined by single crystal X-ray diffraction analysis. It was found that in analyzed molecule the nitro group is in endo-position whereas phenyl group have exo-ori-entation.
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Dual-wavelength laser polarimeter and its performance capabilities
PublikacjaA dual-wavelength optical polarimetric approach has been proposed as a means of elimination of the systematic errors and estimation of the optical anisotropy parameters for a single DKDP crystal. Our HAUP-related polarimeter uses two semiconductor lasers with the neighbouring wavelengths of 635 nm and 650 nm. Based on the temperature dependence analysis of small characteristic azimuths of light polarization with respect to the...
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Kwartalnik Prawa Podatkowego
Czasopisma -
The Behaviour Based Area Coverage of Unknown Environment by Autonomous Mobile Robot Using Modified ''The Way of the Ox'' Algorithm
PublikacjaPrzedstawiono propozycję rozwiązania zagadnienie całkowitego pokrycia terenu w układzie autonomicznego robota mobilnego. W tym celu zmodyfikowano algorytm "siewcy" oraz opracowano odpowiedni model układu, w środowisku Matlab-Simulink. Wykonano serię badań symulacyjnych, których najistotniejsze wyniki opisano w artykule.
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Chemometric determination of solute-affected solvent vibrational spectra as a superior way of information extraction on solute solvation phenomena
PublikacjaW pracy zaprezentowano dwie chemometryczne metody wyznaczania widm zaburzonych rozpuszczalnika oraz liczby cząsteczek zaburzonych, na podstawie zmierzonych serii wibracyjnych widm FT-IR roztworów substancji. Pierwsza z metod została stworzona na podstawie Namiarowej Analizy Faktorowej (ang. Target Factor Analysis). Druga z nich wykorzystuje algorytm izolacji widm czystych składników z serii widm mieszanin. Działanie obu metod zostało...
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New easy way preparation of core/shell structured SnO2@carbon spheres and application for lithium-ion batteries
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Site-selective cation–π interaction as a way of selective recognition of the caesium cation using sumanene-functionalized ferrocenes
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Zastosowanie nieradialnego modelu SBM z ograniczeniami wag do pomiaru efektywności dydaktycznej w szkolnictwie wyższym
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DESIGN AND CONSTRUCTION OF TILTED WALLS IN ACCORDANCE WITH CODES' PROVISIONS ON THE EXAMPLE OF THE CONSTRUCTION OF THE MUSEUM OF THE SECOND WORLD WAR IN GDAŃSK
PublikacjaThe purpose of this article was to introduce the design and construction of tiled walls in accordance to codes' restrictions. The construction of the Museum of the Second World War in Gdańsk was chosen to be an example of its successful use in practice. Theoretical knowledge was based on PN-EN 1992-1-1:2008 and fib Model Code for Concrete Structures 2010. Although codes' recommendations seem curt, practice prove structural advance....
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Perceived technostress while learning a new mobile technology: Do individual differences and the way technology is presented matter?
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Statistical process control in software project management : a way to transfer single incident-related knowledge into organizational knowledge
PublikacjaZaproponowano statystyczne podejście do procesu kontroli zarządzania projektami informatycznymi. Przedstawiono sposób zamiany wiedzy incydentalnej na wiedzę organizacyjną.
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Restructuring of CHP utilities as a way of power system capacity increase as well as economic and ecological characteristics improvement systems.
PublikacjaPrywatyzacja polskiego rynku energii elektrycznej i cieplnej spowoduje zmiany w elektrociepłowniach i elektrowniach przemysłowych. Rezultatem modernizacji są zmiany ekonomiczne i ekologiczne. Przedstawiono możliwość zmniejszenia emisji związków siarki i zwiększenie sprawności elektrowni poprzez dobudowanie do układu konwencjonalnego zespołu turbin gazowych opalanych gazem naturalnym.