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Search results for: mikroskopia elektronowa (sem)
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Effect of Semiconductor Element Substitution on the Electric Properties of Barium Titanate Ceramics
PublicationThe investigated ceramics were prepared by a solid-state reaction from simple oxides and carbonates with the use of a mixed oxide method (MOM). The morphology of BaTi0.96Si0.04O3 (BTSi04) ceramics was characterised by means of a scanning electron microscopy (SEM). It was found that Si+4 ion substitution supported the grain growth process in BT-based ceramics. The EDS results confirmed the high purity and expected quantitative composition...
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Highly Active TiO2 Microspheres Formation in the Presence of Ethylammonium Nitrate Ionic Liquid
PublicationSpherical microparticles of TiO2 were synthesized by the ionic liquid-assisted solvothermal method at different reaction times (3, 6, 12, and 24 h). The properties of the prepared photocatalysts were investigated by means of UV-VIS diffuse-reflectance spectroscopy (DRS), Brunauer–Emmett–Teller (BET) surface area measurements, scanning electron microscopy (SEM), X-ray diffraction analysis (XRD), and X-ray photoelectron spectroscopy...
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New ceramic materials derived from pyrolyzed poly(1,2-dimethylsilazane) and starch as a potential anode for Li-ion batteries
PublicationNewmaterialswere obtained by pyrolysis of starch (S) and poly(1,2-dimethylsilazane) (PSN) (weight ratio: PSN/S 30/70) at temperature a) 500 °C, b) 700 °C and c) 900 °C. Ceramic materials were characterized by infrared spectroscopy, TGA, Raman spectroscopy and SEM. New Si\O and shifted Si\C stretching vibration modes emerged confirming direct interaction between silicon originating fromsilazane and oxygen coming fromstarch. The...
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Novel Functionalization of Boron-Doped Diamond by Microwave Pulsed-Plasma Polymerized Allylamine Film
PublicationWe report the novel modification of a hydrogen-terminated polycrystalline boron-doped electrode with a microwave pulsed-plasma polymerized allylamine. Boron-doped diamond (BDD) was coated with a very thin layer of adherent cross-linked, pinhole- and additive-free allylamine plasma polymer (PPAAm) resistant to hydrolysis and delamination and characterized by a high density of positively charged amino groups. The pulsed microwave...
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Advantageous conditions of saccharification of lignocellulosic biomass for biofuels generation via fermentation processes
PublicationProcessing of lignocellulosic biomass includes four major unit operations: pre-treatment, hydrolysis, fermentation and product purifcation prior to biofuel generation via anaerobic digestion. The microorganisms involved in the fermentation metabolize only simple molecules, i.e., monosugars which can be obtained by carrying out the degradation of complex polymers, the main component of lignocellulosic biomass. The object of this...
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Laser-assisted modification of titanium dioxide nanotubes in a tilted mode as surface modification and patterning strategy
PublicationElectrochemical anodization is regarded as a facile and easily scalable fabrication method of titania nanotubes (TiO2NTs). However, due to the extended duration of calcination and further modifications, much faster alternatives are highly required. As a response to growing interest in laser modification of nanotube arrays, a comprehensive investigation of pulsed-laser irradiation and its effect onto TiO2NT properties has been carried out....
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In Vitro Biological Characterization of Silver-Doped Anodic Oxide Coating on Titanium
PublicationDespite the high biocompatibility and clinical effectiveness of Ti-based implants, surface functionalization (with complex osteointegrative/antibacterial strategies) is still required. To enhance the dental implant surface and to provide additional osteoinductive and antibacterial properties, plasma electrolytic oxidation of a pure Ti was performed using a nitrilotriacetic acid (NTA)-based Ag nanoparticles (AgNP)-loaded calcium–phosphate...
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Laser-assisted approach for improved performance of Au-Ti based glucose sensing electrodes
PublicationThis paper focuses on the synthesis route and electrochemical properties of electrocatalytic material based on gold nanoparticles (NPs) embedded in a structured titanium template obtained via optimized anodization, chemical etching and laser processing. SEM inspection reveals the presence of Au NPs (60–90 nm in diameter) sited in the titanium foil cavities. Performed electrochemical measurements enable nomination of the set of working...
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AutoCAD: Examination of Factors Influencing User Adoption
PublicationThe primary purpose of the research is to examine and validate determinants of user intention to use AutoCAD software, utilising the constructs from prior studies in a more integrated model. The paper proposes a revised Technology Acceptance Model (TAM) for measuring the adoption of AutoCAD. In the study, a latent construct PPA (perceived physical accessibility) was added to the proposed research model as a new determinant of AutoCAD...
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High-temperature Corrosion of ~ 30 Pct Porous FeCr Stainless Steels in Air: Long-Term Evaluation Up to Breakaway
PublicationIn this work, a long-term (up to 6000 hours) corrosion evaluation of three porous (~ 30 pct of initial porosity) ferritic iron-chromium alloys with different Cr contents (20, 22, and 27 wt pct of Cr) was carried out at 600 C, 700 C, 800 C, and 900 C in air. Mass gain measurements and SEM analyses revealed that at temperatures above 600 C, all alloys exhibit breakaway corrosion, whereas at 600 C, none of the alloys were heavily...
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Photocatalytic decolourization of Rhodamine-B dye by visible light active ZIF-8/BiFeO3 composite
PublicationIn this work, preparation of ZIF-8 supported BiFeO3 photocatalyst by ultrasound cavitation technique was reported. The synthesized materials were characterized using solid UV absorption spectroscopy, Raman Spectroscopy, and SEM. The catalytic function of synthesized photocatalyst under ultraviolet and visible light was examined for the decolourization of Rhodamine-B (Rh-B) dye. To understand the action of the photocatalyst on Rh-B...
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Role of size scale of ZnO nanoparticles and microparticles on toxicity toward bacteria and osteoblast cancer cells
PublicationThe specific role of size scale, surface capping, and aspect ratio of zinc oxide (ZnO) particles on toxicity toward prokaryotic and eukaryotic cells was investigated. ZnO nano and microparticles of controlled size and mor- phology were synthesized by wet chemical methods. Cytotoxicity toward mammalian cells was studied using a human osteoblast cancer cell line and antibacterial activity using Gram-negative bacteria (Escherichia...
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Tuning of eg electron occupancy of MnCo2O4 spinel for oxygen evolution reaction by partial substitution of Co by Fe at octahedral sites
PublicationTo study the effect of partial Co substitution by Fe in the B site of MnCo2O4 spinel on its physicochemical and electrochemical properties, a series of MnCo2-xFexO4 powders (x=0.125; 0.250; 0.500; 0.750; 1.000) were synthesized by means of the sol-gel method. The produced powders were characterized by powder X ray diffraction (pXRD), scanning and transmission electron microscopy (SEM & TEM) coupled with energy dispersive spectroscopy...
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Studies on the Combined Impact of Starch Source and Multiple Processing on Selected Properties of Thermoplastic Starch/Ethylene-Vinyl Acetate Blends
PublicationThermoplastic starch (TPS)/ethylene vinyl acetate (EVA) blends compatibilized with polyethylene-graft-maleic anhydride (PE-g-MA) were prepared from various native starches (potato, maize and waxy maize) and subjected to multiple extrusion cycles. Source of starch has significant impact on its composition, hence properties of obtained TPS and their blends with EVA. Higher content of amylopectin in waxy maize starch, comparing to...
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Experimental tuning of AuAg nanoalloy plasmon resonances assisted by machine learning method
PublicationPlasmonic nanostructures based on AuAg nanoalloys were fabricated by thermal annealing of metallic films in an argon atmosphere. The nanoalloys were chosen because they can extend the wavelength range in which plasmon resonance occurs and thus allow the design of plasmonic platforms with the desired parameters. The influence of initial fabrication parameters and experimental conditions on the formation of nanostructures was investigated....
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The Physicochemical and Antibacterial Properties of Chitosan-Based Materials Modified with Phenolic Acids Irradiated by UVC Light
PublicationThis paper concerns the physicochemical properties of chitosan/phenolic acid thin films irradiated by ultraviolet radiation with wavelengths between 200 and 290 nm (UVC) light. We investigated the preparation and characterization of thin films based on chitosan (CTS) with tannic (TA), caffeic (CA) and ferulic acid (FA) addition as potential food‐packaging materials. Such materials were then exposed to the UVC light (254 nm) for...
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Enhanced photocatalytic properties of lanthanide-TiO2 nanotubes: An experimental and theoretical study
PublicationA series of Er-, Yb-, Ho-, Tb-, Gd-, Pr-TiO2 nanotubes (RE-NTs) was prepared via an electrochemical method. The as-prepared photocatalysts were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), UV–vis absorption, scanning electron microscopy (SEM) and luminescent spectroscopy. The experiments demonstrated that toluene in the gas phase was successfully degraded under visible light (LEDs λmax = 465...
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Placement niestacjonarne II stopień Elektrotechnika 2 sem.
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WCh, II st, 2 sem, 21/22z
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Inżynieria Biomedyczna V sem (WETI + WFTiMS + WCH)
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Psychologia transportowa - Transport, sem. V - 2022/23
e-Learning CoursesKurs przeznaczony dla studentów V semestru kierunku Transport.
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Placement II stopień Inżynieria Środowiska 3 sem.
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Inorganic Chemistry, GT 2 sem 2021/2022
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Chemia fizyczna - ćwiczenia - sem. IIICh - 23/24
e-Learning CoursesKurs obejmuje materiał pierwszego semestru ćwiczeń do przedmiotu Chemia Fizyczna dla studentów kierunku studiów Chemia (I stopień, semestr III) na Wydziale Chemicznym w postaci prezentacji oraz umożliwia kontakt z prowadzącym za pomocą czatu. Materiał obejmuje dwa bloki zagadnień: (I) Termodynamika i termochemia oraz (II) Równowagi fazowe i chemiczne. Prowadzący: dr hab. inż. Piotr Bruździak, prof. PG
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Chemia Budow. (niestac. II sem) 21/22
e-Learning CoursesMateriały do wykładu z przedmiotu Chemia dla studentów kierunku Budownictwo (studia I stopnia) semestru II (semestr letni). Tematyka kursu obejmuje podstawowe zagadnienia z chemii ogólnej, jak również specjalistyczne zagadnienia z zakresu chemii budowlanej, w tym: - podstawy chemii kwantowej, - reakcje chemiczne (stechiometria, podstawy termodynamiki i kinetyki reakcji), - fizykochemia wody, - roztwory wodne (stężenia,...
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SAOZ - Projekt Architektoniczny sem. II (2020/21)
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Placement II stopień Inż. Materiałowa 1 sem.
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Chemia budowlana [ćwiczenia] I sem, Budownictwo [stac]
e-Learning CoursesKurs chemia budowlana [ĆWICZENIA] dedykowany jest dla kierunku Budownictwo i jest on obowiązkowy dla studentów I-szego semestru. W czasie kursu studenci będą mieli okazję rozwiązywać zadania problemowe i obliczeniowe z zakresu chemii ogólnej i budowlanej. Przykłady zadań obliczeniowych bezpośrednio związanych z budownictwem przybliżą studentom praktyczne zastosowanie chemii w tej dziedzinie. Przedmiot realizowany jest w Katedrze...
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Makroekonomia Analityka Gospodarcza, sem.2 lato 2023
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Techniki obrazowania medycznego - sem. leti 2022/23
e-Learning CoursesI stopień IBio
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Drogi Szynowe - sem VI - Wykład 22/23
e-Learning CoursesCelem przedmiotu jest przedstawienie konstrukcji dróg szynowych, charakterystyki elementów nawierzchni szynowej oraz omówienie zagadnień (podstawowych) związanych z projektowaniem układów torowych (linie kolejowe, szynowy transport miejski), utrzymaniem dróg szynowych i inżynierią ruchu kolejowego
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Technika cyfrowa - laboratorium 2022/2023 sem. letni.
e-Learning CoursesKurs wspomagający prowadzenie zajęć z przedmiotu "Technika Cyfrowa - Laboratorium".
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Chemia Bud III sem (B2) D. Zalewska3
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PROJEKT KONSERWATORSKI II | SEM. LETNI 2021/22
e-Learning CoursesZadaniem kursu projektowania konserwatorskiego jest opracowanie projektu architektonicznego w oparciu o studium historyczne i autorską waloryzację konserwatorską obiektu/zespołu zabytkowego, a w konsekwencji uzyskanie wiedzy na temat architektonicznych i urbanistycznych uwarunkowań projektowania konserwatorskiego.
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Placement niestacjonarne Analityka I st. 2 sem.
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Hydrologia _ IŚ, inż., stacjonarne, sem. IV - Nowy
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Energetyka sem 1 - Matematyka 2021/22 (D.Beger)
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Placement Elektronika/Telekomunikacja I st. 2 sem.
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Optymalizacja systemów inżynierskich - 20/21 Sem. L
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Wodociągi sem. VI (lato 2022/2023, NST)
e-Learning CoursesKurs jest przeznaczony dla studentów studiów niestacjonarnych I stopnia (semestr VI)
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Inwestycje alternatywne NST sem. zima 23/24
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Mechanika i Budowa Maszyn V sem (WIMiO)
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Kosztorysowanie robót specjalnych - sem. zimowy 2022/2023
e-Learning CoursesKurs na e-nauczaniu wspierający zajęcia stacjonarne Kurs jest przeznaczony dla Studentów II semestru studiów stacjonarnych magisterskich kierunku budownictwo, WILIŚ, specjalności Technologia i Zarządzanie w Budownictwie Osoba odpowiedzialna za przedmiot: dr inż. Beata Grzyl, prof. uczelni: beata.grzyl@pg.edu.pl
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Podstawy budownictwa - sem III GP 2022-23
e-Learning CoursesKurs dla studentów 3. semestru
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Wykłady - Mechanika, ZiIP (II sem., I st)
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Fizyka dla chemików 2023/2024 sem 1
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Optymalizacja systemów inżynierskich - 21/22 Sem. L
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WM - grupa pościgowa, sem. letni 2022/2023
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BADANIA MARKETINGOWE _ZII N_2022/2023 - sem. letni
e-Learning CoursesCelem przedmiotu jest zapoznanie studentów z różnymi metodami pozyskiwania i analizy informacji niezbędnych do podejmowania decyzji w obszarze marketingu.
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Biochemia - seminarium, Biotechnologia sem. VI, 2021/2022
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