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Wyniki wyszukiwania dla: size exclusion chromatography
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Novel liquid chromatography method based on linear weighted regression for the fast determination of isoprostane isomers in plasma samples using sensitive tandem mass spectrometry detection
PublikacjaA simple, fast, sensitive and accurate methodology based on a LLE followed by liquid chromatography–tandem mass spectrometry for simultaneous determination of four regioisomers (8-iso prostaglandin F2α, 8-iso-15(R)-prostaglandin F2α, 11β-prostaglandin F2α, 15(R)-prostaglandin F2α) in routine analysis of human plasma samples was developed. Isoprostanes are stable products of arachidonic acid peroxidation and are regarded as the...
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The clamping selection method to reduce the vibration of large-size workpieces during the face milling process
PublikacjaThe article introduces a method for selecting the best clamping conditions to obtain vibration reduction during milling of large-size workpiece. It is based on experimental modal analysis performed for a set of assumed, fixing conditions of a considered workpiece to identify Frequency Response Functions (FRFs) for each tightening torque of the mounting screws. Simulated plots of periodically changing nominal cutting forces are...
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Multi-Criteria Optimization for Fleet Size with Environmental Aspects
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Floe-size distributions in laboratory ice broken by waves
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Floe-size distributions in laboratory ice broken by waves
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Floe-size distributions in laboratory ice broken by waves
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Floe-size distributions in laboratory ice broken by waves
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Country selection strategies based on value, size and momentum
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Oil refinery dusts: morphological and size analysis by TEM
PublikacjaThe objectives of this work were to develop a means of sampling atmospheric dusts on the premises of an oil refinery for electron microscopic study to carry out preliminary morphological analyses and to compare these dusts with those collected at sites beyond the refinery limits. Carbon and collodion membranes were used as asupport for collection of dust particles straight on transmission electron microscopy (TEM) grids. Micrographs...
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Carrot root size distribution in response to biostimulant application
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Size Reduction of Microwave Couplers by EM-Driven Optimization
PublikacjaThis work addresses simulation-driven design optimization of compact microwave couplers that explicitly aims at circuit footprint area reduction. The penalty function approach allows us to minimize the area of the circuit while ensuring a proper power division between the output ports and providing a sufficient bandwidth with respect to return loss and isolation around the operating frequency. Computational cost of the optimization...
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Broadband Microstrip Patch Antenna with Reduced Transversal Size
PublikacjaW pracy przedstawiono propozycję anteny szerokopasmowej o ograniczonych wymiarach poprzecznych. Szerokopasmowość uzyskano poprzez stosowanie grubego podłoża i sprzężenia elektromagnetycznego poprzez dwie szczeliny sprzęgające. Wymiar poprzeczny łaty zredukowano poprzez zastosowanie szczeliny typu H. Antena została zaprojektowana i wykonana, zaś zmierzone pasmo wyniosło 29% dla WFS <1.5. Stwierdzono jednak, że charakterystyki...
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Universal construction of genuinely entangled subspaces of any size
PublikacjaWe put forward a simple construction of genuinely entangled subspaces – subspaces supporting only genuinely multipartite entangled states – of any permissible dimensionality for any number of parties and local dimensions. The method uses nonorthogonal product bases, which are built from totally nonsingular matrices with a certain structure. We give an explicit basis for the constructed subspaces. An immediate consequence of our...
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Influence on micrograins size on the distance between the workpiece and the lap.
PublikacjaNa kształtowanie powierzchni docieranej główny wpływ ma błąd kształtu zastosowanego narzędzia. Intensywność docierania zależy od wielkości zastosowanych ziaren ściernych, które również wpływają na błędy kształtu przedmiotu. W referacie przedstawiono wyniki obliczeń odległości przedmiotu od powierzchni narzędzia w funkcji wielkości ziaren ściernych.
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Thermal degradation assessment of canola and olive oil using ultra-fast gas chromatography coupled with chemometrics
PublikacjaOil blending is often used to enhance the properties of vegetable oils. The admixture of a more thermally stable oil makes the resulting blend more suitable for use in frying. A new method of quality assessment of vegetable oils used in frying is presented in this paper. In this method, ultra-fast gas chromatography coupled with flame ionization detector and chemometrics is employed. Principal component analysis was used for data...
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Estimation of object size in the calibrated camera image = Estymacja rozmiaru obiektów w obrazach ze skalibrowanej kamery
PublikacjaIn the paper, a method of estimation of the physical sizes of the objects tracked by the camera is presented. First, the camera is calibrated, then the proposed algorithm is used to estimate the real width and height of the tracked moving objects. The results of size estimation are then used for classification of the moving objects. Two methods of camera calibration are compared, test results are presented and discussed. The proposed...
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FE analysis of a coupled energetic-statistical size effect in plain concrete beams with varying material properties.
PublikacjaThe numerical FE investigations of a coupled energetic-statistical size effect in unnotched concrete beams of similar geometry under quasi-static three point bending were performed within elasto-plasticity with non-local softening. The stochastic FE analyses were carried out with three different beam sizes. Deterministic calculations were performed with the uniform distribution of a uniaxial tensile strength. In statistical calculations...
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Study of pH and temperature effect on lipophilicity of catechol-containing antioxidants by reversed phase liquid chromatography
PublikacjaLipophilicity of selected antioxidant phytochemicals, including flavonoids, phenolic acids and xanthonoids, was determined by reversed phase high performance liquid chromatography with UV detection (RP-HPLC-UV). The analyses run at different temperature and pH conditions in isocratic mode suggested that lipophilicity as distribution coefficient (logD) between aqueous and organic phase decreases with increasing temperature. For...
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Using pattern recognition entropy to select mass chromatograms to prepare total ion current chromatograms from raw liquid chromatography–mass spectrometry data
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A new silylating reagent – dimethyl(3,3,3-trifluoropropyl)silyldiethylamine – for the derivatisation of non-steroidal anti-inflammatory drugs prior to gas chromatography–mass spectrometry analysis
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Investigation of Wood Flour Size, Aspect Ratios, and Injection Molding Temperature on Mechanical Properties of Wood Flour/Polyethylene Composites
PublikacjaIn the present research, wood flour reinforced polyethylene polymer composites with a coupling agent were prepared by injection molding. The effects of wood flour size, aspect ratios, and mold injection temperature on the composites’ mechanical properties were investigated. For the preparation of the polymer composites, five different formulations were created. The mechanical properties including tensile strength and the modulus,...
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Gas chromatography-olfactometry (GC-O), electronic noses (e-noses) and electronic tongues (e-tongues) for in vivo food flavour measurement
PublikacjaThe capter revies two types of artificial olfaction instrumentation, i.e. gas-chromatography-olfactometry (GC-O) and chemical sensor technologies (electronic nose and tongue), combined with multivariate data processing methods as promising approaches for rapid analysis of food. The chapter also includes examples of specific applications for the detection of food flavour and volatile components.
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Size effect in concrete beams under bending – influence of the boundary layer and the numerical description of cracks
PublikacjaIn the paper the size effect phenomenon in concrete is analysed. The results of numerical simulations of using FEM on geometrically similar un-notched and notched concrete beams under bending are presented. Concrete beams of four different sizes and five different notch heights under three-point bending test were simulated. In total 18 beams were analysed. Two approaches were used to describe cracks in concrete. First, eXtended...
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Explicit Size-Reduction-Oriented Design of a Compact Microstrip Rat-Race Coupler Using Surrogate-Based Optimization Methods
PublikacjaIn this paper, an explicit size reduction of a compact rat-race coupler implemented in a microstrip technology is considered. The coupler circuit features a simple topology with a densely arranged layout that exploits a combination of high- and low-impedance transmission line sections. All relevant dimensions of the structure are simultaneously optimized in order to explicitly reduce the coupler size while maintaining equal power...
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A method of predicting the best conditions for large-size workpiece clamping to reduce vibration in the face milling process
PublikacjaThe paper presents an innovative method of solving the problem of vibration suppression during milling of large-size details. It consists in searching for the best conditions for clamping the workpiece based on a rapid modal identification of the dominant natural frequencies only and requires repetitive changes in the tightening torque of the clamping screws. Then, by estimating the minimum work of the cutting forces acting in...
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Application of gas chromatography–tandem mass spectrometry for the determination of amphetamine-type stimulants in blood and urine
PublikacjaAmphetamine, methamphetamine, phentermine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), and 3,4-methylenedioxy-N-ethylamphetamine (MDEA) are the most popular amphetamine-type stimulants. The use of these substances is a serious societal problem worldwide. In this study, a method based on gas chromatography-tandem mass spectrometry (GC-MS/MS) with simple and rapid liquid-liquid extraction (LLE)...
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Authenticity Assessment of the "Onisiówka" Nalewka Liqueurs Using Two-Dimensional Gas Chromatography and Sensory Evaluation
PublikacjaThe “Onisiówka” nalewka liqueur is a regional Polish alcoholic beverage, which is inscribed on the list of regional and traditional products of the Ministry of Agriculture and Rural Development in Poland. It is produced from multiflower honey, black elderberry flower syrup, and spirit. Due to fact that the “Onisiówka” nalewka liqueur has never been investigated, these studies are the foundation for further work on this regional...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublikacjaHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Long-Term Impact of Wind Erosion on the Particle Size Distribution of Soils in the Eastern Part of the European Union
PublikacjaWind erosion is the leading cause of soil degradation and air pollution in many regionsof the world. As wind erosion is controlled by climatic factors, research on this phenomenon isurgently needed in soil and land management in order to better adapt to climate change. In thispaper, the impact of wind erosion on the soil surface in relation to particle size distribution wasinvestigated. Changes in percentage of sand, silt and...
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Patch size setup and performance/cost trade-offs in multi-objective antenna optimization using domain patching technique
PublikacjaA numerical study concerning multi-objective optimization of antenna structures using sequential domain patching (SDP) technique has been presented. We investigate the effect of various setups of the patch size on the operation of the SDP algorithm and possible trade-offs concerning the quality of the Pareto set found by SDP and the computational cost of the optimization process. Our considerations are illustrated using a UWB monopole...
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Rapid determination of multiple aminoglycoside antibiotics in veterinary formulations by ion-pair chromatography coupled with evaporative light scattering detection
PublikacjaA fast and simple method for simultaneous determination of eight aminoglycoside antibiotics using ion-pairing liquid chromatography (IPLC) coupled with evaporative light scattering detection (ELSD) has been developed and validated. Separation of amikacin, apramycin, gentamicin (as a sum of gentamicin C1, C2 and C1A), kanamycin A, neomycin B, paromomycin, streptomycin and tobramycin was achieved using C18 column with H2O and MeOH/acetone,...
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Calixarenes as stationary phases in High Performance Liquid Chromatography
PublikacjaPraca przeglądowa przedstawia dotychczasowe metody syntezy faz stacjonarnych na bazie pochodnych kaliksarenów, kaliksrezorcyarenów i kalikspiroli chemicznie ziązanych z żelem krzemionkowym lub dynamicznie na nim obsadzonych. Podsumowano zastosowanie tych faz w rozdzielaniu szeregu klas związków organicznych i nieorganicznych metodą wysokosprawnej chromatografii cieczowej.
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Identification of acrylate copolymers using pyrolysis and gas chromatography
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On Decision-Making Strategies for Improved-Reliability Size Reduction of Microwave Passives: Intermittent Correction of Equality Constraints and Adaptive Handling of Inequality Constraints
PublikacjaDesign optimization of passive microwave components is an intricate process, especially if the primary objective is a reduction of the physical size of the structure. The latter has become an important design consideration for a growing number of modern applications (mobile communications, wearable/implantable devices, internet of things), where miniaturization is imperative due to a limited space allocated for the electronic circuitry....
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Inverse modeling for fast design optimization of small-size rat-race couplers incorporating compact cells
PublikacjaIn the paper, a framework for computationally-efficient design optimization of compact rat-race couplers (RRCs) is discussed. A class of hybrid RRCs with variable operating conditions is investigated, whose size reduction is obtained by replacing ordinary transmission lines with compact microstrip resonant cells (CMRCs). Our approach employs a bottom-up design strategy leading to the development of compact RRCs through rapid design...
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Development of an Analytical Protocol for Determination of Cyanide in Human Biological Samples Based on Application of Ion Chromatography with Pulsed Amperometric Detection
PublikacjaA simple and accurate ion chromatography (IC) method with pulsed amperometric detection (PAD) was proposed for the determination of cyanide ion in urine, sweat, and saliva samples. The sample pretreatment relies on alkaline digestion and application of Dionex OnGuard II H cartridge. Under the optimized conditions, the method showed good linearity in the range of 1–100 μg/L for urine, 5–100 μg/L for saliva, and 3–100 μg/L for sweat...
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublikacjaA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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Body size and wing asymmetry in bees along an urbanization gradient
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The estimation of norwegian cod size distribution from acoustic data
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Potential of Mean Force of Hydrophobic Association: Dependence on Solute Size
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Risk-based explanation for the country-level size and value effects
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Tighter bounds on the size of a maximum P3-matching in a cubic graph
PublikacjaW pracy pokazano, że największe P3-skojarzenie dla dowolnego grafu o n>16 wierzchołkach składa się z przynajmniej 117n/152 wierzchołków.
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Feature type and size selection for adaboost face detection algorithm
PublikacjaThe article presents different sets of Haar-like features defined for adaptive boosting (AdaBoost) algorithm for face detection. Apart from a simple set of pixel intensity differences between horizontally or vertically neighboring rectangles, the features based on rotated rectangles are considered. Additional parameter that limits the area on which the features are calculated is also introduced. The experiments carried out on...
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Specific cutting resistance while sawing of wood - the size effect
PublikacjaW artykule przedstawiono wyniki analiz zmian właściwego oporu skrawania, przy zastosowaniu współczesnej mechaniki pękania z uwzględnieniem wiązkości. Analizy wykonano dla procesu przecinania drewna na pilarce ramowej PRW15M drewna jesionu i jesionu modyfikowanego termicznie. Zastosowane podejście pozwala na wyjaśnienie zjawiska wzrostu właściwego powierzchniowego oporu skrawania dla niewielkich grubości warstwy skrawanej jako efektu...
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Applications of compression techniques for reducing the size of multibeam sonar records
PublikacjaJednym z najczęściej używanych urządzeń służących do szeroko rozumianego telemonitoringu morskiego są sonary wielowiązkowe (ang. Multibeam systems - MBS). Ich wysoka wydajność w tworzeniu informacji o obiektach znajdujących się pod wodą skutkuje w dużych ilościach danych pozyskiwanych podczas rejsów badawczych i pomiarowych. W tym kontekście, proces przechowywania i zarządzania takim magazynem danych staje się istotnym problemem...
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Accelerometer-based Human Activity Recognition and the Impact of the Sample Size
PublikacjaThe presented study focused on the recognition of eight user activities (e.g. walking, lying, climbing stairs) basing on the measurements from an accelerometer embedded in a mobile device. It is assumed that the device is carried in a specific location of the user’s clothing. Three types of classifiers were tested on different sizes of the samples. The influence of the time window (the duration of a single trial) on selected activities...
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IFF/SSR rectangular patch antenna with reduced transversal size
PublikacjaW artykule przedstawiono antenę mikropaskową dla systemów IFF/SSR, zasilaną poprzez szczelinę typu H. Zastosowanie tego typu szczeliny pozwoliło na 36-procentową redukcję wymiaru poprzcznego anteny,co jest szczególnie istotne ze względu na potencjalne zastosowanie anteny w szykach.Pomierzone parametry eektryczne anteny to: VSWR < 1.5; stosunek polaryzacji ortogonalnej do właściwej < 30 dB w obu płaszczyznach;zysk > 7 dBi.
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Analysis of size and shape of abrasive micrograins in lapping of assembly joints
PublikacjaPrzedstawiono skomputeryzowana analizę wielkości i kształtu mikroziaren ściernych. W badaniach mikroziaren węglika boru, węglika krzemu i elektrokorundu zastosowano mikroskopie optyczna oraz specjalistyczne oprogramowanie MultiScan v.6.08
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Deterministic and statistical size effect during shearing of granular layer
PublikacjaArtykuł omawia deterministyczny i statystyczny efekt skali w materiałach granulowanych podczas ścinania cienkiej warstwy piasku między dwoma bardzo szorstkimi ścianami. Obliczenia wykonano metodą elementów skończonych na bazie mikropolarnego prawa hipoplastycznego. Pokazano wyniki efektu skali przy zastosowaniu różnych metod redukujących ilość realizacji pól losowych dla początkowego wskaźnika porowatości..
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FE-simulations of size effects in granular and quasi-brittle materials
PublikacjaW artykule przedstawiono symulacje efektów skali w materiałach granulowanych i kruchych. Obliczenia wykonano dla ściskania dwuosiowego i fundamentu w przypadku materiałów granulowanych oraz belek zginanych w przypadku materiałów kruchych. Do obliczeń wykorzystano mikropolarne prawo hipoplastyczne i sprężysto-plastyczne prawo z nielokalnym osłabieniem.