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Search results for: WET SYTHESIS
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Comprehensive study on graphene hydrogels and aerogels synthesis and their ability of gold nanoparticles adsorption
PublicationGraphene hydrogels were prepared by ascorbic acid-assisted gelation of graphene oxide (GO) aqueous suspensions both in acidic and basic conditions. Different mass ratio of ascorbic acid (AA) to GO was used (namely 20:1 and 10:1). In order to eliminate the influence of AA on the final structure of hydrogels, samples without AA were prepared by a hydrothermal gelation of GO in an autoclave. An in-depth structural characterization...
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A new approach to the stereoselective synthesis of trans-3-carbamoyl-b-lactam moieties†
PublicationOne-pot synthesis of optically active 1,4-disubstituted-3-carbamoyl-azetidinones from 5-[(N-arylamino)- (hydroxyl)methylene]-2,2-dimethyl-1,3-dioxa-4,6-diones and chiral aldimines is achieved via thermal generation of carbamoyl ketenes and subsequent [2+2] cycloaddition. Three possible chiral induction approaches were tested and (R)-(+)-1-phenylethylamine was confirmed as the best chiral auxiliary. Among the four possible diastereoisomers,...
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The synthesis and structure of a potential immunosuppressant: N-mycophenoyl malonic acid dimethyl ester
PublicationThe synthesis of a potential immunosuppressant, i.e. dimethyl ester of N-mycophenoyl malonic acid was optimized in the reaction of mycophenolic acid (MPA) with amino malonic dimethyl ester in the presence of propanephosphonic anhydride (T3P) as a coupling reagent. The structural properties of the obtained MPA derivative were investigated by NMR, MS and single crystal X-ray diffraction methods. Theoretical considerations of conformational...
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Voiceless Stop Consonant Modelling and Synthesis Framework Based on MISO Dynamic System
PublicationA voiceless stop consonant phoneme modelling and synthesis framework based on a phoneme modelling in low-frequency range and high-frequency range separately is proposed. The phoneme signal is decomposed into the sums of simpler basic components and described as the output of a linear multiple-input and single-output (MISO) system. The impulse response of each channel is a third order quasi-polynomial. Using this framework, the...
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Solid-phase synthesis and characterization of N-acetylated Gly-His-Lys analogues
PublicationZaprezentowano nowe analogi tripeptydu Gly-His-Lys (GHK), stanowiącego sekwencję naturalnie występującą w -II-łańuchu kolagenu, skąd jest uwalniany w stanach zapalnych i w procesach gojenia się ran. Gly-His-Lys jest szeroko stosowany na rynku kosmetycznym w połączeniu z kwasem palmitynowym, który ułatwia jego wnikanie w głąb skóry. Zaplanowane modyfikacje zawierały fragment Gly-X-Y (X=Met, Hyp, Hyp-Met, Gly-Hyp; Y=Lys, D-Lys) i...
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Comparison of Optimization Techniques for Coupling Matrix Synthesis Using Eigenvalue Based Approach
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A Green Chemistry "environmentally friendly" approach to the synthesis of chloro-intermediates of ephedrine/pseudoephedrine
PublicationMethylamphetamine is an addictive stimulant drug that strongly activates certain systems in the brain. It is closely related chemically to amphetamine, but the central nervous system effects of methamphetamine are greater. There is much interest in methylamphetamine among scientists and therefore the synthesizes of methylamphetamine and its metabolites are carried out on a large scale in chemical laboratories. Globally, ephedrine...
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Synthesis of 5-Substituted 1H-Tetrazoles from Nitriles in the Presence of Heterogeneous Catalyst
PublicationTetrazoles are five-membered heterocyclic compounds containing in their rings four nitrogen atoms. They have wide applications as corrosion inhibitors, analytical reagents, high-energy materials and gas generating compositions. Tetrazoles also play important role in coordination chemistry as ligands and in medicinal chemistry as metabolically stable surrogates for carboxylic acids. In recent years, investigation of new method of...
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Inhibitors of glucosamine-6-phosphate synthase as potential antimicrobials or antidiabetics – synthesis and properties
PublicationGlucosamine-6-phosphate synthase (GlcN-6-P synthase) is known as a promising target for antimicrobial agents and antidiabetics. Several compounds of natural or synthetic origin have been identified as inhibitors of this enzyme. This set comprises highly selective L-glutamine, amino sugar phosphate or transition state intermediate cis-enolamine analogues. Relatively low antimicrobial activity of these inhibitors, poorly penetrating...
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Computer-assisted pronunciation training—Speech synthesis is almost all you need
PublicationThe research community has long studied computer-assisted pronunciation training (CAPT) methods in non-native speech. Researchers focused on studying various model architectures, such as Bayesian networks and deep learning methods, as well as on the analysis of different representations of the speech signal. Despite significant progress in recent years, existing CAPT methods are not able to detect pronunciation errors with high...
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Synthesis of bimetallic Co–Pt/cellulose nanocomposites for catalytic reduction of p-nitrophenol
PublicationIn this study, bimetallic nanoparticles (NPs) of Co–Pt anchored on cellulose nanofibers (CNFs) for catalytic applications were synthesized via a sonochemical approach. The electro-spinning technique was employed for the synthesis of CNFs from cellulose acetate. The thorough characterization of synthesised Co–Pt/CNF nanocomposites was performed with the help of scanning electron microscopy (SEM), Fourier transform infra-red (FT-IR)...
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Ladder-Based Synthesis and Design of Low-Frequency Buffer-Based CMOS Filters
PublicationBuffer-based CMOS filters are maximally simplified circuits containing as few transistors as possible. Their applications, among others, include nano to micro watt biomedical sensors that process physiological signals of frequencies from 0.01 Hz to about 3 kHz. The order of a buffer-based filter is not greater than two. Hence, to obtain higher-order filters, a cascade of second-order filters is constructed. In this paper, a more...
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New synthesis route of highly porous InxCo4Sb12 with strongly reduced thermal conductivity
PublicationHighly porous, In-filled CoSb3 skutterudite materials with an attractive thermoelectric figure of merit (ZT * 1) and corresponding dense samples were fabricated through the cost-effective method of reduction in oxides in dry hydrogen and the pulsed electric current sintering (PECS) method, respectively. The reduction process was described in detail using in situ thermogravimetric analysis of Co2O3, Sb2O3 and In(NO3)35H2O separately...
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Shape-controllable synthesis of GdVO4 photocatalysts and their tunable properties in photocatalytic hydrogen generation
PublicationNovel visible light responsive materials for water splitting are essential for the efficient conversion of solar energy into hydrogen bond energy. Among other semiconductors, gadolinium orthovanadate has appropriate conduction and valence band edges positioned to split water molecules and a narrow band gap that allows the use of visible light for hydrogen generation. Thus, we present here that hydrogen evolution under visible light...
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Molecularly Imprinted Polymers for Stir Bar Sorptive Extraction: Synthesis, Characterization, and Application
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Beta-Galactosidases of Pseudoalteromonas sp. – Characteristics and application for lactose hydrolysis and galactopyranosides synthesis
PublicationBeta-galactosidase [EC 3.2.1.23] is an enzyme that catalyzes the hydrolysis of O-glycosidic linkages in galactosides. It has biotechnological applications in the dairy industry for the production of milk with a low content of lactose and galactooligosacharides for use in healthy food. The transgalactosylation activity of beta-galactosidase can be used in the synthesis of alkyl galactopyranosides. Due to the fact that conditions of...
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Trakt porodowy we współczesnym szpitalu.
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Rosja we wczesnych utworach Mickiewicza
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Regionalizm we współczesnej architekturze Kaszub
PublicationWspółczesne procesy społeczno-gospodarcze przeobrażeń polskiej wsi doprowadziły do zmian w sferze kulturowej, których wyrazem stały się m.in.: zanik tradycyjnych cech przestrzennych krajobrazu kulturowego wsi i upowszechnienie zrywających z tą tradycją zuniformizowanych wzorców zabudowy i układów przestrzennych osiedli wiejskich. Celowość nawiązania we współczesnej architekturze Kaszub do ich tradycji budownictwa ludowego ma więc...
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Światło we współczesnej przestrzeni publicznej
PublicationArtykuł opisuje znaczenie oświetlenia przestrzeni publicznych. Wyróżnione zostały różne podejścia do używania tworzywa jakim jest światło sztuczne w kreowaniu scenografii przestrzeni publicznej.
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Inspiracje muzyczne we współczesnej architekturze.
PublicationW pracy podjęty został temat złożonych relacji pomiędzy architekturą i muzyką oraz udział muzyki - tytułowej inspiracji - we współczesnej praktyce architektonicznej. Głównym zadaniem pracy było zebranie i usystematyzowanie wiedzy na temat podejmowanych prób udziału muzyki w tworzeniu architektury oraz ukazanie nowych sposobów kształtowania przestrzeni, jakie stwarza wykorzystanie muzyki - jako nauki i sztuki - w dziele architektonicznym,...
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Sektor MSP we współczesnej gospodarce
PublicationPraca uwzględnia najnowszy dorobek teorii ekonomii, jak również badania nad sektorem MSP w krajach wysoko rozwiniętych prowadzone na przełomie XX i XXI wieków. Zawiera także analizy najnowszych dostępnych danych statystycznych z wielu krajów. Jest próbą odpowiedzi na szereg pytań takich jak np.: W czym przejawia się wpływ sektora MSP na wzrost gospodarczy?Czy znaczenie sektora MSP w wysoko rozwiniętych krajach nadal rośnie?Czy...
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Marketing relacji we współczesnym świecie
PublicationTeoria i praktyka marketingu ulegają ciągłej ewolucji, podążając za zmianami gospodarczymi, społecznymi oraz technologicznymi i dostosowując się do nich. Obecne trendy, które napędzają zmiany w globalnym świecie biznesu powodują, że silne relacje z klientami są bardziej niż kiedykolwiek, niezbędne dla strategii firm, które chcą osiągać przewagę konkurencyjną. Nowe warunki działania przedsiębiorstw to również świat, w którym miesza...
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Nuclear Magnetic Resonance data for the synthesis of esterase cleavable antifungal conjugates containing fatty acids as molecular carriers
Open Research DataNMR data for novel organic compounds - conjugates composed of C2-18 fatty acid (FA) residues as a molecular carrier and 5-fluorocytosine (5-FC) as an active agent, released upon the action of intracellular esterases on the ester bond between FA and “trimethyl lock” intramolecular linker.
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Organic syntheses greenness assessment with multicriteria decision analysis
PublicationGreen chemistry requires a metrics system that is comprehensive by the criteria included and simple in the application at the same time. We propose the application of multicriteria decision analysis for com- parative greenness assessment of organic synthesis procedures. The assessment is based on 9 criteria (the reagent, reaction efficiency, atom economy, temperature, pressure, synthesis time, solvent, catalyst and reactant) for...
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Collocations et représentation féminine dans les oeuvres de Colette : Une analyse linguistique et littéraire
PublicationSidonie-Gabrielle Colette played a significant role in the development of French literature. Her novels vividly depict independent and self-aware women, thereby reflecting the author herself. Colette’s works have captured the attention of researchers and have been the subject of numerous studies. In this proposed research, an interdisciplinary approach combining literary and linguistic perspectives is adopted to explore Colette’s...
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Optoelectronic Devices, Sensors, Communication and Multimedia, Photonics Applications and Web Engineering, Wilga, May 2012
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Biomedical, Artificial Intelligence, and DNA Computing Photonics Applications and Web Engineering, Wilga, May 2012
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Suitability of Laser Engineered Net Shaping Technology for Inconel 625 Based Parts Repair Process
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Impact of Movement Tempo Distribution on Bar Velocity During a Multi-Set Bench Press Exercise
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Modelling of the soft X-ray tungsten spectra expected to be registered by GEM detection system for WEST
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How Good Is My Project? Experiences from Projecting Software Quality Using a Reference Set
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AN EXPERIMENTAL STUDY OF THE PHOTOCATALYTIC HYDROGEN PRODUCTION IN THE LABORATORY-SCALE SET-UP DEPENDING ON THE PROCESS CONDITIONS
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Molecular mechanism(s) of regulation(s) of c-MET/HGF signaling in head and neck cancer
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Mass spectrometry reveals the presence of specific set of epigenetic DNA modifications in the Norway spruce genome
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Reduction of Conducted Emissions Generated by WPT Systems with Multilevel Inverters using Spread Spectrum Approach
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Methodology for developing Web-Based applications from reusable components using open source tools
PublicationGlobalna sieć stwarza nowe mozliwości dla projektantów IT. Pozwala na budowanie aplikacji z wielu części zwanych komponentami i rozproszonych w różnych miejscach sieci. metodologia wskazuje jak zbudować wszystkie elementy systemu: warstwę logiki biznesowej, dostępu do danych oraz prezentacji z gruboziarnistych komponentów. Takie mozliwości daje język Java i powiązane z nim technologie open-source: EJB do tworzenia komponentów biznesowych...
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Rapid development of custom web application with ruby on rails framework on the example of group project system
PublicationTechnology industry labor market requires engineers with a good preparation for work with project's tasks and team cooperation skills. One of the way for achieve that abilities during technical university education are students group projects. Running of group projects at university brings new challenges, from recruitment of students with required skills for par-ticular project, to lack of industrial procedures and ready to use...
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EFFECT OF CHITOSAN AND LIPID LAYERS DEPOSITED ONTO POLYETHYLENE TEREPHTHALATE (PET) ON ITS WETTING PROPERTIES
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SELECTING A REPRESENTATIVE DATA SET OF THE REQUIRED SIZE USING THE AGENT-BASED POPULATION LEARNING ALGORITHM
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Set membership estimation of parameters and variables in dynamic networks by recursive algorithms with moving measurment window
PublicationW artykule rozważana jest łączna estymacja przedziałowa zmiennych i parametrów w złożonej sieci dynamicznej w oparciu niepewne modele parametryczne i ograniczoną liczbę pomiarów. Opracowany został rekursywny algorytm estymacji z przesuwnym oknem pomiarowym, odpowiedni dla monitorowania sieci on-line. Okno pomiarowe pozwala na stabilizowanie klasycznego algorytmu rekurencyjnego estymacji i znacznie poprawienie obcisłości estymat....
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Collaborative planning? Not yet seen in Poland. Identifying procedural gaps in the planning system 2003–2023
PublicationCollaborative planning aims to increase the legitimacy of decision-making in spatial development. In this approach, planning involves debate and engagement in discourse, and participation and interaction between actors are thus at the heart of the planning process. This article examines whether the planning system in Poland as defined for the period 2003–2025 provides a level of participation and deliberation and other qualities...
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Experimental investigations of hydraulic jump created by a two-phase impin-ging jet on a solid surface
PublicationPrzedstawiono rezultaty badań eksperymentalnych powstawania uskoku hydraulicznego tworzonego przez dwufazową strugę uderzającą.
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Creating neural models using an adaptive algorithm for optimal size of neural network and training set.
PublicationZaprezentowano adaptacyjny algorytm generujący modele neuronowe liniowych układów mikrofalowych, zdolny do oszacowania optymalnego rozmiaru zbiory uczącego i sieci neuronowej. Stworzono kilka modeli nieciągłości falowodowych i mokropaskowych, a następnie zweryfikowano ich poprawność porównując wyniki analiz metodą dopasowania rodzajów i metodą momentów filtrów pasmowo-przepustowych.
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Experimental study of the fuel jet combustion in high temperature and low oxygen content exhaust gases
PublicationPrzeprowadzono badania eksperymentalne spalania pojedynczego strumienia paliwa gazowego. Paliwo podawano współosiowo do generowanych przez konwencjonalny palnik gazowy spalin o wysokiej temperaturze i niskiej zawartości tlenu. Badano wpływ zawartości tlenu w utleniaczu na widzialność płomienia i skład produktów spalania.
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Why set of experience knowledge structure can be considered a knowledge representattion for formal decision events?
PublicationOmówiono zasady reprezentacji wiedzy przy pomocy zbioru dośwadczeń. Uzasadniono wybór takiej reprezentacji na tle badańliteraturowych.
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A Web-GIS tool for diagnosing spatial orientation of young adults: design and evaluation of Geo-Survey
PublicationSpatial orientation is the effectiveness with which one is able to assess the mutual location of objects relative to a point of reference or a system of coordinates. Traditionally, this ability has been evaluated through field navigation tests, which do not take into account the prevailing influence of free online maps and virtual walks on a person’s interpretation of space. In this context, this study presents a Web-GIS tool designed...
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Net-zero carbon condition in wastewater treatment plants: A systematic review of mitigation strategies and challenges
PublicationThe wastewater sector accounts for up to 7 and 10% of anthropogenic CH4 and N2O emissions, respectively. Nowadays wastewater treatment plants are going through a paradigm shift to approach a net-zero carbon condition. Numerous ongoing measures have taken place to identify the sources of greenhouse gases and minimize the carbon footprint. This paper systematically reviews all known practices leading towards net-zero carbon wastewater...
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Wpływ parametru WSR procesu SBM na jakość estetyczną wytwarzanych pojemników z PET
PublicationAbstrakt w materiałach konferencyjnych konferencji Młodzi dla techniki 2015
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Stereo vision with Equal Baseline Multiple Camera Set (EBMCS) for obtaining depth maps of plants
PublicationThis paper presents a method of improving the estimation of distances between an autonomous harvesting robot and plants with ripe fruits by using the vision system based on five cameras. The system is called Equal Baseline Multiple Camera Set (EBMCS). EBMCS has some features of a camera matrix and a camera array. EBMCS is regarded as a set of stereo cameras for estimating distances by obtaining disparity maps and depth maps. This...