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Search results for: PHASE CHANGE MATERIAL
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How Do Intermolecular Interactions Evolve at the Nematic to Twist–Bent Phase Transition?
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Phase diagram of P3HT:PC70BM thin films based on variable-temperature spectroscopic ellipsometry
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Anomalous Thermal Behavior of Salicylsalicylic Acid and Evidence for a Monotropic Transition to a Nematic Phase
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The existence and gas phase acidity of the HAlnF3n+1 superacids (n=1–4)
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A new method for preparation of rutile phase titania photoactive under visible light
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Volatile organic compound separation from gas phase using ionic liquids
PublicationZanieczyszczenie powietrza lotnymi związkami organicznymi staje się światowym problemem ochrony środowiska w związku z ich toksycznymi właściwościami. W związku z tym poszukuje się nowych, efektywnych technologii oczyszczania strumieni gazowych. Powszechnie stosowaną metodą jest utlenianie termiczne. Wiąże się ono jednak z Wysokiem zużyciem energii i efektami ubocznymi w postaci emisji dwutlenku węgla i tlenków azotu. Alternatywą...
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Solid phase synthesis and biological activity of linear tuftsin and retro-tuftsin derivatives
PublicationPrzedstawiono syntezę na fazie stałej nowych pochodnych tuftsyny i retro-tuftsyny i ich mikrobiologiczne właściwości. Otrzymane pochodne zawierały wiązanie izopeptydowe między epsilon-aminową grupą lizyny a takimi aminokwasami jak: Ala, beta-Ala, Val, Ile, Gly.
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Solid phase synthesis of conjugates of tuftsin analogues with 1-nitro-acridine derivatives
PublicationZsyntetyzowano na fazie stałej koniugaty 1-nitro-akrydyny z pochodnymi tuftsyny modyfikowanymi na grupie epsilon-aminowej lizyny prostymi aminokwasami, np. alaniną, valiną, beta-alaniną. Końcowe produkty były charakteryzowane za pomocą MS, NMR, analizy elementarnej i przekazane do badań ich aktywności przeciwnowotworowej.
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Effect of structure modification with potassium on grains layer creation process and phase transitions
PublicationZbadano szkła germanianowo-ołowiowe i krzemianowo bizutowe. Wartwy metalicznych granul wytwarzano w nich poprzez redukcję powierzchni w atmosferze wodoru. Praca dotyczy wpływu potasu na tworzenie się warstwy granul oraz na procesy topnienia i krzepnięcia granul w trakcie obróbki termicznej.
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Application of stereology for two-phase flow structure validation in fluidized bed reactors
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Numerical calculation of three-phase transformer's residual flux in ATP and PSpice programs.
PublicationW artykule przedstawiono analizę przebiegów prądu i strumienia magnetycznego podczas wyłączania transformatora energetycznego, wykonaną w celu określenia strumieni szczątkowych. Wykorzystano do tego celu modele obwodowe zbudowane w oparciu o programy symulacyjne ATP (Alternative Transients Program) i PSpice. Wyniki obliczeń okazały się bardzo zbliżone dla obu modeli. Przy ich wykorzystaniu obliczono strumienie szczątkowe w kolumnach...
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublicationOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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Preliminary investigations on biological treatment of aqueous phase separated from cutting fluids
PublicationZaprezentowano wyniki fizykochemicznego podczyszczania przepracowanych cieczy obróbkowych pochodzących z różnych źródeł. Emulsje przepracowanych cieczy obróbkowych zostały rozdzielone na fazę organiczną i wodną z wykorzystaniem różnych koagulantów. Wydzielona faza wodna została następnie poddana biologicznemu oczyszczaniu z wykorzystaniem osadu czynnego. W wyniku oczyszczania ścieków uzyskano 59-88% obniżenie wartości ChZT.
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Influence of Firing Temperature on Phase Composition and Color Properties of Ceramic Tile Bodies
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Effect of brookite on the photocatalytic properties of mixed-phase TiO2 obtained at a higher temperature
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How Does International Competitiveness Affect Economic Development? A Two-Phase Hypothesis
PublicationThis paper analyses the impact of international competitiveness on economic development, based on the World Economic Forum Global Competitiveness Index (GCI) and GDP/capita of 125 countries during the period 2007-2010. The results reveal two phases of the evolution of competitiveness. When GCI < 4.5 (on 1-7 scale), any improvement of a country’s competitiveness affects current development more than future development. When...
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In-situ odd random phase electrochemical impedance spectroscopy study on the electropolymerization of pyrrole on iron in the presence of sodium salicylate – The influence of the monomer concentration
PublicationIn this work, the potentiostatic electropolymerization of polypyrrole (PPy) on iron in aqueous solution of sodium salicylate and pyrrole is studied in situ by odd random phase electrochemical impedance spectroscopy (ORP-EIS). The influence of the pyrrole concentration on the electrosynthesis process is investigated. The ORP-EIS technique ensures a reliable analysis of the PPy electrosynthesis on iron by means of an advanced data...
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Fabrication and photoactivity of ionic liquid–TiO2 structures for efficient visible-light-induced photocatalytic decomposition of organic pollutants in aqueous phase
PublicationTo investigate the effect of the ionic liquid (IL) chain length on the surface properties and photoactivity of TiO2, a series of TiO2 microspheres have been synthesized via a solvothermal method assisted by 1-methyl-3-octadecylimidazolium chloride ([ODMIM][Cl]) and 1-methyl-3-tetradecylimidazolium chloride ([TDMIM][Cl]). All as-prepared samples were characterized by X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy...
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Ionogel fibres of bis(trifluoromethanesulfonyl)imide anion-based ionic liquids for the headspace solid-phase microextraction of chlorinated organic pollutants
PublicationIonogels, a family of hybrid materials in which ionic liquids (ILs) are confined in a sol–gel network, are receiving much attention in a variety of scientific and technological fields. In this work, ionogels derived from three different ILs based on the anion bis(trifluoromethanesulfonyl)imide (TFSI), namely 1-butyl- 3-methylpyridinium bis(trifluoromethanesulfonyl)imide ([C4C1Py][TFSI]), 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesulfonyl)imide...
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Electrochemically Obtained TiO2/CuxOy Nanotube Arrays Presenting a Photocatalytic Response in Processes of Pollutants Degradation and Bacteria Inactivation in Aqueous Phase
PublicationTiO2/CuxOy nanotube (NT) arrays were synthesized using the anodization method in the presence of ethylene glycol and different parameters applied. The presence, morphology, and chemical character of the obtained structures was characterized using a variety of methods—SEM (scanning electron microscopy), XPS (X-ray photoelectron spectroscopy), XRD (X-ray crystallography), PL (photoluminescence), and EDX (energy-dispersive X-ray spectroscopy)....
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Measurement of the temperature change of PVCP tissue phantom illuminated by dermatological laser 1.series
Open Research DataApplication of laboratory set-up for characterization of thermal properties of optical tissue phantoms during laser irradiation is presented. The produced system utilizes a thermographic camera VIGOcam v50 and a dermatological laser system with a 975 nm diode laser module. The set-up was used to perform measurements of the temporal and spatial temperature...
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Optimization of vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction for quantification of niclosamide in real samples
PublicationIn this manuscript, a green and fast vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction (VA-HMDES-DLPME) method was developed for the selective extraction and determination of niclosamide in read samples, including rice, medicine tablets, and water samples. Here, hydrophobic magnetic deep eutectic solvents were used as the extracting solvent without requiring any centrifugation...
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Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)
PublicationThe paper presents a novel pine bark based biosorbent for solid-phase extraction (SPE). The morphology and composition of the pine bark were characterized using Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The biosorbent was used for the preparation of wastewater for the determination of phenylbutazone, sulfamethazine, carbendazim, and linuron by high performance liquid chromatography with...
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West 86th-A Journal of Decorative Arts Design History and Material Culture
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublicationBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Modelling hydraulic and capillary-driven two-phase fluid flow in unsaturated concretes at the meso-scale with a unique coupled DEM-CFD technique
PublicationThe goal of the research was to demonstrate the impact of thin porous interfacial transition zones (ITZs) between aggregates and cement matrix on fluid flow in unsaturated concrete caused by hydraulic/capillary pressure. To demonstrate this impact, a novel coupled approach to simulate the two-phase (water and moist air) flow of hydraulically and capillary-driven fluid in unsaturated concrete was developed. By merging the discrete...
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Complex modulus of Cement Bitumen Treated Material Mixture C3E4 cores obtained from the field section (28-365 days of curing at the field and later in laboratory at 20C)
Open Research DataDataset presents data of complex modulus determined for cold recycled mixture – cement bitumen treated material mixture with following binding agents: 3% cement, 4% emulsion (C3E4). Mixture was designed according to Polish requirements for the base course of pavement. Specimen were obtained from the field at 28, 180, 270 and 365 days after compaction....
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The Opoka-Rock from the Mesozoic/Neogene Contact Zone in the Bełchatów Lignite Deposit – Characteristics of a Petrographic Nature and as a Raw Material
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Toward mechanosynthesis of diamondoid structures: V. Silicon as the material of choice for preliminary implementation of intermediate generation of nano-machine systems
PublicationStosując ostatnio wprowadzony przez Drexlera ''moduł skalowany stałą sieciową'' KLM, porównano dwa potencjalne nano-materiały, krzem i diament. Szczegółowe porównanie właściwości fizycznych i chemicznych wykazuje, że krzem może być rozważany jako materiał z wyboru dla pierwotnej implementacji pośredniej generacji nano-systemów.
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Synthesis, Characterization, and Catalytic Applications of the Ti-SBA-16 Porous Material in the Selective and Green Isomerizations of Limonene and S-Carvone
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Exploring the Relationship between Particulate Matter Emission and the Construction Material of Road Surface: Case Study of Highways and Motorways in Poland
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Immobilization of TiO2 and Fe–C–TiO2 photocatalysts on the cotton material for application in a flow photocatalytic reactor for decomposition of phenol in water
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Finite element modeling of plastic hinges based on ductility demand-capacity method using nonlinear material for dynamic analysis
PublicationThe article discusses modeling plastic hinges in reinforced concrete interme-diate supports using finite elements methods. The ductility demand-capacitymethod was used to determine the geometrical parameters of cross-section plas-ticization zones, their ability to move and rotate, as well as their ductility. Dueto the varied geometry and stiffness of the supports and their nonlinear behav-ior under dynamic load, this method was...
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Structural and Material Determinants Influencing the Behavior of Porous Ti and Its Alloys Made by Additive Manufacturing Techniques for Biomedical Applications
PublicationOne of the biggest challenges in tissue engineering is the manufacturing of porous structures that are customized in size and shape and that mimic natural bone structure. Additive manufacturing is known as a sufficient method to produce 3D porous structures used as bone substitutes in large segmental bone defects. The literature indicates that the mechanical and biological properties of scaffolds highly depend on geometrical features...
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Quantitative determination of processed waste expanded perlite performance as a supplementary cementitious material in low emission blended cement composites
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Finite element investigations of granular material behaviour during cyclic wall shearing under a constant normal stiffness condition
PublicationW artykule przedstawiono wyniki numnerycznej analizy zachowania sie materiałów granulowanych podczas cyklicznego ścinanai wzdłuz szorstkiej ściany z warunkiem stałej sztywności normalnej. Obliczenia wykonano przy zastosowaniu metody elementów skończonych i mikropolarnego nodelu hipopalstycznego. Obliczenia wykonano dla róznych sztywności, początkowych wskaźników porowatości i sredniej średnicy ziarna. Wyniki numeryczne porównano...
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Modelling of full-scale silo experiments with flow correcting inserts using material point method (MPM) based on hypoplasticity.
PublicationCharakterystyki przepływu materiałów sypkich w silosach mają znaczenie dla naporów wywieranych na ściany silosu. Można je zmieniać za pomocą różnych wkładek. W pracy omówiono wyniki liczbowe dotyczące ograniczonego przepływu niespoistego ziarnistego piasku w pełnowymiarowym silosie metalowym z różnymi symetrycznie rozmieszczonymi wkładami, służącymi do korekcji wzorca przepływu (podwójny stożek, stożek w stożku i odwrócony stożek)....
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Comparison of XPS spectra of Ag3d for silver nanostructures and bulk material
Open Research DataAg nanostructures were prepared on borosilicate glass (Corning 1737F) and Si substrates. In both cases, the substrateswere cleaned with acetylacetone and then rinsed in ethanol. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The...
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Solid phase microextraction–comprehensive twodimensional gas chromatography–time-of-flight mass spectrometry: a new tool for determining PAHs in airport runoff water samples
Publicationfundamental aspect of airport operations is the pollution caused by airport runoff waters. Polycyclic aromatic hydrocarbons (PAHs) are one of the most important groups of xenobiotics which are commonly found in runoff water originating from airports. Only very limited data on the analysis of airport runoff water have been published until now. Therefore, a reliable and accurate analytical method based on headspace solid-phase microextraction...
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Rapid and Green Separation of Mono- and Diesters of Monochloropropanediols by Ultrahigh Performance Supercritical Fluid Chromatography–Mass Spectrometry Using Neat Carbon Dioxide as a Mobile Phase
PublicationThis study demonstrates the effect of column selectivity and density of supercritical carbon dioxide (SC-CO2) on the separation of monochloropropanediol (MCPD) esters, known as food toxicants, using SC-CO2 without addition of cosolvent in ultrahigh performance supercritical fluid chromatography–mass spectrometry (UHPSFC-MS). This study shows that over 20 2-monochloropropanediol (2-MCPD) and 3-monochloropropanediol (3-MCPD) mono-...
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Deflection measurement of field section with pavement with base course made of Cement Bitumen Treated Material Mixture C3E4 (28, 180, 270, 365 days after compaction)
Open Research DataDataset presents data of deflections determined for pavement with base course made of cold recycled mixture – cement bitumen treated material mixture with following binding agents: 3% cement, 4% emulsion (C3E4). Mixture was designed according to Polish requirements for the base course of pavement. Mixture was mixed in stationary plant and compacted...
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Structural phase transitions and photoluminescence properties of oxonitridosilicate phosphors under high hydrostatic pressure
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Development and validation of urinary nucleosides and creatinine assay by capillary electrophoresis with solid phase extraction
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Headspace Liquid-Phase Microextraction of Chlorobenzenes in Soil with Gas Chromatography-Electron Capture Detection
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Solid Phase Photocatalytic Reaction on the Soot/TiO2 Interface: The Role of Migrating OH Radicals
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Matrix Metalloproteinase-9 Is Required for Hippocampal Late-Phase Long-Term Potentiation and Memory
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Comparison the Accuracy of the Extrapolation Methods of the Time Phase Coincidence in Synchronization of Power Generating Units
PublicationW artykule opisano metody ekstrapolacji chwili zgodności fazowej napięć łączonych obiektów elektroenergetycznych. Przeprowadzono analizę porównawczą wybranych metod ekstrapolacji w równych warunkach pracy oraz przedstawiono najistotniejsze wyniki badań.
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Assessment of phase stability and in vitro biological properties of hydroxyapatite coatings composed of hexagonal rods
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pH Gradient as a Tool for the Separation of Ionizable Analytes in Reversed-Phase High-Performance Chromatography
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STUDYING THE PROCESS OF OBTAINING PHOSPHATES OF METALS BASED ON THE PHASE EQUILIBRIA OF FOUR COMPONENT SYSTEMS
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