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Search results for: meldrum's acid
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Propensity of salicylamide and ethenzamide cocrystallization with aromatic carboxylic acids
PublicationThe cocrystallization of salicylamide (2-hydroxybenzamide, SMD) and ethenzamide (2-ethoxybenzamide, EMD) with aromatic carboxylic acids was examined both experimentally and theoretically. The supramolecular synthesis taking advantage of the droplet evaporative crystallization (DEC) technique was combined with powder diffraction and vibrational spectroscopy as the analytical tools. This led to identification of eleven new cocrystals...
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Bile Acids: Key Players in Inflammatory Bowel Diseases?
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Electric chips for rapid detection and quantification of nucleic acids
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Biodegradability of modified emulsifiers - esters of polyols and fatty acids
PublicationBadano podatność na biodegradację wybranych emulgatorów estrów polioli i kwasów tłuszczowych przy użyciu testu zamkniętej butelki (OECD 301 D). Stwierdzono, że badane emulgatory nie mogą zostać uznane za łatwo ulegające biodegradacji. Najwyższy poziom rozkładu (57,3%) osiągnął emulgator C14Gna, najniższy (29,8%) AEGNa.
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Mechanism of the reaction of Lawesson's reagent with N-alkylhydroxamic acids
PublicationIdentyfikacja fosforowych produktów powstających w reakcji kwasów hydroksamowych z odczynnikiem Lawessona pozwoliła ustalić mechanizm tytułowej reakcji. Wykorzystano w tym celu spektroskopię 31P NMR. Wzorce labilnych produktów otrzymano na niezależnej drodze syntetycznej lub przeprowadzono je w trwałe pochodne, które wyizolowano z mieszanin reakcyjnych. Produktem przejściowym badanej reakcji okazał się odpowiedni O-ditiofosfonylowany...
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Ion Chromatography in Environmental Analysis of Selected Organic Acids
PublicationLow molecular mass carboxylic acids (LCAs) occur in many environmental compartments dueto natural processes and human activity. When volatile and nonvolatile acids are to be monitored then liquidchromatography, including ion chromatography seems a method of choice. At high pH the acids are inionized form and can be separated as carboxylats by means of anion exchange chromatography. LCAs canalso be separated at low pH by ion exclusion...
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Fatty acids as molecular carriers in cleavable antifungal conjugates
PublicationConjugates composed of C2-18 fatty acid (FA) residues as a molecular carrier and 5-fluorocytosine (5-FC) as an active agent, released upon the action of intracellular esterases on the ester bond between FA and “trimethyl lock” intramolecular linker, demonstrate good in vitro activity against human pathogenic yeasts of Candida spp. The minimal inhibitory concentrations (MIC) values for the most active conjugates containing caprylic...
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State aid for shipyards
Open Research DataThe dataset encompassed a choice of the most important legal acts, a list of selected Polish bibliography and a list of important individual decisions issued on the topic of state aid for shipyards in Poland and in selected UE countries. The data constitute a description of the basic state aid instruments used in practise in the period 1999-2018, but...
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Determination of changes in viscosity of poly(acrylic acid) PAA solutions depending on shear rate.
Open Research DataThe rheological characteristics of poly(acrylic acid) PAA solutions were based on viscosity measurements using a Brookfield viscometer, using LV SC4 - 27 spindles and shear rates from 1,7 to 39 s-1 (Fig. 1). PAA solutions with were prepared in water. The data allowed to characterize the used PAA and assess their functional parameters as rheology modifying...
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Rheology studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains MFR/MVR (melt flow rate) rheology studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The study aims to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different temperatures...
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Physicochemical studies (Raman, XRD) of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains physico-chemical examination of a new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include Raman spectroscopy and X-ray diffraction...
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Topography studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains topography studies with scanning electron microscope of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material...
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Electrochemical analyses of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains cyclic voltammetry studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different temperatures...
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Thermal analyses of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains thermal analyses (TGA, DTG, DSC) studies of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material at different...
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The corrosion studies of 3,4,5-trihydroxybenzoic acid as an effective corrosion inhibitor of low alloy steel
Open Research DataThe dataset contains the electrochemical studies evaluating if gallic acid is a corrosion inhibitor for low alloy steel. Three measurements were carried out each case; corrosion potential (label ecorr), electrochemical impedance spectroscopy (label eis) and cyclic polarization (label cp). The measurements were carried out in sodium chloride, acidified...
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The effect of zinc oxide concentration on dry matter content of chitosan gels in carbonic acid.
Open Research DataThe dataset contains results determining the effect of zinc oxide addition at different concentrations on the dry matter content of chitosan gels in carbonic acid after a specified time. Zinc oxide at concentrations of 0.5 and 1% was added as a powder to a 1% solution of chitosan in carbonic acid and then homogenized. Differences were observed in the...
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Symposium on Assessment of Quality S/W Dev Tools
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MAC contention in a wireless LAN with noncooperative anonymous stations
PublicationRozpatruje się model sieci bezprzewodowej wykorzystywanej przez wzajemnie nieprzenikalne grupy stacji anonimowych. Przy ustalonej regule wyłaniania zwycięzcy rywalizacji o dostęp do medium, stacje posiadają swobodę wyboru strategii selekcji szczeliny rywalizacyjnej. Dla szerokiego zbioru możliwych strategii proponuje się metodologię ich oceny i testowania wydajności opartą na pojęciu zbliżonym do ewolucyjnej stabilności.
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Flexural behaviour of concrete slabs reinforced with FRP bars in experiments and according to aci ACI 440.1R guide
PublicationThe paper presents research conducted on two concrete slabs reinforced with the carbon composite bars and two other concrete slabs reinforced with basalt composite bars. The carbon bars were plain, while the basalt ones were ribbed. The slabs were experimentally investigated in the flexural state of effort with the concentrated forces applied. The results are compared with the analytical solution proposed in the guide ACI 440.1R-06...
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High power, medium voltage, modular active power filtering system
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MEDIUM-TERM WAVE AND CURRENT MODELLING FOR A MESOTIDAL WADDEN SEA COAST
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Modeling of the finite amplitude plane wave propagation in non-dissipative medium
PublicationPraca prezentuje wyniki analizy teoretycznej zagadnienia propagacji fali płaskiej o skończonej amplitudzie w ośrodku wodnym bez dyssypacji. Przedstawiono model matematyczny i przykładowe wyniki obliczeń numerycznych. Model matematyczny zbudowano w oparciu o jednowymiarowe równania mechaniki płynów. Do rozwiązania zagadnienia zastosowano metodę różnic skończonych. Analizowano zmiany ciśnienia i zmiany widma. Badano zbieżność i dokładność...
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Wytwarzanie bezmatrycowego materiału odniesienia lotnych analitów w medium gazowym
PublicationW pracy przedstawiono wyniki kolejnego etapu badań nad możliwością wytworzenia bezmatrycowego materiału odniesienia lotnych związków organicznych w mediach gazowych. Do generowania składników mierzonych (chlorek metylu lub eten) odpowiednich gazowych mieszanin wzorcowych wykorzystano technikę termicznego rozkładu związków powierzchniowych. Przedmiotem badań były:-włókna szklane z naniesionym cienkim filmem poliimidowym, pokryte...
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Iron filled single-wall carbon nanotubes – A novel ferromagnetic medium
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Cash Flow Management in Small and Medium Enterprises in Times of Economic Uncertainty
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Properties of a polyethyleneimine-based sensor for measuring medium and high relative humidity
PublicationW artykule przedstawiono metodę przygotowania filmów polimerowych o zwiększonej odporności na działanie wody. Polietylenoimina została usieciowana w podwyższonej temperaturze. Określono optymalną kompozycję polimeru oraz temperaturę sieciowania. Czujniki rezystancyjne przygotowano metodą ''dip-coating''. Otrzymane czujniki charakteryzują się doskonałą trwałością w wysokich wilgotnościach. Elektryczne parametry czujników określono...
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Electromagnetic wave scattering by a set of axially symmetric omega-medium cylinder
PublicationZaprezentowano analizę rozproszenia fali elektromagnetycznej od układu obiektów cylindrycznych zbudowanych z materiałów pseudochiralnych, umieszczonych w złączach falowodowych lub wolnej przestrzeni. Analiza bazuje na iteracyjnej procedurze rozproszenia i metodzie dopasowania rodzajów.
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Knowledge Safety in Small and Medium Sized Service Companies:Case Study Analysis
PublicationPurpose: This paper aims to explore the topic of knowledge safety, defined as the state of knowledge being safe from loss, attrition, oblivion or theft. The paper first presents a theoretical background and review of previous studies on knowledge loss and retention and then illustrates the topic of knowledge safety with ten case studies from the small and medium-sized enterprises (SMEs) sector. Methodology: The paper is based...
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Analysing selection of low-temperature medium for cogeneration micro power plant
PublicationThe article analyses the ORC system working with dry and wet low-boiling media which are most frequently used in installations of this type. Two types of cycles were examined, which were the cycle with heat regeneration for dry media: fc72, hfe7100, R227ea, R245fa, R423a and R600a, and the cycle without heat regeneration for wet media: R11, R12, R134a, R718 and 507a. The calculations were performed for the assumed required thermal...
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Analysis and Detection of Faults at Insulated Conductors of Overhead Medium Voltage Lines
PublicationThe paper dealt with the issue of breakdowns detection of isolated hanging wires on the medium-voltage transmission. The main aim of article is to describe the function of created breakdowns detector and evaluation its. The breakdowns detector is created based in indicators of faults such as touch between tree limbs and insulated wire, touch tree limbs with several phases or fall insulated wire on the ground. Breakdowns detector...
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Selected Technical Requirements for Photovoltaic Plant Interconnection with a Medium Voltage Grid
PublicationThe article discusses some selected technical requirements, which according to these authors should be recognised and met by photovoltaic power plants connected to national distribution grids in the context of their likely development. This development today is limited, since Polish legislation has not implemented the relevant EU Directive [8]. The study points out the purposefulness of incorporating the necessary requirements...
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Design analysis of Tesla micro-turbine operating on a low-boiling medium
PublicationThis paper presents results of the design analysis of a Tesla bladeless turbine intended for a co-generating micro-power plantof heat capacity 20 kW, which operates in an organic Rankine cycle on a low-boiling medium. Numerical calculations of flowin several Tesla turbine models were performed for a range of design parameters. Results of investigations exhibit interestingfeatures in the distribution of flow parameters within the...
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Analysing selection of low-temperature medium for cogeneration micro power plant
PublicationThe article analyses the ORC system working with dry and wet low-boiling media which are most frequently used in installations of this type. Two types of cycles were examined, which were the cycle with heat regeneration for dry media: fc72, hfe7100, R227ea, R245fa, R423a and R600a, and the cycle without heat regeneration for wet media: R11, R12, R134a, R718 and 507a. The calculations were performed for the assumed required thermal...
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Training Services in Small and Medium-sized Enterprises: Evidence from Poland
PublicationIn the knowledge-based economy knowledge and skills are becoming more and more significant for the success of companies. This applies also to firms from small and medium-sized enterprises (SMEs) sector. As large companies in many cases posses special divisions devoted to trainings, they normally have no problems with updating the knowledge and skills of their employees. The situation is different with regard to SMEs, which often...
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Knowledge management approaches of small and medium-sized firms: a cluster analysis
PublicationPurpose This paper aims to categorise the approaches to knowledge management (KM) by companies. In the literature, there is no consensus on a universal or “best” approach to KM. Especially, this paper singles out and discusses the variegated features that characterise the implementation of KM by small- and medium-sized enterprises (SMEs) having different characteristics. Design/methodology/approach A cluster analysis was used...
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Shaping the competence of future spatial policymakers for small- and medium-sized towns
PublicationIn this article, the authors aim to present issues addressed within the framework of the architecture and spatial development courses offered by the Faculty of Architecture at Gdańsk University of Technology (FA-GUT), Gdańsk, Poland. These issues concern competence in the education of future spatial planners and their readiness to deal with the development challenges facing small- and medium-sized towns. Within the article, the...
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Ciecze głęboko eutektyczne pochodzenia naturalnego jako nowe medium ekstrakcji
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Energy losses reduction in the medium voltage cable line – case study
PublicationThe paper presents an analysis of energy losses in a power cable system, which is composed of two 30 kV cable lines. This cable system is located at the seaside holiday area, so the load profile during a year is specific. Energy losses related to reactive power transmission, as well as to currents induced in the sheaths of the cables, are subject to analysis. Measurements were made in the system in order to prepare a computer model...
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Earthquake-Induced Pounding of Medium-to-High-Rise Base-Isolated Buildings
PublicationDuring earthquakes, out-of-phase vibrations in adjacent buildings with limited distance may cause pounding between them. In recent years, the use of seismic isolation has expanded considerably as an effective approach to reduce seismic damage. However, the isolated building experiences large displacements during earthquakes, and there is a possibility of collisions with adjacent structures. The research on earthquake-induced pounding...
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Improvement of Task Management with Process Models in Small and Medium Software Companies
PublicationSmall and medium software companies exhibit many special features that give reason for a dedicated approach to process improvement. They often cannot afford implementing maturity models or quality standards both in terms of time and money. Instead, they expect simpler solutions that can allow to run projects in more systematic and repeatable way, increase quality and knowledge management. In this paper, we present a method focused...
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Subjective and Objective Quality Evaluation Study of BPL -PLC Wired Medium
PublicationThis paper presents results of research on the effectiveness of bi-directional voice transmission in a 6 kV mine cable network using BPL-PLC (Broadband over Power Line - Power Line Communication) technology. It concerns both emergency cable state (supply outage with cable shorted at both ends) and loaded with distorted current waveforms. The narrowband (0.5 MHz–15 MHz) and broadband (two different modes, frequency range of 3 MHz–7.5...
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Sławomir Milewski prof. dr hab. inż.
PeopleSławomir Milewski, born in 1955 in Puck, Poland, graduated in 1979 in Chemistry from the Faculty of Chemistry, Gdańsk University of Technology (GUT). In 1984 was employed at the Department of Pharmaceutical Technology and Biochemistry. In 1985 he got his PhD, in 1994 became a DSc (habilitation) and in 2002 got the professorship in chemical sciences. Currently he is a full professor and Head of the Department of Pharmaceutical Technology...
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Special hearing aid for stuttering people
PublicationDzięku postępowi w dziedzienie cyfrowego przetwarzania sygnałów możliwe stało zbudowanie subminiaturowego urządzenia łączącego funkcje aparatu słuchowego i korektora mowy. Takie urządzenie, mimo niewielkich rozmiarów, jest w stanie wykonywać skomplikowane alggorytmy a jego oprogramowanie może być łatwo zmieniane. W pracy skupiono się na zagadnieniach związanych z opracowniem prototypu i implementacją algorytmów korekcji słuchu...
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Contactless hearing aid designed for infants
PublicationIt is a well known fact that language development through home intervention for a hearing-impaired infant should start in the early months of a newborn baby's life. The aim of this paper is to present a concept of a contactless digital hearing aid designed especially for infants. In contrast to all typical wearable hearing aid solutions (ITC, ITE, BTE), the proposed device is mounted in the infant's bed with any parts of its set-up...
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Uwarunkowania fizyczne w opracowaniu wyników badań eksperymentalnych. W:Geotechnika w budownictwie i górnictwie. Red. W. Brząbała, J. Butyra, S. Gałczyński. Wrocław: P. Wroc.**2003 s. 134-141, 9 rys. bibliogr. 5 poz.
PublicationW wielu przypadkach opracowanie wyników badań uzyskanych w formie tabelarycznej wymaga aproksymacji danych funkcją ciągłą. Poszukiwana funkcja jest kom-binacją skończonej liczby funkcji podstawowych. W artykule opisano sytuacje, w której aproksymacja wielomianami wysokiego (trzeciego i czwartego) stop-nia, mimo małych różnic pomiędzy danymi eksperymentalnymi a funkcją aprok-symującą nie może być zastosowana ze względu na utratę...
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S-seco-porphyrazine as a new member of the seco-porphyrazine family – Synthesis, characterization and photocytotoxicity against cancer cells
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Ochrana před úrazem elektrickým proudem při použití proudových chráničů v obvodech s měniči frekvence
PublicationObwody zawierające przemienniki częstotliwości charakteryzują się tym, że kształt prądu ziemnozwarciowego zależy od miejsca zwarcia. Prądy ziemnozwarciowe mogą mieć różną częstotliwość oraz być mocno odkształcone, a także, w zależności od zastosowanego układu prostownikowego, mogą być jednokierunkowe o małym lub dużym tętnieniu. Kształt i częstotliwość prądu znacząco wpływa na poprawne działanie wyłączników różnicowoprądowych....
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Preliminary Microbiological Tests of S-Carvone and Geraniol and Selected Derivatives of These Compounds That May Be Formed in the Processes of Isomerization and Oxidation
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Analiza słonecznego ogrzewania wody. Instalacje Sanitarne**2002 nr 3 s. 30-32, 6 rys.
PublicationPrzedstawiono studium parametryczne oceny ekonomicznej efektywności insta-lacji slonecznego ogrzewania wody, wykorzystującej zmodyfikowaną do potrzebenergetyki słonecznej metodę ''Zaktualizowanej Wartości Netto'' -NPVW. Stwier-dzono istnienie znacznych obszarów opłacalności słonecznego ogrzewania wodyw okresie 25-letniego horyzontu czasowego. Jest jednak konieczna pomoc rządowa w zakresie inwestowania na instalację słoneczną.
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Gry bardzo serio. CXO Nowy Magazyn Kadry Zarządzającej.**2002 nr 12 s.26-28.
PublicationGry symulacyjne Lean są typem symulacji społecznej, której zasady są opartenie na współzawodnictwie, ale na wypracowaniu zespołowej taktyki działania.Celem symulacji jest wzmacnianie u uczących się umiejętności współdziałania,negocjowania, osiągania kompromisu, wypracowania wspólnej strategii Leanprzez wszystkich uczestników zespołu reprezentujących różne interesy. Arty-kuł przedstawia rodzaje gier symulacyjnych, sposoby...