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Wyniki wyszukiwania dla: characterization
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An Overview of Several Inhibitors for Alzheimer’s Disease: Characterization and Failure
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Visualization and characterization of prolamellar bodies with atomic force microscopy
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Nanostructure characterization of (SmS)1.19TaS2 by means of STM/STS
PublikacjaW publikacji przedstawiono badania za pomocą techniki STM i STS powierzchni kryształów warstwowego związki typu misfit(SmS)1.19TaS2. Badania pozwalają sądzić, że powierzchniową warstwą jest warstwa Sm-S.
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Wide range of properties of polyurethanes for medicine - characterization of biomaterials
PublikacjaW artykule opisano różnorodność poliuretanów stosowanych na polu biomedycznym. Wyrózniono mtody otrzymywania materiałów o róznych własciwościach, a tym samym zastosowaniach. Opisano 10 serii potrzymanych PU oraz wyniki charakterystyki fizycznej, powierzchniowej i biologicznej tych poliuretanów.
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Preparation and characterization of TiO2 nanostructures for catalytic CO2 photoconversion
PublikacjaThe titanium dioxide target (99.7%) of 1 cm in dia was ablated in vacuum by laser pulses(6 ns) at 266 nm and at repetition rate of 10 Hz. During deposition the laser fluence between 1 and 3.5 J/cm2 and the O2 pressure from the range of 10-2 - 1 Pa were applied. The thin TiO2 films were deposited on glass substrate (1 × 1 cm2) heated up to 500 °C. The chemical composition of the film and samples produced by annealing were investigated...
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Densimetric and ultrasonic characterization of urea and its derivatives in water
PublikacjaW oparciu o pomiary gęstości dla serii roztworów jak i rozpuszczalnika wykonanych w temperaturach 15, 20, 25, 30 i 35oC wyznaczono pozorne molowe objętości mocznika, N-metylomocznika, N,N'-dimetylomocznika, N,N,N',N'-tetrametylomocznika, N-etylomocznika, N,N'-dietylomocznika jak i N-butylomocznika w wodzie. Dodatkowe pomiary szybkości dźwięku przeprowadzone w temperaturze 25oC pozwoliły obliczyć ściśliwości adiabatyczne, pozorne...
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Preparation and characterization of rigid polyurethane -polyglycerol nanocomposite foams
PublikacjaThis work reports on the preparation of polyurethane–polyisocyanurate (PUR–PIR) foams containing different polyglycerols and layered silicate nanoclays. The rigid polyurethane foams were obtained in a laboratory scale, in a single step method, from a two-component system with a NCO to OH groups ratio equal to two. The reaction mixture consisted of the proper amounts of a commercial oligoetherpolyol, polyglycerol, catalysts, water,...
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Novel Biomass-Based Polymers: Synthesis, Characterization, and Application
PublikacjaA wide range of polymers were prepared from biomass-derivatives, using different polymerization mechanisms. Well-defined, fully hydroxy-functional polyesters based on aliphatic diols were synthesized, using either conventional metal-based catalysts or the organic superbase 1,5,7-triazabicyclododecene (TBD). Unsaturated polyesters were also made, offering additional functionality to these biobased resins. Metal-catalyzed or enzymatic...
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Characterization of novel trehalose synthase from Deinococcus geothermalis.
PublikacjaThe method of trehalose extraction from yeast or othernatural sources is unsuitable for industrial production becauseof its low yield and high cost. Thus, the trehalose synthesizingenzyme systems that originated from a few microorganisms have been investigated.
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Analysis and characterization of coordination compounds by resonance Raman spectroscopy
PublikacjaResonance Raman spectroscopy has become a powerful tool to study excited-state geometries, excited-state charge distributions and photoinduced reaction dynamics in coordination compounds. Due to their rich photophysical properties coordination compounds are utilized for a variety of applications ranging from DNA sensing to photocatalysis. This review features recent applications of various resonance Raman scattering techniques...
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Characterization of recombinant homocitrate synthase from Candida albicans
PublikacjaLYS21 and LYS22 genes from Candida albicans encoding isoforms of homocitrate synthase (HCS), an enzyme catalyzing the first committed step in the L-lysine biosynthetic pathway, were cloned and expressed as NoligoHistagged fusion proteins in Escherichia coli. The purified gene products revealed HCS activity, i.e. catalyzed the condensation of α-ketoglutarate with acetyl-coenzyme A to yield homocitrate. The recombinant enzymes were purified...
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Characterization of the Functionally Graded Shear Modulus of a Half-Space
PublikacjaIn this article, a method is proposed for determining parameters of the exponentialy varying shear modulus of a functionally graded half-space. The method is based on the analytical solution of the problem of pure shear of an elastic functionally graded half-space by a strip punch. The half-space has the depth-wise exponential variation of its shear modulus, whose parameters are to be determined. The problem is reduced to an integral...
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CHARACTERIZATION STUDY ON MECHANICAL PROPERTIES OF POLYESTER COATED FABRIC
PublikacjaThe scope of the paper is to determine the mechanical properties of the Precontraint 1302 polyester coated fabric under uniaxial and biaxial tensile tests. The results are compared for Precontraint 1302 fabric and other types of coated fabrics. The author applied an orthotropic model and a dense net model to reflect the polyester coated fabric performance under uniaxial and biaxial tensile tests. Material parameters are specified...
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Application of Impedance Spectroscopy for Bi1−xNdxFeO3 Ceramics Characterization
PublikacjaIn the present paper the synthesis conditions for fabrication of Bi1−xNdxFeO3 ceramics are reported. The single phase polycrystalline samples of Bi1−xNdxFeO3 were prepared by standard solid state reaction method from the mixture of oxides viz.: Bi2O3, Fe2O3 and Nd2O3. The samples were characterized by impedance spectroscopy in the frequency range 10Hz – 1MHz at room temperature.
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SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF NIOBIUM-DOPED HYDROXYAPATITE CERAMICS
PublikacjaHydroxyapatite (HAp) ceramic materials are considered as one of the most promising implant materials in bone surgery and in dentistry. They exhibit unique biocompatibility, bioactivity, and osteoconductivity, which are the most desirable biomaterial features. However, HAp itself is brittle, has low strength, high degree of crystallinity and low solubility at physiological pH. Doping synthetic HAp with metal ions plays an important...
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Mid-infrared spectroscopy for characterization of Baltic amber (succinite)
PublikacjaNatural Baltic amber (succinite) is the most appreciated fossil resin of the rich cultural traditions dating back to prehistoric times. Its unequivocal identification is extremely important in many branches of science and trades including archeology, paleontology, chemistry and finally mineralogical and gemological societies. Current methods of modification of natural succinite are more and more sophisticated making the identification...
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Porous structure of clinoptilolite and problems connected with its characterization.
PublikacjaPrzedstawiono: stan wiedzy nt technik oznaczania porowatości i powierzchni właściwej różnego typu materiałów, oraz wyniki badań fizykochemicznych naturalnych zeolitów pochodzących z obszaru Zakarpacia (Ukraina).
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Design of low noise preamplifers for characterization of LSCO bolometers
PublikacjaW artykule przedstawiono wymagania stawiane układom do pomiaru szumów bolometrów. Ze względu na niski poziom mierzonych szumów układy te wymagają zastosowania niskoszumnych przedwzmacniaczy i układów ustalających punkt pracy badanych detektorów. Omówiono konstrukcje dwóch przedwzmacniaczy z zintegrowanymi układami polaryzacji. Przedstawiono wyniki pomiarów szumów w zakresie częstotliwości 10-90Hz. Przedstawiono możliwości ulepszenia...
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Synthesis and Characterization of Poly(zwitterionic) Structures for Energy Conversion and Storage
PublikacjaZwitterions are unique class of molecules that possess two functional groups bearing electric charges, one positive and second negative. This setup results in peculiar properties such as high water retention and anti-fouling capability. Therefore, zwitterionic coatings and gels are commonly applied in e.g. biosensing and bioelectronic devices. Despite those applications, there are other perspectives for zwitterionic materials....
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New Complementary Resonator for Permittivity- and Thickness-Based Dielectric Characterization
PublikacjaThe design of high-performance complementary meta-resonators for microwave sensors featur-ing high sensitivity and consistent evaluation of dielectric materials is challenging. This paper presents the design and implementation of a novel complementary resonator with high sensi-tivity for dielectric substrate characterization based on permittivity and thickness. A comple-mentary crossed arrow resonator (CCAR) is proposed and integrated...
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Growth, Crystal Structure and Magnetic Characterization of Zn-Stabilized CePtIn4
PublikacjaThe growth and characterization of CePtIn4, stabilized by 10% Zn substitution for In, is reported. The new material is orthorhombic, space group Cmcm (No. 63), with lattice parameters a = 4.51751(4) Å, b = 16.7570(2) Å, and c = 7.36682(8) Å, and the refined crystal composition has 10% of Zn substituted for In, i.e., the crystals are CePt(In0.9Zn0.1)4. Crystals were grown using a self-flux method: only growths containing Zn yielded...
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Graphene-based Silicone rubber Nanocomposites: Preparation, Characterization, and Properties
PublikacjaThis study aims to understand better the mechanical, thermal, and tribological behavior of silicone rubber nanocomposites. Graphite, exfoliated graphite, reduced graphene oxide, ionic liquid modified graphene oxide, silane-modified graphene oxide, fumed silica, and other fillers were used in this study. Adding graphene-based fillers to the silicone rubber matrix substantially improves the nanocomposite's mechanical, thermal, and...
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Electromagnetic characterization of a silver nanowire grating embedded into a dielectric slab
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Applying of the optical time-of-flight spectroscopy for the paper and pulp characterization
PublikacjaW pracy przedstawiono korzyści wykorzystania optycznej spektroskopii czasu przelotu w badaniach papieru i miazgi drzewnej. Przedmiotem badań były różne gatunki papieru oraz miazgi drzewnej (bez obróbki cieplnej, po obróbce cieplnej lub po obróbce chemicznej). W pomiarach wykorzystano półprzewodnikowe lasery impulsowe oraz w charakterze fotoodbiorników kamerę smugową lub licznik fotonów.
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Characterization of low-dose doxorubicin-loaded silica-based nanocomposites
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Preparation and characterization of TiO2/carbon nanowall composite on a transparent substrate
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Development and Characterization of Bioactive Polypropylene Films for Food Packaging Applications
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Biochemical and Structural Characterization of SplD Protease from Staphylococcus aureus
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The progress in characterization of polyurethanes morphology with different microscopic methods----WYJAŚNIĆ-----
PublikacjaW pracy opisano wyniki badań dotyczące analizy morfologii poliuretyanów określanej różnymi metodami. Omówiono mikroskopię optyczną, elektronową, mikroskopię termiczną, mikroskopię fluoroscencyjną, mikro-Ramana i mikroskopię sił atomowych.
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Growth and characterization of chalcopyrite nanocrystals: beyond conventional thin films
PublikacjaPrzedstawiona została sucha metoda wytwarzania na podłożach stałych kryształów chalkopirytu zawierających miedź z wykorzystaniem prekursorów metalicznych. Dzięki odpowiedniemu doborowi parametrów nakładania otrzymano zarówno nanokryształy oraz polikrystaliczne struktury submikronowe jak i makroskopowe klastry. Zamieszczona została charakterystyka wytworzonych materiałów otrzymana techniką mikroskopii skaningowej.
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Characterization of a cryptic plasmid pSFKW33 from Shewanella sp. 33b
PublikacjaA cryptic plasmid pSFKW33 from psychrotrophic bacterium Shewanella sp. 33B, an isolate from the Gulf of Gdansk (the Baltic Sea), was sequenced and characterized. It is an 8021 bpcircular molecule with 38% GC content, which shows a distinctive nucleotide sequence without homology to other known plasmids. The nucleotide sequence analysis predicts eight open reading frames. The deduced amino acid sequence of ORF-1 shared significant...
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Pitting corrosion characterization by electrochemical noise measurements on asymmetric electrodes
PublikacjaKorozja wżerowa stali nierdzewnych może być wykryta za pomocą obserwacji charakterystycznych sygnałów prądowych, jakie płyną między dwiema elektrodami metalowymi. W artykule proponuje się wyznaczanie funkcji bispektrum dla układu dwóch elektrod o istotnie różnej powierzchni narażonej na występowanie korozji. Proponowana metoda została zastosowana do analizy korozji wżerowej stali 0H18N9 powstającej pod wpływem 1M roztworu FeCl3...
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Preparation and Surface Characterization of Chitosan-Based Coatings for PET Materials
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Reduced graphene oxide and inorganic nanoparticles composites – synthesis and characterization
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Thermal and Electrical Characterization of the Carbon Nanofibers Based Cement Composites
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Physicochemical and photocatalytic characterization of mesoporous carbon/titanium dioxide spheres
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Photoelectrochemical and thermal characterization of aromatic hydrocarbons substituted with a dicyanovinyl unit
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Characterization of the natural chemical and osmotic environment of early wheat embryogenesis
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Microwave solvothermal synthesis and characterization of manganese-doped ZnO nanoparticles
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Copolyester-coated mineral fertilizers – preparation, characterization, and nutrient release
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Synthesis and Characterization of Magnetic Nanomaterials with Adsorptive Properties of Arsenic Ions
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Identification and characterization of Staphylococcus spp. and their susceptibility to insect apolipophorin III
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Characterization of NiTi SMA in its unusual behaviour in wear tests
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Ziziphora taurica subsp. taurica: Analytical Characterization and Biological Activities
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Slow growth conservation and molecular characterization of Deutzia scabra Thunb
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Preparation and physicochemical characterization of ceramic supports for supported liquid membranes
PublikacjaImmobilizowane membrany ciekłe stały się przedmiotem intensywnych badań w ostanich latach, głównie w procesach oczyszczania strumieni gazowych. Kluczowym czynnikiem mającym wpływ na efektywność tych procesów ma czas życia układu membranowego, a zatem odpowiedni dobór nośnika i fazy membranowej. W porównaniu do nośników polimerowych, ceramiczne charakteryzują się większą grubością, jednak są bardziej stabilne termicznie. Praca...
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Fabrication and characterization of anode supported solid oxide fuel cells
PublikacjaW tej pracy, napylanie aerozolowe zawiesiny proszków jest oceniane jako metoda osadzania cienkich elektrolitów tlenkowych ogniw paliwowych. Metoda ta jest tania, prosta i mam zalety w stosunku do szeroko stosowanej metody sitodruku. Wpływ parametrów osadzania: stężenie zawiesiny, ciśnienie robocze są w artykule omawiane.
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Characterization of structural, thermal and mechanical properties of bismuth silicate glasses
Publikacjahe influence of heating and reduction processes on the structural, thermal and mechanical properties of bismuth-silicate glasses has been investigated. Two compositions of glasses: 40Bi2O3–60SiO2 (Bi0.57Si0.43Ox) and 27Bi2O3–73SiO2 (Bi0.43Si0.57Ox) were fabricated by a typical melt quenching technique. Then the reduction in hydrogen at 380 °C for 20, 42 or 67 h was performed. It was found that a 50 μm-thick layer was formed on...
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Characterization of Defects Inside the Cable Dielectric With Partial Discharge Modeling
PublikacjaThe continuous monitoring of power system devices is an important step toward keeping such capital assets safe. Partial discharge (PD)-based measurement tools provide a reliable and accurate condition assessment of power system insulations. It is very common that voids or cavities exist in every solid dielectric insulation medium. In this article, different voids are modeled and analyzed using an advanced finite element (FE)-based...
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Preparation and Characterization of Films Based on Disintegrated Bacterial Cellulose and Montmorillonite
PublikacjaThe food packaging materials from natural polymers including polysaccharides offer an ecologically important alternative to commonly used synthetic, non-biodegradable counterparts. The purpose of this work was to modify of bacterial cellulose (BC) leading to the improvement of its functional properties in terms of use as a food packaging material. Effects of disintegration of BC and addition of montmorillonite (MMT) on its water...