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Search results for: nasal discharge samples
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Application of ion chromatography for the determination of inorganic ions, especially thiocyanates in human saliva samples as biomarkers of environmental tobacco smoke exposure
PublicationŚrodowiskowy dym tytoniowy jest jednym z czynników decydujących o jakości powietrza wewnętrznego różnego typu pomieszczeń zamkniętych. Toksyczne składniki wydzielające się wraz z głównym i bocznym strumieniem dymu tytoniowego mają istotny wpływ na skład chemiczny płynów biologicznych. Jednym z biomarkerów narażenia na szkodliwe składniki środowiskowego dymu tytoniowego są jony rodankowe. Celem badań było znalezienie korelacji pomiędzy...
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The research of the contamination levels present in samples of precipitation and surface waters collected from the catchment area Fuglebekken (Hornsund, Svalbard Archipelago)
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Effective phospholipid removal from plasma samples by solid phase extraction with the use of copper (II) modified silica gel cartridges
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Biogeochemia selenu i jego monitoring w materiałach biologicznych pochodzenia ludzkiego = Selenium biochemistry and its monitoring in biological samples
PublicationNa przestrzeni ostatnich kilkudziesięciu lat selen stał się przedmiotem intensywnych badań naukowych w wielu dyscyplinach nauki. Najczęściej poruszanymi zagadnieniami są aspekty związane z biochemią, geologią, toksykologią, wykorzystaniem przemysłowym selenu oraz jego wpływem na organizmy żywe. Powodem szczególnego zainteresowania tym pierwiastkiem jest niewielka różnica pomiędzy jego poziomem niezbędnym a toksycznym oraz szereg...
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Simultaneous determination of individual isothiocyanates in plant samples by HPLC-DAD-MS following SPE and derivatization with N-acetyl-l-cysteine
PublicationThe procedure for the isothiocyanates (ITCs) determination that involves derivatization with N-acetyl-l-cysteine (NAC) and separation by HPLC was developed. Prior to derivatization, plant ITCs were isolated and purified using solid-phase extraction (SPE). The optimum conditions of derivatization are: 500 μL of isopropanolic eluate obtained by SPE combined with 500 μL of derivatizing reagent (0.2 M NAC and 0.2 M NaHCO3 in water)...
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Application of Ion Chromatography for the Determination of Inorganic Ions, Especially Thiocyanates, in Human Semen Samples as Biomarkers of Environmental Tobacco Smoke Exposure.
PublicationPalenie tytoniu stanowi istotne źródło zanieczyszczenia powietrza wewnętrznego. Szkodliwość palenia tytoniu potwierdzają zarówno badania doświadczalne, jak i opracowania epidemiologiczne. Celem przeprowadzonych prac badawczych było uzyskanie informacji o poziomie zawartości jonów nieorganicznych, a zwłaszcza jonów rodankowych (jako biomarkerów narażenia na szkodliwe składniki obecne w środowiskowym dymie tytoniowym) w próbkach...
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Comparison of the Measurement Techniques Employed for Evaluation of Ambient Air Odour Quality Influenced by Operation of Industrial Sewage Treatment Plant
PublicationThe paper presents the results of investigation on ambient air quality evaluation with respect to concentration of odorants in a vicinity of a sewage treatment plant of the LOTOS Group S.A. petroleum plant. The investigation was performed during winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type...
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Monitoring of odour nuisance in the Tricity Agglomeration
PublicationThe paper describes a principle of operation of odour nuisance monitoring network, which is being designed in the Tricity Agglomeration. Moreover, it presents the preliminary results of an investigation on ambient air quality with respect to odour nuisance in a vicinity of the municipal landfill. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The...
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Comparison of the measurement techniques employed for evaluation of ambient air odour quality
PublicationThe paper presents the results of investigation on ambient air odour quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field...
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Rate performance of (NH4)2V10O25·8H2O as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the ammonium vanadate nanostructures obtained by the hydrothermal method under an initial pressure of 50 bar ((NH4)2V10O25·8H2O). The battery tests of the samples were performed using the ATLAS 0961 MBI multichannel battery testing system with different current densities in the voltage...
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Rapid and simple multi-analyte LC–MS/MS method for the determination of benzodiazepines and Z-hypnotic drugs in blood samples: Development, validation and application based on three years of toxicological analyses
PublicationBenzodiazepines (BZDs) and Z-drugs have been particularly important treatments for sleeping and anxiety disorders for many years. However, recently, a number of new benzodiazepines (named designer benzodiazepines, DBZDs) were synthesised, but some of them have never been used in the clinic; they reached the black drug market as new psychoactive substances and are used for recreational purposes. The abuse of these substances has...
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In-situ generation of Ag, Cd, Hg, In, Pb, Tl and Zn volatile species by flowing liquid anode atmospheric pressure glow discharge operated in gaseous jet mode – Evaluation of excitation processes and analytical performance
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Determination of nicotine in saliva, urine and wastewater samples using tantalum metal organic framework pipette tip micro-solid phase extraction
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Application of PSO-artificial neural network and response surface methodology for removal of methylene blue using silver nanoparticles from water samples
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Rate performance of mixture (NH4)2V6O16 and (NH4)2V10O25·8H2O as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the ammonium vanadate nanostructures obtained by the hydrothermal method without initial pressure (mixture (NH4)2V6O16 and (NH4)2V10O25·8H2O). The battery tests of the samples were performed using the ATLAS 0961 MBI multichannel battery testing system with different current densities...
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Fast, sensitive and reliable multi-residue method for routine determination of 34 pesticides from various chemical groups in water samples by using dispersive liquid – liquid microextraction coupled with gas chromatography – mass spectrometry
PublicationA simple and efficient dispersive liquid-liquid microextraction technique (DLLME) was developed by using a mixture of two solvents: 40 μL of tetrachlorethylene (extraction solvent) and 1.0 mL of methanol (disperser solvent), which was rapidly injected with a syringe into 10mL ofwater sample. Some important parameters affecting the extraction efficiency, such as type and volume of solvents, water sample volume, extraction time,...
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A Novel Electrochemical Sensor Based on Graphene Oxide Nanosheets and Ionic Liquid Binder for Differential Pulse Voltammetric Determination of Droxidopa in Pharmaceutical and Urine Samples
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Particle swarm optimization–artificial neural network modeling and optimization of leachable zinc from flour samples by miniaturized homogenous liquid–liquid microextraction
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Synthesis of UiO-66-OH zirconium metal-organic framework and its application for selective extraction and trace determination of thorium in water samples by spectrophotometry
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Highly Sensitive Determination of Bisphenol A in Bottled Water Samples by HPLC after Its Extraction by a Novel Th-MOF Pipette-Tip Micro-SPE
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Determination of organotin compounds in biological samples using accelerated solvent extraction, sodium tetraethylborate ethylation, and multicapillary gas chromatography flame photometric detection.
PublicationPrzedstawiono metodę oznaczania związków cynoorganicznych w próbkach biologicznych. Procedura oparta jest na wykorzystaniu ekstrakcji pod zwiększoną temperaturą i ciśnieniem (ASE) do izolacji związków cynoorganicznych z próbek wątroby morświnów odłowionych w Morzu Bałtyckim. Walidacji metody dokonano na podstawie analizy materiału odniesienia NIES No 11.
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Determination of modifier contents in polymer-modified bitumens and in samples collected from the roads using high performance gel permeation/size exclusion chromatography
PublicationThis paper describes application of high performance gel permeation/size exclusion chromatography (HP-GPC/SEC) for the determination of content of polymer modifiers in modified road bitumens. The obtained results were compared with the measurements based on the procedure recommended by the American Association of State Highway and Transportation Officials, which employs Fourier transform mid-infrared spectroscopy (mid-IR FTIR)....
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples
PublicationCelem prowadzonych badań było opracowanie metodyki oznaczania krótkołańcuchowych kwasów alkanomonokarboksylowych (KKA), opartej na ich izolowaniu i wzbogacaniu za pomocą techniki HS-SPME, a następnie oznaczaniu za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Do ekstrakcji zastosowano włókno pokryte polarną fazą stacjonarną opartą na glikolu polietylenowym (PEG). Dla celów porównawczych zastosowano również...
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SEM micrographs of V2O5 nanorods as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of V2O5 nanorods as cathode materials before and after the galvanostatic charge/discharge curves.
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SEM micrographs of V2O5 nanocrystals as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of V2O5 nanocrystals as cathode materials before and after the galvanostatic charge/discharge curves.
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Application of molecularly imprinted polymer pipette tip micro-solid phase extraction of nalidixic acid and acetaminophen from pills and seawater samples and their determination by spectrophotometry
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Fast determination of bisphenol A in spiked juice and drinking water samples by pipette tip solid phase extraction using cobalt metal organic framework as sorbent
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Application of In-Syringe Dispersive Liquid–Liquid Microextraction and Narrow-Bore Tube Dispersive Liquid–Liquid Microextraction for the Determination of Trace Amounts of BTEX in Water Samples
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Application of response surface methodology for silver nanoparticle stir bar sorptive extraction of heavy metals from drinking water samples: a Box–Behnken design
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DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS IN SOIL SAMPLES USING ULTRASONIC PROBE AND SALT-ASSISTED LIQUID-LIQUID EXTRACTION COUPLED WITH HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY
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Determination of mefenamic acid in urine and pharmaceutical samples by HPLC after pipette-tip solid phase microextraction using zinc sulfide modified carbon nanotubes
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Application of Taguchi L16 design method for comparative study of ability of 3A zeolite in removal of Rhodamine B and Malachite green from environmental water samples
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Co-microprecipitation/flotation of trace amounts of cadmium from environmental samples through its complexation with iodide and neutralization with cetyltrimethylammonium bromide in the presence of perchlorate ions
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Fabrication of a Molecularly Imprinted Polymer Adsorbent for Pipette Tip Micro Solid-phase Extraction of Levofloxacin from Aqueous Samples Prior to its Spectrophotometric Determination
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Solid-Contact Ion-Selective Electrodes with Highly Selective Thioamide Derivatives of p-tert-Butylcalix[4]arene for the Determination of Lead(II) in Environmental Samples
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Izolacja lotnych związków organicznych z próbek wody. Metody i aparatura. Analysis of volatile organic compounds (VOCs) in water samples. Methods and apparatus.
PublicationOmówiono techniki wykorzystywane do przygotowania próbek wody do oznaczeń analitów z grupy lotnych związków organicznych (VOCs) za pomocą chromatografii gazowej. Opisano wady i zalety takich technik jak: bezpośrednie dozowanie próbki wody do kolumny chromatograficznej, ekstrakcja rozpuszczalnikiem, ekstrakcja do fazy stałej lub stacjonarnej, ekstrakcja membranowa oraz analiza fazy nadpowierzchniowej. Omówiono także nowe rozwiązania...
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Solid phase microextraction–comprehensive twodimensional gas chromatography–time-of-flight mass spectrometry: a new tool for determining PAHs in airport runoff water samples
Publicationfundamental aspect of airport operations is the pollution caused by airport runoff waters. Polycyclic aromatic hydrocarbons (PAHs) are one of the most important groups of xenobiotics which are commonly found in runoff water originating from airports. Only very limited data on the analysis of airport runoff water have been published until now. Therefore, a reliable and accurate analytical method based on headspace solid-phase microextraction...
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Influence of pH and low-molecular weight organic compounds in solution on selected spectroscopic and analytical parameters of flowing liquid anode atmospheric pressure glow discharge (FLA-APGD) for the optical emission spectrometric (OES) determination of Ag, Cd, and Pb
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Distribution of volatile organohalogen compounds in petrochemical plant water streams
PublicationThe study assesses halogenated volatile organic compound concentrations in the water and wastewaterstreams of a petrochemical plant. Water samples were collected at 11 sampling points during 5 samplingcampaigns. The samples were collected from the oil dewaxing unit and in the wastewater treatmentplant. Dichloromethane and 1,2-dichloroethane were the most frequently determined compounds. Tetrachloroethenewas also detected at the...
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Synthesis and biological activity of tricyclic aryloimidazo-, pyrimido-, and diazepinopurinediones
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Rate performance of the V2O5 nanocrystals as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanocrystals obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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Rate performance of the V2O5 nanorods as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanorods obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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Determination of profenofos in seawater and foodstuff samples after its molecularly imprinted polymer pipette-tip micro solid phase extraction optimized by response surface methodology
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Comparison of Air-Assisted, Vortex-Assisted and Ultrasound-Assisted Dispersive Liquid–Liquid Microextraction for the Determination of BTEX Compounds in Water Samples Prior to GC-FID Analysis
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Przegląd metod oznaczania pozostałości pestycydów i polichlorowanych bifenyli w próbkach żywności = Methods of determination of residues of pesticides and polychlorinated biphenyls in food samples - a review
PublicationOznaczanie pozostałości pestycydów i analitów z grupy polichlorowanych bifenyli w próbkach żywności wymaga zastosowania specyficznych technik w zakresie przygotowania próbki do analizy, jak i samych technik analizy instrumentalnej, pozwalających na uzyskanie bardzo niskiej granicy oznaczalności. Problemem związanym ze stosowaniem związków z grupy pestycydów i polichlorowanych bifenyli jest konieczność kontroli ich pozostałości...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublicationThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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Electrochemical studies of symmetrical supercapacitors based on BDD, Mn-BDD, Mn-BDD(AN) electrodes
Open Research DataElectrochemical performance of a Supercapacitor device in PVA-H2SO4 gelled electrolyte: Cyclic voltammograms at varying scan rates ranging from 10 to 1000 mV s−1, galvanostatic charge-discharge curves with varying current density, cyclic stability (88000 charge-discharge cycles).
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Modeling and Evaluation of Electric Treeing Phenomena in Polymeric Cable Insulation
PublicationThis paper investigates the treeing phenomenon in polymeric materials such as crosslinked polyethylene (XLPE) that is widely used in medium and high voltage power cables as primary insulation. The modeling of electrical tree growth in the insulation from its initiation to breakdown is significant research work that illustrates the discharge dynamics and its impact on aging process in polymeric insulation. This study utilizes pulse...
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A palatal prosthesis from archaeological research in the St Francis of Assisi church in Cracow (Poland)
PublicationThe hard palate is a septum that not only prevents food from entering between the oral and nasal cavity, but also plays an important role during breathing or speech. The presence of cavities within it negatively affects the comfort of life of people with this type of impairment. Hence, in the literature one can find examples of the use of hard palate prostheses to restore the separation between the nasal and oral cavity. During...