Search results for: CONCRETE ABSORPTION, CORROSION DENSITY, CORROSION RATE, LPR, SULFATES
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Metal-Organic Framework (MOF)/Epoxy Coatings: A Review
PublicationEpoxy coatings are developing fast in order to meet the requirements of advanced materials and systems. Progress in nanomaterial science and technology has opened a new era of engineering for tailoring the bulk and surface properties of organic coatings, e.g., adhesion to the substrate, anti-corrosion, mechanical, flame-retardant, and self-healing characteristics. Metal-organic frameworks (MOFs), a subclass of coordinative polymers...
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ANALIZA STANU TECHNICZNEGO RUROCIĄGÓW: WODY PRZeMYSŁOWEJ I SOLANKI
PublicationPracę wykonano na zlecenie Przedsiębiorstwa Badawczo-Wdrożeniowego "HYDRO-POMP" Sp. z o.o. ul. Wróblewskiego 19, 93-578 Łódź. Wykonawcą zlecenia jest Politechnika Gdańska, Wydział Chemiczny, Katedra Elektrochemii, Korozji i Inżynierii Materiałowej, 80-233 Gdańsk, ul. G. Narutowicza 11/12. Celem pracy była analiza stanu technicznego i badania dwóch rurociągów: solanki oraz wody przemysłowej. Badania wykonywano w warunkach terenowych...
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RESEARCH ON ORGANIC COATINGS DESIGNED FOR UNDERWATER APPLICATIONS
PublicationUnderwater steel structures require periodic maintenance. In the case of vessels, anti-corrosion works are carried out in the shipyard, where very good conditions for applying organic protective coatings can be provided. Very good surface preparation can be obtained by the use of abrasive blasting. The well-prepared metal surface is free from impurities (particularly inorganic salts). Suitable conditions for the application and...
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Evaluation of the current output of polymer anodes used in cathodic protection
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Some Aspects of Potential Measurements in a Stray Current Field
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Use of impedance spectroscopy to evaluate the durability of protective coatings after thermal shock
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Evaluation of the effect of ruthenium oxide on the properties of composite electrodes used in cathodic protection
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Accelerated ageing of organic coating systems by thermal treatment
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Diagnosis of reference electrodes in cathodic protection systems by electrochemical impedance spectroscopy
PublicationPrzedstawiono wyniki badań laboratoryjnych i terenowych przeprowadzonych techniką elektrochemicznej spektroskopii impedancyjnej (EIS). Zaprezentowano widma impedancyjne następujących układów: elektroda odniesienia/elektroda pomocnicza; rurociąg/zakopane i przenośne elektrody odniesienia. Pokazano, że omawiana technika umożliwia badanie stanu technicznego elektrod odniesienia, co zwiększa pewność wyników pomiarów potencjału chronionej...
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A new time-frequency detection method of stray current field interferenceon metal structures.
PublicationA new detection method has been presented of stray current field interference on underground metal structures. The method employs short time Fourier transformation (STFT). This method of analysis allows determination of signal spectral power density changes (e.g., structure potential) in the function of time. In the paper results have been presented of total time–frequency analysis of a pipeline potential in a stray current field...
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Method of sacrificial anode transistor-driving in cathodic protection system
PublicationA magnesium anode driving system has been proposed. A PNP driving transistor has been used. Electrochemical testing in 3%NaCl, results and comparison of the driving system and classic direct anode to cathode connection are presented. The driving system reduced the protection current and stabilized the working conditions of the anode. Higher anode efficiency was achieved. Overprotection and hydrogen embrittlement threats were prevented...
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Studies of the mechanism of metal metal dusting of 10CrMo9-10 steel after 10 years of operation in trhe semi-regenerative catalytic reformer
PublicationThe study showed that metal dusting mechanism of 10CrMo9-10 steel operated in industrial environment differs from models developed in laboratories. Significant differences lie in the fact that the models developed in laboratories only assume the formation of metastable carbide M3C, while studies have shown that the formation of M3C carbides is associated with the transformation of primary carbides and in the next stage is preceded...
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Method of sacrificial anode dual transistor-driving in stray current field
PublicationIn order to control a magnesium anode in a stray current interference field, a dual transistor driving system has been proposed. It consisted of a combination of PNP and NPN transistors. Dual transistor driven system and direct anode to cathode connection were electrochemically tested in 3% NaCl solution. The dual transistor driven system increased the anode efficiency and reduced hydrogen evolution and the risk of embrittlement....
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High-temperature kinetics study of 430L steel powder oxidized in air at 600–850 °C
PublicationThe 430L stainless steel powder with a mean particle size of 95 μm was studied to determine its high-temperature oxidation properties. Continuous thermogravimetric measurements were carried out for 100 h in air at temperatures in the range of 600–850 °C. Even though a considerable amount of Cr (up to ˜5 wt.% Cr) inside the grains was depleted – especially inside small grains – no breakaway oxidation was observed. This indicates...
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Inspection of protective linings using microwave spectroscopy combined with chemometric methods
PublicationOpisano nowa niedestrukcyjna metodę kontroli jakości nowych wykładzin ochronnych na podłożu metalowym oraz oceny ich stanu w trakcie eksploatacji przy zastosowaniu spektroskopii mikrofalowej w szerokim zakresie częstotliwości od 6,5 do 13 GHz. Uzyskane dane pomiarowe dodane zostały obróbce chemometrycznej w celu redukcji ilości danych doświadczalnych i wizualizacji rezultatów. Przedstawiono podstawy teoretyczne metody oraz wyniki...
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Improvement of electrochemical action of zinc-rich paints by addition of nanoparticulate zinc
PublicationThe influence of nanosized particles on electrochemical action of standard zinc-rich paints by means of SEM as well as potential and impedance measurements has been investigated. The motivation for doing this was to obtain additional electrical connection between the spherical microparticles themselves and zinc particles and steel substrate. Overall zinc content was at the level of 92% by weight. Samples with different concentration...
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Electrophoretic co-deposition of Fe2O3 and Mn1,5Co1,5O4: Processing and oxidation performance of Fe-doped Mn-Co coatings for solid oxide cell interconnects
PublicationThe “in-situ” Fe-doping of the manganese cobalt spinel was achieved by electrophoretic co-deposition of Mn1,5Co1,5O4 and Fe2O3 powders followed by a two-step reactive sintering treatment. The effects on the coating properties of two different Fe-doping levels (5 and 10 wt.% respectively) and two different temperatures of the reducing treatment (900 and 1000 °C) are discussed. Samples with Fe-doped coatings demonstrated a lower...
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Assessment of the application of CEM III with exposed aggregate as an alternative to CEM I for road pavements
PublicationThe article presents a results of study on the impact of replacing CEM I SR3/NA by CEMIII/A LH/HSR/NAon the mechanical properties and durability of pavement concrete with exposed aggregate. Was used granite aggregate and washed sand. Water/cement () ratio in the tested concretes constituted 0.35 and 0.4 and part of the cement was replaced with a 5% addition of natural pozzolana – zeolite. Compressive strength tests were performed...
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Examination of the epoxy coating system's resistance to Corrobill
PublicationThe tests of the influence of the surface cleaning agent on the epoxy coating were carried out. Electrochemical and corrosion tests were carried out. The effect of the preparation on the adhesion and hardness of the tested coating was tested.
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Conducting polymers for biodegradable metallic implants
PublicationNowadays permanent metallic cardiovascular stents are long-term implants. The long-time presence of such an implant in human body can cause overgrowth of tissue within the treated portion of the vessel, blockage of the circulatory system and many other clinical complications, such as thrombosis, prolonged physical irritations or chronic inflammation. Therefore, in recent years, there is an interest to create biodegradable metallic...
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Modelling of the Baumann turbine stage operation Part II. Free and kinetic vibrations
PublicationIn this paper has been presented a methodology of validation a novel mathematical model dedicated to evaluation and prediction of material degradation and demage of steam turbine elements such as blades, valves and pipes due to three mechanisms: stress-corosion, high-temperature creep and low-cyclic fatigue. The validation concept is based on an experimental setup manufactured in the Laboratory of Faculty of Mechanical and Power...
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The protective properties of graphene oxide coatings functionalized with phosphorus atoms.
PublicationRecently, electrophoretically deposited graphene oxide coatings are commonly applied as an anti-corrosion layer. However, improper adjustment of electrophoretic deposition (EPD) parameters as well as the hydrophilic nature of graphene oxide contribute to the formation of defects in the coatings and the increase in the wetting properties, respectively, and thus lead to a reduction of protective properties. The growth of wetting...
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Ultimate compressive strength assessment of uncleaned and cleaned corroded plates with locked crack
PublicationThe work presented here investigates the structural response of cleaned corroded plates, subjected to compressive load in the presence of a locked crack, where the change of mechanical properties as a result of corrosion development and the cleaning process is also accounted for. A Finite Element model for assessing the compressive strength, considering geometric and material nonlinearities, is developed, and the analysed plates...
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Application of galvanodynamic impedance spectroscopy for studying passive film cracking under mechanical strain
PublicationThe paper reports the results of simultaneous mechanical and electrochemical investigations on austenitic (18/8) stainless steel in a 2 % solution of sulphuric acid. The measurements were performed using Galvanodynamic Electrochemical Impedance Spectroscopy (GDEIS). Electrochemical analysis of mechanical passive layer cracking and repassivation conditions during a tensile test was carried out. Application of this methodology allowed...
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Ceria Based Protective Coatings for Steel Interconnects Prepared by Spray Pyrolysis
PublicationStainless steels can be used in solid oxide fuel/electrolysis stacks as interconnects. For successful long term operation they require protective coatings, that lower the corrosion rate and block chemical reactions between the interconnect and adjacent layers of the oxygen or the hydrogen electrode. One of the promising coating materials for the hydrogen side is ceria. Using standard sintering techniques, ceria sinters at around...
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SEM micrographs of the topography of Cu-Sn-TiO2 nanocomposite coatings
Open Research DataThe dataset contains the scanning electron microscopy (SEM) micrographs of nanocomposite Cu-Sn-TiO2 coatings electrodeposited from oxalic acid bath containing Cu and Sn salts as well as TiO2 nanoparticles under various treatments: mechanical stirring, ultrasonic or none. The details of the electrodeposition process are presented in the readme file attached...
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MATERIAŁY I ELEMENTY STOSOWANE DO WYKONANIA LEKKIEJ OBUDOWY cz. 1. Materiały metalowe
PublicationW artykule przedstawiono stosowane w lekkich obudowach materiały metalowe i kształtowane z nich wyroby. Omówiono charakterystyczne parametry i różnice technologiczne występujące w produkcji wyrobów. Przedstawiono ocenę odporności korozyjnej materiałów.
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Multicomponent layers for aluminium alloys surface consolidation
PublicationThe main reason of the surface modification of the components such as pistons and cylinder blocks made of cast aluminium alloys is to obtain high hardness, wear and corrosion resistance of the working surface for larger lifetime of the motor-car and aircraft engines. In that aspect, the new conception of development - by hybrid method - of surface layers containing manganese, nitrogen, sulphur (Mn-N-S) and manganese, nitrogen,...
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Effects of solution composition and electrophoretic deposition voltage on various properties of nanohydroxyapatite coatings on the Ti13Zr13Nb alloy
PublicationThe purpose of the research was to establish the influence of the solution composition and the electrophoretic deposition voltage on the coating homogeneity and thickness, nanohardness, adhesion, corrosion resistance and wettability. The Ti13Zr13Nb alloy was coated by the electrophoretic technique with hydroxyapatite in a solution containing 0.1, 0.2 or 0.5 g nanoHAp in 100 mL of suspension and at voltage 15, 30 or 50 V. The scanning...
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Mechanical characteristics of welded joints between different stainless steels grades
Publicationnvestigation of mechanical characteristics of welded joints is one of the most important tasks that allow determining their functional properties. Due to the very high, still rising, cost of some stainless steels it is justified, on economic grounds, welding austenitic stainless steel with steels that are corrosion-resistant like duplex ones. According to forecasts the price of...
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The AFM micrographs and impedance study of epoxy coatings after exposure in corrosive media
Open Research DataThe dataset contains Atomic Force Microscopy (AFM) images and local impedance measurements of epoxy organic coating used as anti-corrosion protection, before and after 2-month exposure to sodium chloride solution. Additionally, there two local impedance spectra recorded after the coating exposure. The first one was recorded on intact coating surface,...
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Failure of austenitic stainless steel tubes during steam generator operation
PublicationThe article presents the failure process of austenitic stainless steels used in power devices, such as heat exchangers, steam generators, in terms of local corrosion: pitting, stress and intergranular corrosion, paying particular attention to welded joints area. The effect of steel chemical composition, microstructure, welding process and work environment was analyzed. The second part of the article presents the results of the...
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Electrophoretic deposition and characterization of composite chitosan/Eudragit E 100 or poly(4-vinylpyridine)/mesoporous bioactive glass nanoparticles coatings on pre-treated titanium for implant applications
PublicationTitanium implants are surface-modified to achieve bioactivity and often antibacterial properties. Such surface coatings may increase corrosion degradation and be weakly attached to the substrate. In the present research, biodegradable composite coatings, investigated so far as smart environment-sensitive, slowly releasing silver to the implant neighborhood, were produced as a combination of chitosan (CS) with Eudragit E 100 (EE100)...
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Straightening of ship hull structure made of 316L stainless steel - tensile test of water cooled materia
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - tensile test of reference material materia (transverse direction)
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - tensile test of reference material materia (longitudinal direction)
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - microstructure of naturally colled material
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - microstructure of water cooled material
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - microstructure of reference material
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Straightening of ship hull structure made of 316L stainless steel - tensile test of naturally cooled material
Open Research DataThe AISI 316L type steel belongs to the group of chromium-nickel stainless steels. They are determined according to European standards as X2CrNiMo17-12-2 and belong to the group of austenitic stainless steels. Steels of this group are used for elements working in seawater environments, for installations in the chemical, paper, and food, industries,...
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Mrówczan sodu z nowym pakietem inhibitorów korozji jako ekologiczny środek do odladzania infrastruktury lotniczej.
PublicationPrzedstawiono wyniki badań korozji kadmowej powłoki na stali oraz korozji po zanurzeniu stopów metali w mrówczanie sodu z nowym pakietem inhibitorów korozji, zawierającym synergiczną kompozycję poliasparaginianu sodu oraz imidazolu. Ponadto wyznaczono zdolność penetracji lodu przez badany układ. Właściwo- ści opracowanej kompozycji odladzającej porównano z właściwościami środków dostępnych na rynku. Uzyskane wyniki wskazują, że otrzymany...
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Underwater Electrochemical Offshore Tests of a Paint Coating Applied in Water on the Legs of an Oil Production Platform
PublicationThis paper presents the methodology developed for underwater measurements using electrochemical impedance spectroscopy (EIS) technique, aimed at determining the resistance of an epoxy coating applied in seawater to the legs of an oil production platform. Performing such underwater tests in an offshore environment was technically challenging. The results of measurements obtained on the platform were confronted with comparative results...
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Properties of nano-Fe3O4 incorporated epoxy coatings from Cure Index perspective
PublicationThe mission of an advanced epoxy-based nanocomposite coating is to provide a given substrate with protection against an unwelcome guest; e.g. corrosive molecules/media, environmental stress, flame, thermal degradation or microorganisms. In such systems, the degree to which superior properties can be guaranteed depends on the state of network formation in the epoxy in the presence of nanoparticles. For low-filled epoxy nanocomposite coatings,...
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Effect of slag coal ash and foamed glass on the mechanical properties of two-stage concrete
PublicationTwo-stage concrete (TSC) is known by various names such as colcrete, Polcrete, preplaced aggregate concrete and prepacked concrete. It is different from traditional concrete in two fundamental ways, namely method of construction and mix proportion. Two-stage concrete (TSC) is defined as firstly, coarse aggregates are placed into the formwork and grout is applied to fill in the between coarse aggregate particles voids. Secondly,...
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TG and DTG profiles for plastics: LDPE, HDPE, PP, PD and PET
Open Research DataThe dataset includes:
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Strontium-based nanosized phosphates as anticorrosive fi llers of epoxy and polyurethane coating compositions
PublicationAnticorrosive epoxy and polyurethane coatings were compounded using zinc-free nanosized phosphates of strontium (SP) or strontium and aluminum (SAP). For comparison, a nanosized calcium aluminum ammonium phosphate (CAP) and a microsized zinc phosphate (ZP) were tested. Results of salts spray and cyclic corrosion tests revealed better anticorrosive properties of the SAP-based coatings...
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Numerical assessment of ultimate strength of severe corroded stiffened plates
PublicationThe objective of this work is to investigate numerically (using the non-linear FEM and the approach stipulated by the Common Structural Rules) the severe nonuniform corrosion degradation effect on the ultimate strength of stiffened plates and compare the results to the already published experimental works. Different factors governing structural behavior of corroded stiffened plates are investigated, such as corrosion degradation level,...
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Manganese Phosphatizing Coatings: The Effects of Preparation Conditions on Surface Properties
PublicationManganese phosphate coating could be used to protect the surface of steel products. However, it is essential to determine the effects which process parameters, as well as the types of additives used, have on the efficiency of coating deposition. Thus, we present here a process of phosphatization of low-alloy steel (for 15 min at 95 ◦C) in manganese/nickel baths followed by a passivation process with the use of a silicon and zircon...
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Time evolution of Electrochemical Impedance spectra of cathodically protected steel in artificial seawater
PublicationUsability of Electrochemical Impedance Spectroscopy data for better cathodic protection control was investigated. Carbon steel – S235JR2 grade specimen were exposed in artificial seawater environment. Samples were polarized and their potentials corresponded to four different cathodic protection degrees. Time evolution of Electrochemical Impedance spectra was investigated. Goodness of fit function (X2) was analysed in terms of proper...
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Production and Properties of the Porous Layer Obtained by the Electrochemical Method on the Surface of Austenitic Steel
Publication: The growing demand for implants has seen increasing interest in the introduction of new technologies and surface modification methods of metal biomaterials. This research aimed to produce and characterize a porous layer grown on austenitic stainless steel 316L, obtained via the anodization process near the micro-arc oxidation, i.e., low voltage micro-arc oxidation (LVMAO). The discussed layer significantly influences the properties...