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Wyniki wyszukiwania dla: speech%20synthesis
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The new diphosphanylphosphido complexes of tungsten(VI) and molybdenum(VI). Their synthesis, structures and properties
PublikacjaWe report on the reactivity of R2P–P(Li)–PR’2 (R = tBu, iPr, R’ = NEt2, iPr) towards diimido complexes [(dippN)2MCl2·dme] (M = Mo, W and dipp = 2,6-iPr2C6H3). A series of new complexes with diphosphanylphosphido ligands R2P–P–PR’2 were isolated. The solid-state structures of [(dippN)2M(Cl)(1,2-η-iPr2P–P– PiPr2)] (2Mo and 2W) and [(dippN)2M(Cl){1,2-η-tBu2P–P–P(NEt2)2}] (3Mo and 3W) were established by single-crystal X-ray diffraction...
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A New Approach to Chemical Recycling of Polyamide 6.6 and Synthesis of Polyurethanes with Recovered Intermediates
PublikacjaA new efficient method for the chemical decomposition of polyamide 6.6 by the glycolysis and amino-glycolysis processes was proposed. The glycolysis was conducted using the mass excess of ethylene glycol (EG) as a decomposing agent in the presence of a catalyst. Also, a mixture of EG and triethylenetetramine was used as another decomposing agent in the amino- glycolysis process. The described process of decomposition did not...
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Solid-phase synthesis and characterization of N-acetylated Gly-His-Lys analogues
PublikacjaZaprezentowano nowe analogi tripeptydu Gly-His-Lys (GHK), stanowiącego sekwencję naturalnie występującą w -II-łańuchu kolagenu, skąd jest uwalniany w stanach zapalnych i w procesach gojenia się ran. Gly-His-Lys jest szeroko stosowany na rynku kosmetycznym w połączeniu z kwasem palmitynowym, który ułatwia jego wnikanie w głąb skóry. Zaplanowane modyfikacje zawierały fragment Gly-X-Y (X=Met, Hyp, Hyp-Met, Gly-Hyp; Y=Lys, D-Lys) i...
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Mariusz Specht
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Nuclear Magnetic Resonance data for the synthesis of esterase cleavable antifungal conjugates containing fatty acids as molecular carriers
Dane BadawczeNMR data for novel organic compounds - conjugates composed of C2-18 fatty acid (FA) residues as a molecular carrier and 5-fluorocytosine (5-FC) as an active agent, released upon the action of intracellular esterases on the ester bond between FA and “trimethyl lock” intramolecular linker.
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Tool Life and Process Dynamics in High Speed Ball End Milling of Hardened Steel
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More wood, less chips: an effect of the cirular saw's rim speed on the kerf width
PublikacjaWartości przemieszczeń poprzecznych piły tarczowej zależą od jej prędkości obrotowej. Wykazano, że podczas zmieniania predkości obrotowej piły wystepują obszary pracy, w których przemieszczenia piły są niewielkie. Wartości te moga być wykorzystywane do optymalizacji procesu cięcia, gdyż wystepuje ścisła zależność pomiędzy obrotami piły i wielkością rzazu. Badania prowadzono na typowej pilarce tarczowej przy cięciu drewna bukowego....
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The critical rotational speed of circular saw: simple measurement method and its practical implementations.
PublikacjaProducenci pił tarczowych są zobligowani do podawania ich dopuszczalnych prędkości obrotowych. Jednakże, umieszczane przez nich prędkości na piłach są często bliskie prędkościom krytycznym lub je przewyższają. Przecinanie takimi narzędziami może być więc niebezpieczne dla obsługującego. Praca przedstawia prostą metodologię wyznaczania prędkości obrotowych krytycznych pił tarczowych. Badania były prowadzone z wykorzystaniem technik...
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Novel adaptive flux observer for wide speed range sensorless control of induction motor
PublikacjaA new adaptive flux observer of induction motor is presented in the paper. The Lyapunov theory is utilized for derivation of the adaptation law of rotor flux angular speed, which acts as unknown parameter in an augmented induction motor model. In the field weakening region, where stray fluxes are comparable with rotor flux magnitude, the air-gap flux stabilization is proposed. An air-gap flux multiscalar model is derived for stator...
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FPGA realization of the high-speed residue-to-binary converter based on the Chinese Remainder Theorem
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Torque transmission diagnostic system for high-speed train using state-space observer
PublikacjaW artykule przedstawiono zagadnienie diagnostyki czujnika prędkości silnika i przekładni mechanicznej pociągu. W celach diagnostycznych zastosowano obserwatory stanu do obliczania prędkości obrotowej silnika i momentu obciążenia. Analiza chwilowych wartości obliczonej prędkości obrotowej oraz momentu obciążenia pozwala na diagnozowanie stanu układu transmisji momentu trakcyjnego. Zaprezentowano wyniki badań symulacyjnych i eksperymentalnych...
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FPGA realization of the high-speed residue-to-binary converter based on chinese remainder theorem
PublikacjaW pracy przedstawiono architekturę, realizację FPGA oraz symulację numeryczną na poziomie bitowym szybkiego konwertera z systemu resztowego do systemu binarnego dla modułów 5-bitowych opartego na chińskim twierdzeniu o resztach. Algorytm konwertera obejmuje obliczanie projekcji ortogonalnych poprzez odczyt pamięci oraz sumowanie modulo M realizowane dwustopniowo, pierwszy stopień oparty o sumatory CSA umożliwia redukcję do zakresu...
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Predictions of cutting power while sawing of birch and beech with the use of modern fracture mechanics
PublikacjaPraca zawiera wyniki badań eksperymentalnych procesu przecinania drewna brzozy i buka piłami o rzazie 2 mm na pilarce ramowej PRW15M. Na podstawie teoretycznego modelu Atkinsa, wyznaczono z danych eksperymentalnych stałe materiałowe (wiązkość i naprężenia tnące w strefie ścinania) i opracowano model do prognozowania mocy skrawania podczas przecinania drewna piłami na pilarce ramowej dla innych wartości rzazu w funkcji posuwu na...
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Contribution of Strength, Speed and Power Characteristics to Change of Direction Performance in Male Basketball Players
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Effect of Pendolino high-speed rail on the structure of buildings located the proximity of the railway tracks
PublikacjaThe following research focuses on the dynamic analysis of the impact of the high-speed train inducted vibrations on the structures located near railway tracks. The office complex chosen as the subject of calculations is located in the northern part of Poland, in Gdańsk, in the proximity of Pendolino, the high speed train route. The high speed trains are the response for the growing needs for more efficient railway system. However...
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Estimating the Average Speed of Public Transport Vehicles Based on Traffic Control System Data
PublikacjaIntelligent Transport Systems are a valuable source of traffic information, covering both private and public vehicles. The main problem, however, is that very few studies are conducted to determine the speed of buses, trams and trolleys in urban networks in relation to traffic conditions. The paper investigates how ITS systems data could be used to model the speed of Public Transport vehicles. This is now possible thanks to the...
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Experimental comparison of the transition speed of a hydrodynamic journal bearing lubricated with oil and magnetorheological fluid
PublikacjaA journal bearing test bench is used to find the transition speed between the hydrodynamic and mixed lubrication regimes for a modified magnetorheological (MR) fluid. It is shown that the transition speed of the bearing can be reduced by applying a local magnetic field near minimum film when it is lubricated with the MR fluid, and that this will only marginally increase friction. The lubricating performance of the MR fluid is compared...
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Effect of pine impregnation and feed speed on sound level and cutting power in wood sawing
PublikacjaThe sound levels along with the cutting power registered during the sawing process of the impregnated and non-impregnated pine wood at two feed speeds are shown and compared in this paper. Statistically significant differences in the acoustic signals occurred at the lower feed rate. The differences became smaller with an increase in the feed speed. In contrast to the sound signal, the differences...
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Speed Observer Structure of Induction Machine Based on Sliding Super-Twisting and Backstepping Techniques
PublikacjaThis paper presents an analysis of the two speed observer structures which are based on the backstepping and sliding super twisting approach. The observer stabilizing functions result from the Lyapunov theorem. To obtain the observer tuning gains the observer structure is linearized near the equilibrium point. The rotor angular speed is obtained from non-adaptive dependence. In the sensorless control system structure the classical...
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Effect of the Drying Method of Pine and Beech Wood on Fracture Toughness and Shear Yield Stress
PublikacjaThe modern wood converting processes consists of several stages and material drying belongs to the most influencing future performances of products. The procedure of drying wood is usually realized between subsequent sawing operations, affecting significantly cutting conditions and general properties of material. An alternative methodology for determination of mechanical properties (fracture toughness and shear yield stress) based...
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Non-Adaptive Rotor Speed Estimation of Induction Machine in an Adaptive Full-Order Observer
PublikacjaIn the sensorless control system of an induction machine, the rotor speed value is not measured but reconstructed by an observer structure. The rotor speed value can be reconstructed by the classical adaptive law with the integrator. The second approach, which is the main contribution of this paper, is the non-adaptive structure without an integrator. The proposed method of the rotor speed reconstruction is based on an algebraic...
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Impact of digital signal processing on FOC current feedback in high-speed PMSM drive
PublikacjaIn applications where size and weight of the electric motor are among major design concerns, Permanent Magnet Synchronous Motors (PMSMs) with wide operational speed-range are commonly preferred. Due to limited inverter switching frequency, high-speed operation of a drive results in a low ratio between the switching frequency and the fundamental frequency of motor voltage. Such operating conditions have been recently identified...
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The effect of the motor filters on earth fault current waveform in circuits with variable speed drives
PublikacjaIn circuits with variable speed drives distorted earth fault current flows. Earth fault current distortion influences the threshold of ventricular fibrillation. This paper presents earth fault current distortion in circuits with variable speed drives when motor filter is used. Two types of motor filter are analyzed. For every type of filter the effect of earth fault current distortion on ventricular fibrillation is evaluated.
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Immunity of residual current devices to the impulse leakage current in circuits with variable speed drives
PublikacjaThis paper concerns reliability of supply in variable speed drive circuits with residual current devices. During normal operation of these circuits high value of leakage current causes unwanted tripping of residual current devices. Immunity of residual current devices to the impulse leakage current should be evaluated. The system for testing of residual current devices and results of the test are presented
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The effect of the motor filters on earth fault current waveform in circuits with variable speed drives
PublikacjaIn circuits with variable speed drives distorted earth fault current flows. Earth fault current distortion influences the threshold of ventricular fibrillation. This paper presents earth fault current distortion in circuits with variable speed drives when motor filter is used. Two types of motor filter are analyzed. For every type of filter the effect of earth fault current distortion on ventricular fibrillation is evaluated.
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The impact of wind farms with fixed speed induction generators on grid damping in Northern Ireland
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Research and Analysis of High-Speed Data Transmission Radio Link Designed for Maritime Environment
PublikacjaIn these article, the realization of digital radio link for high-speed data transmission was presented. Its concept and practical realization, using USRP devices from National Instruments, were described. Developed software for generation and reception of digital signals in baseband, including description of modulation types, and time and frequency synchronization mechanisms, was presented. Moreover, an operation of designed radio...
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Research and analysis of high-speed data transmission radio link designed for maritime environment
PublikacjaIn these article the realization of digital radio link for high-speed data transmission was presented. Its concept and practical realization, using USRP devices from National Instruments, were described. Developed software for generation and reception of digital signals in baseband, including description of modulation types, and time and frequency synchronization mechanisms, was presented. Moreover, an operation of designed radio...
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DYNAMIC ANALYSIS OF THE RAILWAY BRIDGES IN POLAND WITH REGARDS TO HIGH-SPEED TRAINS PASSAGE ADJUSTMENT
PublikacjaThe dynamic analysis of the railway bridge in Tczew was carried out in the article as an example of such bridges adaptation suitability to handle high-speed trains. Calculations of railway bridges are greatly complicated and labor-consuming. The bridge model and a rolling stock passage simulation were developed in the SOFISTIK software. Three types of elements were used for the correct mapping of the structure in the calculation...
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The Experimental Determination of Bearings Dynamic Coefficients in a Wide Range of Rotational Speeds, Taking into Account the Resonance and Hydrodynamic Instability
PublikacjaMethods for the experimental determination of dynamic coefficients are commonly used for the analysis of various types of bearings, including hydrodynamic, aerodynamic and foil bearings. There are currently several algorithms that allow estimating bearing dynamic coefficients. Such algorithms usually use various excitation techniques applied to rotor–bearings systems. So far only a small number of scientific publications show how...
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Simulation and Synthesis in Medical Imaging
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Wind speed, wind direction and solar radiation datasets; wind and solar energy resources analysis
Dane BadawczeDataset contain the results of wind speed, wind direction and solar radiation for wind and solar energy resources analysis performed in years 2008 and 2009. Application for efficiency and profitability of solar and wind power plants anaylsis and for energy generation forecasting algorithms design and anaysis. Datasets used in doctoral dissertations,...
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On the formation process of silicon carbide nanophases via hydrogenated thermally induced templated synthesis
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Novel Catalysts, Room Temperature, and the Importance of Oxygen for the Synthesis of Single-Walled Carbon Nanotubes
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Synthesis of Polycyclic δ-Lactams with Bridged Benzomorphan Skeleton: Selectivity and Diversity Driven by Substituents
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Synthesis of sulfanylidene-diazaspirocycloalkanones in a three-component Mannich-type reaction catalyzed with lactic acid
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Synthesis of 2-Propanoyl-5-Norbornene in Pyridinium Ionic Liquids Catalyzed by Yttrium Salts
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Synthesis of new conjugates of MDP and nor-MDP with retro-tuftsin derivatives as potential immunomodulators
PublikacjaZsyntetyzowano nowe analogi muramylodipeptydu (MDP) i nor-muramylo-dipeptydu (nor-MDP) z pochodnymi retro-tuftsyny jako potencjalne immunomodulatory. Przedstawiono także syntezę odpowiednich pochodnych retro-tuftsyny. Do syntezy wykorzystano metodę mieszanych bezwodników z chloromrówczanem izobutylu i N-metylomorfoliną w bezwodnym DMF.
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Synthesis of Bis(ethylenedithio)dithiadiazafulvalenes (BEDT-DTDAF) and Generation of Charge Transfer Complexes with Tetracyanoquinodimetane
PublikacjaW artykule opisana została synteza Bis(etylenoditio)ditiadiazafulwalenów (BEDT-DTDAF) wykorzystująca jako kluczowe związki przejściowe 4,5-(etylenoditio)tiazol oraz sole 3-aliklo-4,5-(etylenoditio)tiazoliowe oraz generowanie przewodzących kompleksów z przeniesieniem ładunku usyskanych z Bis(etylenoditio)ditiadiazafulwalenów oraz tetracyjanochinodimetanu.
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Stimulated by cyclodextrins high yield synthesis of azocrown analogues comprising pyrrole or imidazole residues
PublikacjaBadano wpływ cyklodekstryn na reakcję syntezy aza-eterów zawierających w strukturze pirol lub imidazol. Stosowano alfa-, beta- i gamma-cyklodekstryny. Uzyskane wyniki analizowano pod kątem sposobu umieszczenia cząsteczki azolu we wnęce cyklodekstryny.
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Synthesis of New Hydrazone Derivatives and Evaluation of their Efficacy as Proliferation Inhibitors in Human Cancer Cells
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Synthesis and photo-conversion of androsta- and pregna-5,7-dienes to vitamin D3-like derivatives
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Synthesis of Fatty Acid Esters of Selected Higher Polyols Over Homogeneous Metallic Catalysts
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Lyotropic liquid crystal based on zinc oxide nanoparticles obtained by microwave solvothermal synthesis
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Synthesis, Pharmacological Evaluation, and Computational Studies of Cyclic Opioid Peptidomimetics Containing β3-Lysine
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Synthesis, structural, electronic and linear electro-optical features of new quaternary Ag2Ga2SiS6 compound
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Synthesis, single crystal growth and properties of Sr 5 Pb 3 ZnO 12
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Synthesis of analogues of anthraquinones linked to tuftsin or retro-tuftsin residues as potential topoisomerase inhibitors
PublikacjaZsyntetyzowano 10 nowych analogów antrachinonów z pochodnymi tuftsyny i retro-tuftsyny jako potencjalne inhibitory topoizomerazy. Substratem wyjściowym były zsyntetyzowane 1,4-, 1,5- i 1,8-bis(tosyloksy)-9,10-antrachinony oraz odpowiednio chronione pochodne tuftsyny i retro-tuftsyny, które otrzymano metodą mieszanych bezwodników z zastosowaniem chloromrówczanu izobutylu i NMM. Reakcje prowadzone były w acetonitrylu pod azotem w...
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Synthesis, spectroscopy and crystal structure determination of heteroleptic cobalt(II) silanethiolates with pyridine derivatives
PublikacjaCztery nowe tri-tert-butoksysilanotiolanowe kompleksy kobaltu(II) z 3- i 4-metylopirydyną zostały zsyntetyzowane i scharakteryzowane. Monometaliczne kompleksy otrzymano w reakcji bimetalicznego kompleksu [Co(SSi(OtBu)3(NH3)]2, który posłużył jako substrat kobaltu(II). Nowe związki zostały scharakteryzowane przy użyciu rentgenografii strukturalnej oraz spektroskopii UV-vis i FT-IR, a także za pomocą analizy elementarnej. Kompleksy...
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High-Entropy Perovskites as Multifunctional Metal Oxide Semiconductors: Synthesis and Characterization of (Gd0.2Nd0.2La0.2Sm0.2Y0.2)CoO3
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