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Search results for: SURFACE CHARACTERIZATION
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Polylactide Films with the Addition of Olive Leaf Extract—Physico-Chemical Characterization
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Biodegradable macromolecular conjugates of citropin: Synthesis, characterization and in vitro efficiency study
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Characterization of magnesium doped lanthanum orthoniobate synthesized by molten salt route
PublicationMolten salt synthesis method has been used to prepare the single phase magnesium doped lanthanum orthoniobate. The phase composition has been checked by X-ray diffraction method and the microstructure studies have been performed by scanning electron microscopy. The high temperature properties of the material have been investigated by thermogravimetry and electrochemical impedance spectroscopy. A dependence between sample total...
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Fabrication and characterization of boron-doped nanocrystalline diamond-coated MEMS probes
PublicationFabrication processes of thin boron-doped nanocrystalline diamond (B-NCD) films on silicon-based micro- and nano-electromechanical structures have been investigated. Nanocrystalline boron doped -diamond (B-NCD) films were deposited using Microwave Plasma Assisted Chemical Vapour Deposition (MW PA CVD) method. The variation of B-NCD morphology, structure and optical parameters were particularly investigated. The use of truncated...
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Partial characterization of indigo (Polygonum tinctorium Ait.) plant seeds and leaves
PublicationThe aim of this study was to assess the contents of indigo's bioactive compounds, its antioxidant and anticancer activities in acetone, hexane and DMSO extracts and to compare the overall bioactivity with another more used medicinal plant named prolipid. It was found that the contents of the bioactive compounds in the studied extracts from different parts of indigo plant varied (P < 0.05): the significantly highest content of polyphenols...
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Characterization of PLZT Thin Films for Fast Electro-Optical Sampling Circuits
PublicationW artykule omówiono technologię wytwarzania cienkich warstw wybranych kompozycji ceramik ołowiowo-lantanowo-cyrkonowo-tytanowych, nazywanych ceramikami PLZT. Przedstawiono wyniki badań jakości warstw za pomocą techniki XRD. wyniki pomiaru grubości warstw, ich względnej przenikalności dielektrycznej i współczynnika załamania. Omówiono kierunki dalszych prac.
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Characterization and photocatalytic activity of rare earth metal-doped titanium dioxide
PublicationW publikacji została przedstawiona metoda otrzymywania fotokatalizatorów na bazie TiO2 modyfikowanego erbem i iterbem. Otrzymane nanocząstki zostały scharakteryzowane za pomocą powierzchni właściwej BET, objętości porów. Zostały przedstawione widma absorpcyjne UV-Vis oraz właściwości fluorescencyjne otrzymanych nanoproszków. Dokonano również przedstawienia wyników pomiaru aktywności fotokatalitycznej pod wpływem promieniowania...
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Characterization and Technical Application of Fine Photocatalytical Particles - A Study of the Immobilization of Photocatalysts
PublicationThe main aim of this dissertation was the transfer of photocatalytical laboratory scale experiments to semi-technical scale. Preliminary experiments of the purification of organic chlorine-loaded waters and the immobilization of photocatalysts were performed, which yielded the research back to the roots of synthesis. The first applied research was carried out on treatment of recreational water. Several light sources, particularly...
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Synthesis and structural characterization of new cyclic siloxane with functionalized organic substituents
PublicationOcta(2-pyridyloxy)cyclotetrasiloxane was isolated as the product of the reaction between silicon disulfide and 2-hydroxypyridine. The new compound has been characterised by single crystal X-ray analysis, revealing a planar eight-membered ring with functionalized organic substituents on the silicon atoms.
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Preparation and characterization of porous scaffolds from chitosan-collagen-gelatin composite
PublicationNovel porous scaffolds composed of chitosan, collagen and gelatin were prepared and characterized. For preparing scaffolds gelatin and collagen isolated from fish skins with various physicochemical properties were used. In order to reduce preparation solubility glutaraldehyde in the amount of 1%, w/w relative to the total biopolymers weight in solution was used. All obtained biomaterials showed a homogeneous porosity. Protein polymer...
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Mechanical characterization of a gravel column in a calibration chamber operating as a triaxial cell
PublicationA series of tests considering the behavior of gravel columns was performed. A segment of column with a height of 1 m and a diameter of 0.53 m was modelled in a calibration chamber used as a triaxial cell at three different lateral stress applied. The vertical load transferred on the column head was simulated with steady increase of water pressures in the upper and lower membranes. During the loading the volumetric changes in the...
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Synthesis, characterization, and electrochemical testing of carbon nanotubes derivatized with azobenzene and anthraquinone.
PublicationWielościenne i jednościenne nanorurki węglowe modyfikowano na ścianach bocznych związkami elektrochemicznie aktywnymi, takimi jak azobenzen i antrachinon. Funkcjonalizowane nanorurki badano technikami spektroskopowymi i elektrochemicznymi oraz wykorzystując mikroskopię elektronową. Wyniki tych badań potwierdziły chemiczną modyfikację.
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Optical and photoelectrochemical characterization of pulsed laser deposited Bi4V2O11, BICUVOX, and BIZNVOX
PublicationThin layers of three compounds from the BIMEVOX family (Bi4V2O11, Bi2V0.9Cu0.1O5.35, and Bi2V0.9Zn0.1O5.35) were prepared via pulsed laser deposition technique on quartz, silicon, and platinum foil and tested as photoanodes for water photooxidation. The film formation, as well as the crystallization upon heating, was characterized using X-ray diffraction and Raman spectroscopy. The optical properties were investigated using spectroscopic...
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Fully Isohexide-Based Polyesters: Synthesis, Characterization, and Structure-Properties Relations
PublicationHere we present a novel series of biobasedpolyesters solely based on renewable isohexide building blocks,synthesized via melt polymerization. The recently developedisoidide dicarboxylic acid (IIDCA) was polymerized with rigidrenewable diols such as isosorbide (IS), isomannide (IM),isoidide (II), and the novel 2,5-methylene-extended isoididedimethanol (IIDML). Both IIDCA and IIDML weredeveloped to increase the reactivity of the...
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Copolymerization of Styrene and Pentadecylphenylmethacrylate (PDPMA): Synthesis, Characterization, Thermomechanical and Adhesion Properties
PublicationThe copolymerization of styrene (St) with a bioderived monomer, pentadecylphenylmethacrylate (PDPMA), via atom transfer radical polymerization (ATRP) was studied in this work.The copolymerization reactivity ratio was calculated using the composition data obtained from1HNMR spectroscopy, applying Kelen-Tudos and Finemann-Ross methods. The reactivity ratio of styrene (r1=0.93) and PDPMA (r2=0.05) suggested random copolymerization...
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Simple colorimetric copper(II) sensor – spectral characterization and possible applications
PublicationNew o-hydroxyazocompound L bearing pyrrole residue was obtained in the simple synthetic protocol. The structure of L was confirmed and analyzed by X-ray diffraction. It was found that new chemosensor can be successfully used as copper(II) selective spectrophotometric regent in solution and can be also applied for the preparation of sensing materials generating selective color signal upon interaction with copper(II). Selective colorimetric...
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublicationThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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Analytical methods for exhaustive characterization of Brassica plants and dietary products based on them
PublicationGlucosinolates (GLs), and particularly two classes of their degradation products - isothiocyanates (ITC) and indoles - released upon myrosinase catalyzed hydrolysis, belong to the most promising chemopreventive dietary components. Despite their wide use in plant research, studies on chemopreventive mechanisms and industrial utilization in the production of e.g. dietary supplements, the methods of reliable characterization of myrosinase-GLs...
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Medical-Grade PCL Based Polyurethane System for FDM 3D Printing—Characterization and Fabrication
PublicationThe widespread use of three-dimensional (3D) printing technologies in medicine has contributed to the increased demand for 3D printing materials. In addition, new printing materials that are appearing in the industry do not provide a detailed material characterization. In this paper, we present the synthesis and characterization of polycaprolactone (PCL) based medical-grade thermoplastic polyurethanes, which are suitable for forming...
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Buried Object Characterization by Data-Driven Surrogates and Regression-Enabled Hyperbolic Signature Extraction
PublicationThis work addresses artificial-intelligence-based buried object characterization using FDTD-based electromagnetic simulation toolbox of a Ground Penetrating Radar (GPR) to generate B-scan data. In data collection, FDTD-based simulation tool, gprMax is used. The task is to estimate geophysical parameters of a cylindrical shape object of various radii, buried at different positions in the dry soil medium simultaneously and independently...
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Buried Object Characterization Using Ground Penetrating Radar Assisted by Data-Driven Surrogate-Models
PublicationThis work addresses artificial-intelligence-based buried object characterization using 3-D full-wave electromagnetic simulations of a ground penetrating radar (GPR). The task is to characterize cylindrical shape, perfectly electric conductor (PEC) object buried in various dispersive soil media, and in different positions. The main contributions of this work are (i) development of a fast and accurate data driven surrogate modeling...
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Comprehensive study on graphene hydrogels and aerogels synthesis and their ability of gold nanoparticles adsorption
PublicationGraphene hydrogels were prepared by ascorbic acid-assisted gelation of graphene oxide (GO) aqueous suspensions both in acidic and basic conditions. Different mass ratio of ascorbic acid (AA) to GO was used (namely 20:1 and 10:1). In order to eliminate the influence of AA on the final structure of hydrogels, samples without AA were prepared by a hydrothermal gelation of GO in an autoclave. An in-depth structural characterization...
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Piezoresponse force microscopy and dielectric spectroscopy study of Ba0.6Sr0.4TiO3 thin films
PublicationResearch on synthesis, characterization and determination of processing – structure – property relationships of commercially important ferroelectric thin films has been performed. The sol-gel-type solution deposition technique was applied to produce good quality thin films of Ba0.6Sr0.4TiO3 (BST60/40) chemical composition on the stainless steel substrates. The thin films were characterized in terms of their microstructure, crystal...
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The Characterization of Ground Raspberry Seeds and the Physiological Response to Supplementation in Hypertensive and Normotensive Rats
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Molecularly Imprinted Polymers for Stir Bar Sorptive Extraction: Synthesis, Characterization, and Application
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Synthesis and thermal characterization of luminescent hybrid composites based on bisphenol A diacrylate and NVP
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Synthesis and characterization of periphery-functionalized porphyrazines containing mixed pyrrolyl and pyridylmethylamino groups
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Synthesis, characterization, photochemical properties and cytotoxicity of the novel porphyrazine functionalized with nitroimidazolylbutylsulfanyl groups
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Structural and Pharmacological Characterization of Phenylalanine-Based AMPA Receptor Antagonists at Kainate Receptors
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Isolation and Characterization of NP-POL Nonapeptide for Possible Therapeutic Use in Parkinson’s Disease
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Characterization of a Unique Bordetella bronchiseptica vB_BbrP_BB8 Bacteriophage and Its Application as an Antibacterial Agent
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Rime samples characterization and comparison using classical and fuzzy principal components analysis
PublicationEfektywność dwóch nowych algorytmów w stosunku do klasycznego wariantu techniki PCA porównano analizując dane dotyczące zanieczyszczeń próbek sadzi zebranych na terenie trzech stacji w okresie 2004-2007. Zastosowane algorytmy FPCA-1 i FPCA-o pozwalają na wyodrębnienie większej liczby miejsc zbierania próbek i analitów w stosunku do sytuacji, kiedy stosuje się klasyczny wariant techniki PCA.
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Characterization of white cabbages from different cultivations by isothiocynates content and antioxidant activities
PublicationBadania epidemiologiczne wskazują, że wraz z zwiększeniem spożywania kapusty maleje ryzyko zachorowania na niektóre nowotwory. Mechanizmy przeciwrakotwórczego działania nie są do końca wyjaśnione, jednak wiele badań przeprowadzonych z wykorzystaniem zwierząt i ludzi sugeruje, że substancje występujące w tych roślinach, szczególnie izotiocyjaniany (ITC) modulują aktywność enzymów I i II fazy. Aktywność przeciwutleniająca jest innym...
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Optical and chemical characterization of thin TiNx films deposited by DC-magnetron sputtering
PublicationThin titanium nitride (tinx) films were deposited on silicon substrates by means of a reactive dc-magnetron plasma. Layers were synthesized under various conditions of discharge power and nitrogen flows in two operation modes of the magnetron (the so-called "balanced" and "unbalanced" modes). The optical constants of the tinx films were investigated by spectroscopic ellipsometry (se). X-ray photoelectron spectroscopy (xps) was...
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Preparation and characterization of silk fibroin/collagen sponge modified by chemical cross-linking
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Synthesis and Characterization of Nitrogen-doped Carbon Nanotubes Derived from g-C3N4
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Preparation and characterization of catalyst mix Fe-Co/MgO for carbon nanotubes growth
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Impedance characterization of the process of polyaniline first redox transformation after aniline electropolymerization
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Synthesis and characterization of modified silica gel as an intermediate in the generation of gaseous standard mixtures
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Synthesis and in vitro characterization of freeze-dried doxorubicin-loaded silica/PEG composite
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Morphologic, Phylogenetic and Chemical Characterization of a Brackish Colonial Picocyanobacterium (Coelosphaeriaceae) with Bioactive Properties
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Molecular Characterization of Growth Hormone-producing Tumors in the GC Rat Model of Acromegaly
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Characterization and properties of LDPE/(ground tire rubber)/crosslinked butyl rubber blends
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The FT-IR and Raman Spectroscopies as Tools for Biofilm Characterization Created by Cariogenic Streptococci
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Sythesis and Characterization of Optical Sol-Gel Adhesive for Military Protective Polycabonate Resin.Wytwarz
PublicationPrzedstawiono proces syntezy spoiw optycznych do laminatów poliwęglanowych. Scharakteryzowano właściwości optyczne i mechniczne. W procesie syntezy zastosowano monitoring ramanowski do diagnostyki przebiegu bazowych reakcji chemicznych.
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Starch-grafted-N-vinylformamide copolymers manufactured by reactive extrusion: synthesis and characterization
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Synthesis and characterization of crystalline Fe3O4 nanoparticles Synteza i charakterystyka nanokrystalicznego Fe3O4
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Cloning and characterization of the dnaK heat shock operon of the marine bacterium Vibrio harveyi
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Characterization of Mesorhizobium huakuii lipid A containing bothD-galacturonic acid and phosphate residues.
PublicationLipid A jest mieszaniną co najmniej 6 związków, różniących się stopniem fosforylacji i strukturą kwasów tłuszczowych przyłączonych do szkieletu polisacharydowego. Szkielet cukrowy zawiera beta(1'->6)połączone dwie cząsteczki 2,3-diamino-2,3-dideoksyglucosy (DAG)oraz aglikon kwas alfa-D-galaktouronowy.
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Preparation, characterization, and manufacturing of new polymeric materials for 3D printing for medical applications
PublicationThis work concerns the synthesis, formation, and characteristics of new filaments for 3D printing in FDM™/FFF technology for medical purposes. Two types of filaments were developed, i.e. degradable polyurethane and biodegradable polylactide-starch. The influence of the 3D printing process on selected filament properties was investigated. A detailed analysis of the filament formation process by the extrusion method was carried out,...