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Search results for: nlc
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Abrasive Wear, Scuffing and Rolling Contact Fatigue of DLC-Coated 18CrNiMo7-6 Steel Lubricated by a Pure and Contaminated Gear Oil
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Chromatografia cienkowarstwowa i technika TLC-FID w badaniach składu grupowego, szczególnie, tłuszczów i produktów ich konwersji
PublicationPraca dotyczy zbadania celowości stosowania oraz określenia korzystnych warunków wykorzystania "klasycznej" chromatografii cienkowarstwowej w normalnych układach faz (NP-TLC) oraz techniki chromatografii cienkowarstwowej z detekcją płomieniowo - jonizacyjną (TLC-FID) na pręcikach kwarcowych, jako technik zapewniających oznaczanie składu grupowego, w badaniach nad: - ustaleniem optymalnych warunków rozdzielania grupowego tłuszczów...
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Virtual Space Vector Pulse Width Modulation Algorithm for Three-Level NPC Converters Based on the Final Element Shape Functions
PublicationThe paper puts forth a novel idea for the computation of Nearest Three Virtual Space Vector Pulse Width Modulation for the three level NPC converters. The computations are based on the concept of final element shape function widely used in the domain of finite element analysis. The proposed approach significantly frees the computations from the use of trigonometric functions, which simplifies the computations and permits easier...
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Fingerprint comparison of low-volatile petroleum products by means of Thin Layer Chromatography (TLC) for identification of process leakages and environmental pollution
PublicationW pracy zbadano możliwość zastosowania stosunkowo prostej i szybkiej procedury przygotowania próbki, rozdzielania grup składników techniką cienkowarstwowej chromatografii cieczowej (TLC), wizualizacji w świetle UV 254 oraz 360 nm i analizy porównawczej cech plamek na płytkach TLC do określenia rodzaju niskolotnego materiału ropopochodnego stanowiącego zanieczyszczenie wód procesowych, lub wyciek z instalacji w rafinerii ropy naftowej....
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Speed sensorless asynchronous motor drive with inverter output lc filter
PublicationIn this paper a speed sensorless ac drive with inverter and output LC filter is proposed. A nonlinear, decoupled field oriented control algorithm with a flux and speed close-loop observer is used. In spite of using LC filter on the inverter output, the sensorless system works precisely. That result are obtained as a result of the appropriate estimation and control system use. The theory, simulation, and experimental results are...
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Frequency bands selection of the Portevin-LeChatelier
PublicationEfekt Portevina-LeChateliera ujawnia się w postaci skokowych zmian naprężenia w trakcie procesu odkształcenia próbek pewnych stopów. Zjawisko PLC występuje w kilku odmianach charakteryzujących się istotnymi różnicami zarówno w przestrzennym rozkładzie pasm odkształcenia jak też przebiegu krzywej naprężeniowej. Przebiegi odpowiadające różnym odmianom serration charakteryzują się odmiennymi właściwościami rozkładu energetycznego...
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Advanced Control With PLC—Code Generator for aMPC Controller Implementation and Cooperation With External Computational Server for Dealing With Multidimensionality, Constraints and LMI Based Robustness
PublicationThe manufacturers of Programmable Logic Controllers (PLC) usually equip their products with extremely simple control algorithms, such as PID and on-off regulators. However, modern PLCs have much more efficient processors and extensive memory, which enables implementing more sophisticated controllers. The paper discusses issues related to the implementation of matrix operations, time limitations for code execution within one PLC...
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Reversed-Phase TLC and HPLC Retention Data in Correlation Studies with in Silico Molecular Descriptors and Druglikeness Properties of Newly Synthesized Anticonvulsant Succinimide Derivatives
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Modelling of SO2 and NOx Emissions from Coal and Biomass Combustion in Air-Firing, Oxyfuel, iG-CLC, and CLOU Conditions by Fuzzy Logic Approach
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LC-ESI-MS profiling of Potentilla norvegica and evaluation of its biological activities
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Recent advancements in LC‐MS based analysis of biotoxins: Present and future challenges
PublicationThere has been a rising concern regarding the harmful impact of biotoxins, source of origin, and the determination of the specific type of toxin. With numerous reports on their extensive spread, biotoxins pose a critical challenge to figure out their parent groups, metabolites, and concentration. In that aspect, liquid chromatography‐mass spectrometry (LC‐MS) based analysis paves the way for its accurate identification and quantification....
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Europejska Noc Muzeów na Politechnice Gdańskiej
EventsProgram dostępny na stronie https://pg.edu.pl/otwarta w Aktualnościach
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Europejska Noc Muzeów na Politechnice Gdańskiej
EventsEuropejska Noc Muzeów na Politechnice Gdańskiej. Program w Aktualnościach na stronie pg.edu.pl/otwarta.
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Wioleta Kucharska dr hab. inż.
PeopleWioleta Kucharska (Associate Professor at the Faculty of Management and Economics of the Gdansk University of Technology, Fahrenheit Universities Union, Poland), published so far with Wiley, Springer, Taylor & Francis, Emerald, Sage, Elsevier, and Routledge. She is scientifically involved in tacit knowledge and the company culture of knowledge, learning, and collaboration (KLC approach) topics. Recently, she discovered the...
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Multivariate Optimization of the FLC-dc-APGD-Based Reaction-Discharge System for Continuous Production of a Plasma-Activated Liquid of Defined Physicochemical and Anti-Phytopathogenic Properties
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Association between Breastmilk LC PUFA, Carotenoids and Psychomotor Development of Exclusively Breastfed Infants
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A Robust Method for Sample Preparation of Gastrointestinal Stromal Tumour for LC/MS Untargeted Metabolomics
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Analysis of urinary nucleosides as potential cancer markers determined using LC–MS technique
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Identification of antioxidant polyphenolics from Jasione montana based on a preliminary LC-MS profiling
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Dielectric response of electric-field distortions of the twist-bend nematic phase for LC dimers
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Wpływ parametrów filtra wejściowego lc pojazdu na stabilność trakcyjnego układu zasilania
PublicationW referacie przedstawiono wpływ zmiany parametrów elektrycznych filtra na stabilność układu zasilania trakcji elektrycznej. Zaprezentowano ogólne założenia teoretyczne problemu oraz zaproponowano nowy współczynnik pozwalający na wstępne określenie stabilności sys-temu dla przyjętych parametrów filtra wejściowego. Przedstawiono wyniki analizy symula-cyjnej wykonanej w programie PSpice przy wykorzystaniu opracowanych modeli poszcze-gólnych...
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Novel materials and approaches for solid-phase (micro) extraction in LC-MS-based metabolomics
PublicationMetabolomics offers a unique approach to study biological systems. Liquid chromatography coupled to mass spectrometry serves as a powerful analytical tool to analyze complex mixtures of metabolites. However, successful metabolomic analysis relies on sample preparation. While untargeted analysis traditionally favors nonselective procedures like liquid-liquid extraction (LLE), these methods can compromise analytical performance due...
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Development and validation of an LC–MS/MS method for the determination of biogenic amines in wines and beers
PublicationBiogenic amines are group of organic, basic, nitrogenous compounds that naturally occur in plant, microorganism, and animal organisms. Biogenic amines are mainly produced through decarboxylation of amino acids. They are formed during manufacturing of some kind of food and beverages such as cheese, wine, or beer. Histamine, cadaverine, agmatine, tyramine, putrescine, and b-phenylethylamine are the most common biogenic amines found...
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Crystal structure, DFT-study and NLO properties of the novel copper(I) nitrate π,σ-coordination compound based on 1-allyl-3-norbornan-thiourea
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Phenolic composition and antioxidant properties of polish blue-berried honeysuckle genotypes by HPLC-DAD-MS, HPLC postcolumn derivatization with ABTS or FC, and TLC with DPPH visualization
PublicationIn this study, different Polish cultivars of blue-berried honeysuckles (Lonicera caerulea L.), wild and bog bilberry, were analyzed for bioactive compounds. The chemical properties verified included composition of anthocyanins and other polyphenols, antioxidant activity, and profiles of antioxidants by HPLC postcolumn derivatization or TLC. The antioxidant activities of different blue-berried honeysuckle cultivars were similar...
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Dynamics of fault arc traveling along busbars in high voltage switchboards = Dynamika łuku zwarciowego przemieszczającego się wzdłuż szyn rozdziel-nic wysokiego napięcia
PublicationThe paper presents the results of magnetic induction and electrodynamic force calculations acting on arc column during short-circuit in medium voltage air-insulated bus-bars. The gap between the bars was 120 mm and the prospective short-circuit currents ranged from 4 kA to 8 kA. The paper also shows the measurement results of average velocity fault arc depending on currents arc diameter and arc current was established and described....
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DLC coating in ring-on-ring sliding with water lubrication 10MPa/0.1m/s
Open Research DataWear tests in sliding friction of DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 10MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was augmented by vibration...
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DLC coating in ring-on-ring sliding with water lubrication 20MPa/0.1m/s
Open Research DataWear tests in sliding friction of DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 20MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was augmented by vibration...
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Determining the true content of quercetin and its derivatives in plants employing SSDM and LC–MS analysis
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LC–MS/MS analysis, antioxidant and anticholinergic properties of galanga (Alpinia officinarum Hance) rhizomes
PublicationGalanga (Alpinia officinarum Hance) is a pungent and aromatic rhizome, which is a member of the ginger family (Zingiberaceae). The rhizomes of this plant have been used as a traditional medicine in far east countries for relieving stomach ache, invigorating the circulatory system, treating colds, and reducing swelling. The aim of this study was to investigate antioxidant and anticholinergic properties of galanga. For this purpose,...
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Main strategies, analytical trends and challenges in LC-MS and ambient mass spectrometry-based metabolomics
PublicationA plethora of analytical LC-MS-based methods have been successfully applied to analyses of complex samples of various origin for metabolomics investigations. Over the last ten years, the substantial evolution of ambient mass spectrometry (AMS) techniques has highlighted their tremendous potential in metabolomic studies due to the minimal sample pretreatment requirement and the ability to analyse samples in their native state. This...
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SU‐GG‐T‐208: 3‐D Dosimetric Comparison of IMRT with 2.5 Mm HD120 MLC Using Optical CT Based Polymer Gel and PRESAGE Dosimeters
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Jaroslaw Spychala dr
PeopleOprócz bardzo dobrego wykształcenia osoba posiada również wieloletnie doświadczenie zawodowe, które jest poświadczeniem tego, że potrafi wykorzystać swoją wiedzę teoretyczną w praktycznych działaniach. Doświadczenie zawodowe jest bardzo bogate i rozbudowane. Ze względu na nabyte całkiem nowe umiejętności zwiększa się atrakcyjność doświadczonego pracownika. Są to między innymi kreatywne myślenie, zorientowanie na cel, odporność...
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Quantification of methadone and its metabolites: EDDP and EMDP determined in autopsy cases using LC‐MS/MS
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Levels of 13 multi-class pesticide residues in Polish honeys determined by LC-ESI-MS/MS
PublicationLevels of 13 pesticides in 40 honey samples form Poland are reported. A rapid and sensitive method was developed for the LC-ESI-MS/MS determination of multi-class pesticide residues in honey samples. Liquid-liquid extraction (LLE) on a diatomaceous earth support (requiring the use of small amounts of organic solvent), followed by chromatographic separation on a C18 column and gradient elution were employed. The method quantifies...
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An LC-MS/MS Method for a Comprehensive Determination of Metabolites of BTEX Anaerobic Degradation in Bacterial Cultures and Groundwater
PublicationBTEX (benzene, toluene, ethylbenzene, and the different xylene isomers), known for carcinogenic and neurotoxic effects, are common environmental contaminants. The first step for the development of the bioremediation technologies is the detection of intense microbial degradation in contaminated waters in the quest for the most active bacterial strains. This requires the multispecies analysis for BTEX metabolites which are considered...
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Analysis of bisphenols and their derivatives in infant and toddler ready-to-feed milk and powdered milk by LC MS/MS
PublicationReady-to-feed milk and powdered milk packed in different types of packaging lined with resin are chosen as the primary or complementary diet for infants and toddlers. An HPLC–MS/MS method was established and validated for the determination of nineteen bisphenols and their derivatives in such samples. The recoveries were from 31% to 120%, while the values of limit of detection and quantification were in the range of 0.24–0.40 and...
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Speed Sensorless AC Drive with Inverter LC Filter and Fault Detection Using Load Torque Signal
PublicationThe industrial development in recent years has seen a major increase in the use of induction motors, whereby the cost has to be as low as possible and the lifetime as long as possible. To follow up this desire, investigations in this area have become very intense. For that reason, this paper presents a solution for driving an induction motor and simultaneous fault detection with no need for additional sensors. In order to achieve...
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Jarosław Guziński prof. dr hab. inż.
PeopleJaroslaw Guzinski received M.Sc., Ph.D. and D.Sc. degrees from the Electrical Engineering Department at Technical University of Gdansk, Poland in 1994, 2000 and 2011 respectively. Since 2016 he is Associate Professor at Gdansk University of Technology. Currently he is the head of the Department of Electric Drives and Energy Conversion. From 2006 to 2009 he was involved in European Commission Project PREMAID Marie Curie, ‘Predictive...
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Zastosowanie funkcji kształtu elementu skończonego w modulacji szerokości impulsów na przykładzie modulacji dwufazowej z kompensacją napięcia niezrównoważenia w trójpoziomowym falowniku napięcia 3l-NPC
PublicationPrzedstawiono problem modulacji napięcia jako problem wyznaczania współrzędnych punktu figury lub bryły geometrycznej. Do wyznaczenia współczynników wypełnień w modulacji szerokości impulsów zastosowano funkcje kształtu elementu skończonego. Wskazano zalety takiego podejścia i możliwości uogólnienia algorytmu modulacji. Opisano algorytm modulacji dwufazowej SVPWM z kompensacją oscylacji napięcia niezrównoważenia z jednoczesną stabilizacją...
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DLC coating doped with W in ring-on-ring sliding with water lubrication 20MPa/0.1m/s
Open Research DataWear tests in sliding friction of 1% W (tungsten) doped DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 20MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was...
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DLC coating doped with W in ring-on-ring sliding with water lubrication 10MPa/0.1m/s
Open Research DataWear tests in sliding friction of 1% W (tungsten) doped DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 10MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was...
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Zastosowanie chromatografii cieczowej w odwróconym układzie faz (RP-LC) w rozdzielanie i oznaczaniu polifenoli i naftochinonów w materiałach roslinnychreversed = Phase liquid chromatography (RP-LC) for separation and quantitative determination of polyphenols and naphtoquinones in plant materials
PublicationW pracy przedstawiono przegląd metod rozdzielania i oznaczania naftochinonów i polifenoli pochodzących z materiału roślinnego, z wykorzystaniem technik chromatograficznych w układzie faz odwróconych - RP-TLC (Reversed-Phase Thin Layer Chromatography) oraz RP-HPLC (Reversed-Phase High Performance Liquid Chromatography). Przeanalizowano procedury przygotowania próbki, etap rozdzielania, a także kontroli czystości zbieranych frakcji....
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Oil removal from polluted soil by washing with surfactants solutions in dynamic conditions
PublicationFor washing of the oil from polluted soil surfactants solutions were applied. In a research a nonionic synthetic surfactant - polyoxyethylene ether of synthetic fatty alcohol (Rokanol NL6), rhamnolipid biosurfactant JBR 425 (Jeneil Biosurfactant Co. LLC) and their mixtures were used. Results of oil removal from peat soil and sand with mixtures of surfactants solutions at concentration 0,5 g/dm...
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Lipidomic characteristics of three edible cold-pressed oils by LC/Q-TOF for simple quality and authenticity assurance
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Suppression of Supply Current Harmonics of 18-Pulse Diode Rectifier by Series Active Power Filter with LC Coupling
PublicationThe reported research aims at improving the quality of three-phase rectifier supply currents. An effective method consists of adding properly formed booster voltages to the fundamental supply voltages using a series active filter. In the proposed solution, the booster voltages are generated by three single-phase systems consisting of inverters, LC filters, and single-phase transformers. The application of LC couplings ensures low...
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Enzymatyczne przeestryfikowanie oleju rzepakowego kwasem kaprynowym w układzie reakcyjnym o minimalnej zawartości wody
PublicationOpisano wyniki badań nad wbudowywaniem się kwasu kaprynowego w triacylogli-cerole (TAG) oleju rzepakowego w procesie enzymatycznego przeestryfikowania, prowadzonego w obecności małej ilości wody. Katalizatorem procesu był sn-1,3 specyficzny enzym lipolityczny, Lipozyme IM. Parametrem zmiennym był czas reakcji. Produkty przeestryfikowania analizowano stosując technikę chromatografii kolumnowej, TLC i GLC oraz hydrolizę enzymatyczną...
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Stopniowa chromatografia cienkowarstwowa w normalnych układach faz (NP-TLC), jako technika rozdzielania i oceny składu grupowego frakcji asfaltenowych z utleniania pozostałości próżniowej ropy naftowej
PublicationW pracy opisano wyniki badań nad opracowaniem metodyki oceny składu grupowego i czystości frakcji asfaltenowych techniką chromatografii cienkowarstwowej w normalnych układach faz (NP-TLC). Skupiono się na doborze takich parametrów/warunków rozdzielania, jak stężenie i masa próbki, a także skład i kolejność eluentów stosowanych podczas rozwijania chromatogramów TLC. Zastosowana trój-stopniowa metodyka polega na nałożeniu 5 µL frakcji...
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DLC coating in ring-on-ring sliding with saline solution (0.9% wt.) lubrication 20MPa/0.1m/s
Open Research DataWear tests in sliding friction of DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 20MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9% wt.). Tribometer: PT-3. Overall test time >15h. The test was augmented...
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DLC coating in ring-on-ring sliding with saline solution (0.9% wt.) lubrication 10MPa/0.1m/s
Open Research DataWear tests in sliding friction of DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 10MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9% wt.). Tribometer: PT-3. Overall test time >15h. The test was augmented...