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Metal complexes with mixed s-donor ligands - a route via silanethiolates
PublikacjaW ramach prezentowanej pracy przedstawiono pierwsze próby syntezy mieszanych układów zawierających jednocześnie przykoordynowane reszty ditiokarbaminianową oraz silanotiolanowych. W badaniach posłużono się - jako substratami tri-tert-butoksysilanotiolanami kompleksami Cd, Zn, Cu, Pb, Hg, Ag i Co, a także solami kwasów: dietyloditiokarbaminowego oraz pirolidynoditiokarbaminowego. W przypadku związku Ag nie udało się wyizolować stałych...
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Mechanism of the reaction of Lawesson's reagent with N-alkylhydroxamic acids
PublikacjaIdentyfikacja fosforowych produktów powstających w reakcji kwasów hydroksamowych z odczynnikiem Lawessona pozwoliła ustalić mechanizm tytułowej reakcji. Wykorzystano w tym celu spektroskopię 31P NMR. Wzorce labilnych produktów otrzymano na niezależnej drodze syntetycznej lub przeprowadzono je w trwałe pochodne, które wyizolowano z mieszanin reakcyjnych. Produktem przejściowym badanej reakcji okazał się odpowiedni O-ditiofosfonylowany...
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Ograniczniki bezpiecznikowe prądów zwarciowych na duże prądy robocze.
PublikacjaPrzedstawia się ogólną ideę ograniczania prądów zwarciowych w obwodach o dużych prądach roboczych niskiego i średniego napięcia w oparciu o bezstykowe hybrydowe ograniczniki prądu z wykorzystaniem specjalnych, krótkotopikowych bezpieczników. Idea takich ograniczników polega na zastąpieniu łącznika zestykowego ogranicznika hybrydowego bezpiecznikiem o minimalnej długości topika z intensywnym chłodzeniem topika przez osiowe przewodnictwo...
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Driver’s Condition Detection System Using Multimodal Imaging and Machine Learning Algorithms
PublikacjaTo this day, driver fatigue remains one of the most significant causes of road accidents. In this paper, a novel way of detecting and monitoring a driver’s physical state has been proposed. The goal of the system was to make use of multimodal imaging from RGB and thermal cameras working simultaneously to monitor the driver’s current condition. A custom dataset was created consisting of thermal and RGB video samples. Acquired data...
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<i>N,N,N</i>-Trimethyl-N-(methyl 5-deoxy-2,3-<i>O</i>-isopropylidene-β-D-ribofuranosid-5- yl)ammonium 4-methylbenzenesulfonate sesquihydrate.
PublikacjaThe structure of the title compound, [C12H24NO4][C7H7O3S]·1.5H2O, contains alternating layers parallel to (001) of hydrophobic and polar character, stabilized by C-H...O hydrogen bonding. The furan ring adopts an envelope conformation with the C(OMe) atom as the flap, and the dioxolane ring is twisted about one of the O-C(methine) bonds. A comparison to related compounds is presented. The tosylate-O atoms were disordered over two...
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A structure and simulation-driven design of compact CPW-fed UWB antenna
PublikacjaIn this letter, a structure of a miniaturized ultra-wideband CPW-fed antenna and its design proce-dure are presented. The antenna is a modified version of the design previously proposed in the literature, with additional degrees of freedom introduced in order to improve the structure flexibility. The small size is achieved by executing a rigorous optimization procedure that consists of two stages: (i) smart random search carried...
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Chromogenic amides of pyridine-2,6-dicarboxylic acid as anion receptors
PublikacjaThe synthesis of simple, chromogenic pyridine-2,6-dicarboxylic acid amides, derivates of isomeric nitroanilines and aminonitrophenols, and their ion binding properties are described. The ligands' response to ionic species was examined by naked eye and was studied with the use of UV-Vis spectroscopy in DMSO and its mixture with water. The effect of the localisation and the type of the substituents in aromatic rings were discussed....
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Selective detection of F- by chromogenic tetrazole receptor
PublikacjaA chromogenic anion host 4, containing two amide functionalities linked to azo dye and tetrazole rings was synthesized and its complexes with various anions were investigated. The results show that receptor 4 can recognize selectively biologically important F- ion. The binding affinity for F- was investigated by naked-eye colour change, UV-Vis and 1H NMR spectroscopy. Addition F- ion in CH3CN and DMSO to receptor 4 cause a colour...
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The enantiomeric determination of chloro-precursors of methamphetamine
PublikacjaImpurity profiling and classification of seized methamphetamine may supply valuable information with respect to the conditions and the chemicals used in the illicit methamphetamine manufacture and may provide information on the original source of the sample. Determination of the stereochemical makeup of forensic samples is important as well for the same reasons. Laboratories in many places are engaged in clandestine manufacture...
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Comparison of the coordination geometries of Zn(II) and Cd(II) ions in complexes with water, methanol and bulky aryloxysilanethiolate ligands
PublikacjaZinc and cadmium complexes containing silanethiolate anions and methanol or water were synthesized and characterized by X-ray diffraction, FT-IR and NMR spectroscopy, and DFT calculations. Contrary to zinc, the cadmium ion utilizes very weak donors to complete its coordination sphere; it forms contacts to phenyl rings of the silanethiolate ligand. Two zinc analogs of the general formula [Zn{SSi(OAr)3}2(L)2] where L = CH3OH (2)...
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Crystal structure and physical properties of new Ca2TGe3 (T = Pd and Pt) germanides
PublikacjaThe crystallographic, electronic transport and thermal properties of Ca2PdGe3 and Ca2PtGe3 are reported. The compounds crystalize in an ordered variant of the AlB2 crystal structure, in space group P6/mmm, with the lattice parameters a = 8.4876(4) Å/8.4503(5) Å and c = 4.1911(3) Å/4.2302(3) Å for Ca2PdGe3 and Ca2PtGe3, respectively. The resistivity data exhibit metallic behavior with residual-resistivity-ratios (RRR) of 13 for...
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Design and optimization of a novel miniaturized low-profile circularly polarized wide-slot antenna
PublikacjaThis paper presents a novel structure of a compact circularly polarized (CP) antenna. CP is obtained using a parasitic quasi-rectangular strip placed coplanar to the feedline. A ground plane perturbation combined with the asymmetric geometry of the coplanar waveguide ground planes is utilized to excite additional CP modes. All antenna dimensions are rigorously optimized to achieve the best possible performance in terms of the impedance...
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Listening to Live Music: Life beyond Music Recommendation Systems
PublikacjaThis paper presents first a short review on music recommendation systems based on social collaborative filtering. A dictionary of terms related to music recommendation systems, such as music information retrieval (MIR), Query-by-Example (QBE), Query-by-Category (QBC), music content, music annotating, music tagging, bridging the semantic gap in music domain, etc. is introduced. Bases of music recommender systems are shortly presented,...
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New Analogues of Mycophenolic Acid
PublikacjaMycophenolic acid (MPA) possesses antibacterial, antifungal, antiviral, immunosuppressive and anticancer properties. It is a non-competitive and reversible inhibitor of dehydrogenase inosine-5'-monophosphate (IMPDH). This compound belongs to the immunosuppressive drugs used for the prevention of both acute and chronic transplant rejection. Until now, two derivatives of MPA have been used clinically: mycophenolate mofetil (MMF,...
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The Quaternization Reaction of 5-O-Sulfonates of Methyl 2,3-o-Isopropylidene-β-D-Ribofuranoside with Selected Heterocyclic and Aliphatic Amines
PublikacjaThe synthesis of N-((methyl 5-deoxy-2,3-O-isopropylidene-β-D-ribofuranoside)-5-yl) ammonium salts are presented. To determine the effect of the nucleophile type and outgoing group on the quaternization reaction, selected aliphatic and heterocyclic aromatic amines reacted with: methyl 2,3-O-isopropylidene-5-O-tosyl-β-D-ribofuranoside or methyl 2,3-O-isopropylidene-5-O-mesyl-β-D -ribofuranoside or methyl 2,3-O-isopropylidene-5-O-triflyl-β-D-ribofuranoside...
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A Wind Energy Conversion System Based on a Generator with Modulated Magnetic Flux
PublikacjaIn this work, the concept of an energy conversion system for wind turbines based on the modified permanent magnet synchronous generator (PMSG) is presented. In the generator, a pair of three-phase windings is used, one of which is connected in a “star” and the second in a “delta” configuration. At the outputs of both windings, two six-pulse uncontrolled (diode) rectifiers are included. These rectifiers are mutually coupled by a...
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Silicon Oxycarbide-Graphite Electrodes for High-Power Energy Storage Devices
PublikacjaHerein we present a study on polymer-derived silicon oxycarbide (SiOC)/graphite composites for a potential application as an electrode in high power energy storage devices, such as Lithium-Ion Capacitor (LIC). The composites were processed using high power ultrasound-assisted sol-gel synthesis followed by pyrolysis. The intensive sonication enhances gelation and drying process, improving the homogenous distribution of the graphitic...
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A Subspace-Splitting Moment-Matching Model-Order Reduction Technique for Fast Wideband FEM Simulations of Microwave Structures
PublikacjaThis article describes a novel model-order reduction (MOR) approach for efficient wide frequency band finite-element method (FEM) simulations of microwave components. It relies on the splitting of the system transfer function into two components: a singular one that accounts for the in-band system poles and a regular part that has no in-band poles. In order to perform this splitting during the reduction process, the projection...
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Reactivity of bulky aminophosphanes towards small molecules: Activation of dihydrogen and carbon dioxide by aminophosphane/borane frustrated Lewis pairs
PublikacjaA series of mono- and bisaminophosphanes with formulas R2NPR’R’’ and (R2N)2PR’ (R = iPr, Cy; R’ = Ph, Cy; R’’ = iPr) were characterized by X-ray analysis, NMR spectroscopy and computational methods. The common structural futures of these species are short and polarized PAN bonds, a pyramidal geometry at the P atom and an almost planar geometry at the N atoms. According to DFT calculations, these...
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INTERNAL DETERMINANTS OF FIRMS’ INNOVATIVENESS
PublikacjaThis article presents an analysis of the determinants of a firm’s innovativeness deriving from its internal potential and characteristics. The analysis is based on research carried out on 1355 firms that applied for public subsidies from the Innovative Economy Operational Program in 2014. The methods applied are logit regression, comparative analysis and literature review. The analysis is structured ac- cording to Bielski’s model...
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Influence of chemical structure on physicochemical properties and thermal decomposition of the fully bio-based poly(propylene succinate-co-butylene succinate)s
PublikacjaIn this work, two polyesters and four copolyesters were studied. All materials were synthesized to obtain the monomers dedicated for thermoplastic polyurethane elastomers. For this type of PUR, the monomers should characterize by appropriate selected physicochemical properties and macromolecular structure distribution, which depends on synthesis conditions. The study of chemical structure with extensive and knowledgeable analysis...
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BADANIA NAGNIATANYCH POŁĄCZEŃ WTŁACZANYCH NA WAŁACH OKRĘTOWYCH
PublikacjaPrzedstawiono przyczyny możliwości zwiększenia trwałości wałów okrętowych, wskutek podwyższenia wytrzymałości zmęczeniowej połączenia wtłaczanego śruba - wał śrubowy przez nagniatanie. Badania wykonano na próbkach o średnicy 25 mm na specjalnie w tym celu zbudowanej maszynie zmęczeniowej MZ 30 z wodnym systemem chłodzenia próbki. Próbki wykonano ze stali C35 a tuleje ze stopu Novoston. Tuleje te zostały wtłoczone na stożek, wytwarzając...
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Synthesis of thiol derivatives of azobenzocrown ethers. The preliminary studies on recognition of alkali metal ions by gold nanoparticles functionalized with azobenzocrown and lipoic acid
PublikacjaThe article presents the synthesis of novel 13- and 16-membered azobenzocrown derivatives with peripheral thiol moieties and preliminary studies assessing their possible application in plasmonic sensors based on gold nanoparticles. The effect of the length of the chain connecting the macrocycle with the thiol group and the effect of the presence of the additional functional compound,...
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Impact of Galileo Observations on the Position and Ambiguities Estimation of GNSS Reference Stations
PublikacjaDevelopment of Galileo navigation system has caused that it is increasingly used in various areas. One of the most important of them is precise positioning of the reference networks. In this paper we present the impact of Galileo observations on the differential precise positioning as well as ambiguities resolution of selected GNSS stations. We tested five different solutions: GPS-only, Galileo-only, GPS/Galileo, GPS/GLONASS and...
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Rapid redesign of multiband antennas with respect to operating conditions and material parameters of substrate
PublikacjaThis work addresses geometry parameter scaling of multi-band antennas for Internet of Things applications. The presented approach is comprehensive and permits re-design of the structure with respect to both the operating frequencies and material parameters of the dielectric substrate. A two-step procedure is developed with the initial design obtained from an inverse surrogate model constructed using a set of appropriately prepared...
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Experimental Studies of Concrete-Filled Composite Tubes under Axial Short- and Long-Term Loads
PublikacjaThe paper presents experimental studies on axially compressed columns made of concrete-filled glass fiber reinforced polymer (GFRP) tubes. The infill concrete was C30/37 according to Eurocode 2. The investigated composite pipes were characterized by different angles of fiber winding in relation to the longitudinal axis of the element: 20, 55 and 85 degrees. Columns of two lengths, 0.4 m and 2.0 m, were studied. The internal diameter...
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Analysis of efficiency of phosphates sorption by different granulation of selected reactive material
PublikacjaIn the light of the need to find an effective way to remove phosphorus from wastewater, studies on the suitability of sorption materials in this process should be conducted. The aim of the study was to examine the potential benefits of using selected adsorbents to reduce orthophosphates from the model solution under steady conditions. The study was conducted on a laboratory scale using synthetic wastewater with concentration of...
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Design of a compact planar transmission line for miniaturized rat-race coupler with harmonics suppression
PublikacjaThis paper presents an elegant yet straightforward design procedure for a compact rat-race coupler (RRC) with an extended harmonic suppression. The coupler’s conventional λ/4 transmission lines (TLs) are replaced by a specialized TL that offers significant size reduction and harmonic elimination capabilities in the proposed approach. The design procedure is verified through the theoretical, circuit, and electromagnetic (EM) analyses,...
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Assessment of Corrosive Behaviour and Microstructure Characterization of Hybrid Friction Stir Welded Martensitic Stainless Steel
PublikacjaThis study examined the effect of induction heating on the microstructure and corrosion characteristics of hybrid friction stir welded AISI 410 stainless steel. Five joints have been produced with different friction stir welding parameters like welding speed, spindle speed, plunge depth, and induction power. Their microstructures were evaluated using a scanning electron microscope, and chemical composition was examined using...
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Decolorisation of Methylene Blue with Sodium Persulfate Activated with Visible Light in the Presence of Glucose and Sucrose
PublikacjaThe paper presents the results of research on the methylene blue (MB) degradation with sodium persulfate (PDS) activated with visible light (Vis) in the presence of glucose and sucrose. The following test were examined: absence and presence of sugars in concentrations of 50–300 mM, presence and absence of Vis radiation, pH of the model solution (6.0–12.0), identification of free radicals, kinetics of the pseudo-first-order reaction....
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Fracture Surface Topography Parameters for S235JR Steel Adhesive Joints After Fatigue Shear Testing
PublikacjaThis paper presents the experimental results of a study investigating the effect of holes and notches made on the overlap ends on the strength of adhesive joints. Single-lap joints made of S235JR steel sheets bonded with Araldite 2024-2 epoxy adhesive were tested. For comparative reasons, static shear strength tests and high-cycle fatigue strength tests were performed. Adhesive-filled joints having three holes, each with a diameter...
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Recombinant !ermostable AP Exonuclease from Thermoanaerobacter tengcongensis: Cloning, Expression, Purification, Properties and PCR Application
PublikacjaApurinic/apyrimidinic (AP) sites in DNA are considered to be highly mutagenic and must be corrected to preserve genetic integrity, especially at high temperatures. !e gene encoding a homologue of AP exonuclease was cloned from the thermophilic anaerobic bacterium Thermoanaerobacter tengcongensis and transformed into Escherichia coli. The protein product showed high identity (80%) to human Ape1 nuclease, whereas to E. coli exonuclease...
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Optimization of capillary isotachophoretic method for determination of major macroelements in blue honeysuckle berries (Lonicera caerulea L.) and related products
PublikacjaA reliable and repeatable isotachophoretic method for the simultaneous determination of K+, Na+, Ca2+, Mg2+ and ammonium in berries of different blue honeysuckle cultivars was developed. The usefulness of the complex-forming equilibria in determining the cations mentioned above was studied. The addition of 7.5 mM 18-crown-6 and 2 mM α-hydroxyisobutyric acid to sulfuric acid enhanced the separation capacity of the leading electrolyte....
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Wpływ warunków zgrzewania metodą Friction Stir Welding na własności mechaniczne i jakość złączy ze stopu aluminium
PublikacjaCelem niniejszych badań było porównanie wpływu kształtu narzędzia na złącze oraz uzyskanie wartości parametrów zgrzewania tarciowego z przemieszaniem (FSW) zapewniających najlepszą możliwą jakość złącza. Zastosowanym materiałem był stop aluminium EN AW-3004 (AlMn1Mg1). Według najlepszej wiedzy autorów dotychczas nie przedstawiono żadnych badań tego stopu w kwestii zgrzewania FSW. Złącza pięcioczołowe wykonano samodzielnie opracowanym...
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Stesses in tank shell with shape deformation
PublikacjaW referacie przedstawiono wyniki pomiarów naprężeń w płaszczy stalowego, rzeczywistego zbiornika. Pomiary przeprowadzono przy pomocy tensometrii elektrooporowej. Obiektem badań był stalowy zbiornik pionowy z dachem pływającym o pojemności nominalnej 12.000 m3. Defermacje płaszcza stalowego badanego obiektu wynoszą od -170 do +150 mm.
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Badania wpływu twardości materiału obrabianego na temperaturę docieraka podczas docierania powierzchni płaskich
PublikacjaPrzedstawiono wyniki badań wpływu twardości materiału obrabianego na wzrost temperatury docieraka. Obrabiano elementy ze stali C45 na docierarce jednotarczowej. Porównano obróbkę elementów walcowych o średnicy 17 mm i twardości 160 i 650 HV mikroziarnami węglika krzemu F400/17. W badaniach wykorzystano kamerę termowizyjną.
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Rozdrobione odpady polimerowe- nowy problem i świadek historii wpływu człowieka na najnowsze dzieje ziemi.
PublikacjaSyntetyczne polimery są nieodłącznym towarzyszem współczesnego człowieka i dowodem jego działalności obecnym w osadach, szczególnie od połowy XX wieku. Przeciętny konsument wprowadza dziennie do środowiska około 2,4 mg mikroplastiku. Terminem "mikroplastik" określa się odpady z tworzyw sztucznych, ktorych wielkość nie przekracza 5 mm.
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Leakage detection and localisation in drinking water distributionnetworks by MultiRegional PCA
PublikacjaMonitoring is one of the most important steps in advanced control of complex dynamic systems. Precise information about systems behaviour, including faults indicating, enables for efficient control. The paper describes an approach to detection and localisation of pipe leakage in Drinking Water Distribution Systems (DWDS) representing complex and distributed dynamic system of large scale. Proposed MultiRegional Principal Component...
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Badania nad rozdzielaniem grupowym i analityką składu grupowego olejów bazowych i smarowych, zwłaszcza o szerokim zakresie polarności składników
PublikacjaRozprawa to studia i badania nad rozdzielaniem i analityką składu grupowego olejów bazowych i smarowych o szerokim zakresie polarności składników. Studium literatury wykazało brak metodyk badania udziału frakcji naftowej i roślinnej w takich olejach oraz nieadekwatność w tym celu HPLC. Pierwsza część pracy to badania nad opracowaniem wielokrotnie zastosowanej w praktyce terenowej metodyki i wyposażenia dla zastosowania fluorescencji...
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Experimental and theoretical analysis of dryout in annular flow
PublikacjaW pracy opisano badania eksperymentalne kryzysu wrzenia typu dryout, przeprowadzone w pionowych rurkach o średnicy wewnętrznej 1.15 i 2.3 mm z wykorzystaniem dwóch czynników roboczych, tj. SES36 i R123. W oparciu o wyniki tych badań zaproponowano ogólną korelację na krytyczny strumień ciepła w minikanałach.
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Pomiary temperatury podczas gładzenia długich otworów
PublikacjaW artykule przedstawiono wyniki badań temperatury podczas gładzenia otworów w elementach stalowych. Badano otwory o średnicach 75H7 i 150H7 mm. Do analiz zastosowano metodę termowizyjną. Otrzymane wyniki badań pozwolą uzyskać wysoką dokładność wymiarową otworów w częściach metalowych, a także właściwie zaplanować miejsce i czas kontroli końcowej.
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Rury o wielkich średnicach
PublikacjaSpecyfika rurociągów o wielkich średnicach. Współczesne rozwiązania z tworzyw duroplastycznych i termoplastycznych. Problemy lekkiego rurociągu o DN2500 mm. Transport wodny w postaci tratwy jako rozwiązanie dla jednostkowego wyrobu (rury o długości 6 m) o kubaturze ok. 40 m3 i masie ok. 6 ton. Rozwiązanie norweskie
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Does the chemical modification of Nystatin A1 affect the drug's ability to overcome the multidrug resistance of fungi?
PublikacjaAlthough the contemporary medicine keeps moving forward, disseminated infections caused by fungal pathogens are an emerging challenge. The dramatic rise of fungal diseases, especially the most life-threatening systemic mycoses is associated with a permanently growing number of immunodeficient patients. Undoubted difficulties in the treatment of fungal infections are caused by lack of highly effective and selective antifungal drugs,...
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Products of Photo- and Thermochemical Rearrangement of 19-Membered di-tert-Butyl-Azoxybenzocrown
PublikacjaThe preparation and characterization of products of the photochemical and thermochemical rearrangements of 19-membered azoxybenzocrowns with two, bulky, tert-butyl substituents in benzene rings in the para positions to oligooxyethylene fragments (meta positions to azoxy group, i.e., t-Bu-19-Azo-O have been presented. In photochemical rearrangement, two colored typical products were expected, i.e., 19-membered o-hydroxy-m,m′-di-tert-butyl-azobenzocrown...
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Actual and reference evapotranspiration for a natural, temperate zone fen wetland – Upper Biebrza case study
PublikacjaEvapotranspiration is the key and predominant component of the water balance in wetlands. Direct evapotranspiration measurements are challenging in wetlands due to their remoteness and high surface water level. This article describes the actual (ETa and reference evapotranspiration (ET0) from a cultivated wet meadow located in the Biebrza National Park – the largest national park in north-east Poland, Central Europe. The data were...
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Analysis of surface roughness of chemically impregnated Scots pine processed using frame-sawing machine
PublikacjaThe objective of this work was to evaluate the effect of the impregnation process of pine wood (Pinus sylvestris L.) on roughness parameters of the surface processed on a frame sawing. The samples weredried and impregnated using a commercial procedure by a local company. The touch method withthe use of measuring stylus (pin) was employed to determine of surface roughness of the samplesconsidering parameters, namely, arithmetical...
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Stanowisko laboratoryjne do badania mechanizmów odkształcalnych o kinematyce równoległej
PublikacjaW pracy przedstawiono projekt stanowiska laboratoryjnego służącego do badania właściwości kinematycznych mechanizmów odkształcalnych o kinematyce równoległej. Omówiono wymagania, jakie powinno spełniać stanowisko laboratoryjne, aby przeprowadzić analizę odkształcalnego przegubu o rozmiarach od 2.5 mm do 15 mm średnicy, posiadającego trzy sterowalne stopnie swobody. Zaprezentowano unikatowe systemy pomiarowe sił, umożliwiające pomiary...
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Badania eksperymentalne strefy przypodporowej żelbetowych belek częściowo sprężonych
PublikacjaThis project refers to the study the shear zone, under full and partial prestressing in comparison to beams with passive reinforcement.For comparison, variable parameters have been determined:- a/d (from 1,5 to 3,5) - it's shear span to effective depth of the beam . Assuming constant geometrical quantities, "a" is variable.- 26 beams had no vertical shear reinforcement, and the other 26 had closed stirrups.- prestressing intensity...
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A novel method for drop in drop edible oils encapsulation with chitosan using a coaxial technique
PublikacjaThe presented work concerns a novel one step method for oil encapsulation. In this coaxial system the oil constitutes the core of the capsule, while the chitosan solution is the polymer shell surrounding the core to provide separation of the core from the external environment. The paper contains a diagram of the encapsulation equipment and explains the principle of its operation. The experimental results showed the impact of the...
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Structure and hyperfine interactions in Bi1−xNdxFeO3 solid solutions prepared by solid-state sintering
PublikacjaThe series of polycrystalline ceramic powders, Bi1xNdxFeO3 (x = 0.11) was successfully synthesized by mixed oxide method followed by pressureless sintering. X-ray diffraction and Mössbauer spectroscopy were used as complementary methods to study structure and hyperfine interactions of the samples. It was found that with an increase of Nd content, within the range of x = 0.20.3 a structural phase transition from rhombohedral to...