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Optical properties of boron-doped nanocrystalline diamond films studied by spectroscopic ellipsometry
PublikacjaThe optical properties of boron-doped nanocrystalline diamond films, coated using Microwave Plasma Enhanced Chemical Vapour Deposition (μPE CVD) system, were analyzed by spectroscopic ellipsometry. Diamond films were deposited on silicon substrates. The ellipsometry data (refractive index (n(λ)), extinction coefficient (k(λ)) were modeled using dedicated software. Evolution of the optical structure with boron doping was observed...
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Reaction of aniline with ammonium persulphate and concentrated hydrochloric acid: Experimental and DFT studies
PublikacjaIn this paper, the reaction of aniline with ammonium persulphate and concentrated HCl was studied. As a result of our experimental studies, 2,4,6-trichlorophenylamine was identified as the main product. This shows that a high concentration of HCl does not favour oxidative polymerisation of phenylamine, even though the ammonium persulphate/HCl system is widely used in polyaniline synthesis. On the basis of the experimental data...
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Mechanical, Structural and Diffusion Studies of Hydrogel Polyurethane Nanocomposites Containing Modified Montmorillonite
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Performance of Particle Oxidation Catalyst and Particle Formation Studies with Sulphur Containing Fuels
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Experimental and theoretical studies on the Sulfamethazine-Urea and Sulfamethizole-Urea solid-liquid equilibria
PublikacjaThe miscibility of active pharmaceutical ingredients with excipients is an important aspect in pharmaceutical technology protocols. In this study, the differential scanning calorimetry (DSC) was used for Sulfamethazine-Urea (SI–U) and Sulfamethizole-Urea (SO–U) solid-liquid phase diagrams determination. Both sulfonamides form simple binary eutectics with Urea. The lack of new co-crystal phase formation was confirmed by inspection...
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Galvanostatic impedance measurements for the efficient adsorption isotherm construction in corrosion inhibitor studies
PublikacjaWe present an approach towards an accurate and time-efficient adsorption isotherm determination to evaluate the corrosion inhibitor interaction in electrolytic environments. The approach is based on dynamic impedance spectroscopy measurements in galvanostatic mode (g-DEIS). The studied corrosion inhibitor is continuously injected between the secondary cell and the corrosion cell. The efficiency corresponding to instantaneous inhibitor...
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SEM and TEM Studies on <i>In-Situ</i> Cast Al–TiC Composites
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Nanostructured Lipid Carriers Engineered as Topical Delivery of Etodolac: Optimization and Cytotoxicity Studies
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Identification of yellow luminescence centers in Be-doped GaN through pressure-dependent studies
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X-ray and NMR structural studies of the series of porphyrazines with peripheral pyrrolyl groups
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Selection of reliable reference genes in eutopic and ectopic endometrium for quantitative expression studies
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Femtosecond studies of the excited-state dynamics of ester-alkyloxy substituted zinc phthalocyanines
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Rysunek Jana van Eycka do "Portretu kardynała Albergatiego": studium osobowości.
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The influence of the substrate temperature on the preparation of DNA films for studies under vacuum conditions
PublikacjaExperiments were carried out to determine the dependence of the physical form of supercoiled DNA films on the initial temperature of the substrate. Such films are often used in irradiation experiments involving low energy particles, like electrons or photons. In order to obtain absolute values for cross sections for such experiments, the spatial distribution of the sample in the film has to be well estimated. These investigations...
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EHV transmission lines wires location on line operation issues - case studies
PublikacjaTransmission lines towers construction affects the line parameters and influences on its operation in the future. Misguided design of the tower can lead to serious problems such as overvoltages, electric arc extinction difficulties, voltage asymmetry, resonance phenomena or increasing of magnetic field near the line. The paper points out those threats on example of 400 kV double circuit overhead transmission line with shunt reactors....
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Are stabilizing osmolytes preferentially excluded from the protein surface? FTIR and MD studies
PublikacjaInteractions between osmolytes and hen egg white lysozyme in aqueous solutions were studied by means of FTIR spectroscopy and molecular dynamics. A combination of difference spectra method and chemometric analysis of spectroscopic data was used to determine the number of osmolyte molecules interacting with the protein, and the preferential interaction coefficient in presented systems. Both osmolytes – L-proline and trimethylamine-N-oxide...
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STUDIUM UWARUNKOWAŃ W POZYSKIWANIU FUNDUSZY POZABUDŻETOWYCH 2007-2014 - gmina Sulęczyno
PublikacjaDokument jest analizą pozyskiwania funduszy unijnych przez gminę Suleczyno w latach 2007-2015. Wskazuje na uwarunkowania w pozyskiwaniu, bariery, a także określa główne kierunki zapotrzebowania na najbliższe lata
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Ab initio studies of phonons in MgO by the direct method including LO mode
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Spectroscopic and Spectroelectrochemical Studies on Redox Properties of Zinc Sulfide and Their Consequences on Photocatalytic Activity
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Transcranial magnetic stimulation (TMS) in treatment of psychiatric disorders – review of current studies
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Impact and pitfalls of scaling of left ventricular and atrial structure in population-based studies
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Modified nanodiamond particle size studies by means of dynamic light scattering technique
PublikacjaThe Methods Utilizing the Phenomena of Light Scattering to Measure Particle Size distribution in different solvent, such as deionise water and alcohol and also to study the various structural formation when nanodiamond solution is placed on silicon surface. The purpose of this research project is divided into two parts to configure the measurement units for examining modified nanodiamond particles, examination...
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Modified nanodiamond particle size studies by means of dynamic light scattering technique
PublikacjaThe Methods Utilizing the Phenomena of Light Scattering to Measure Particle Size distribution in different solvent, such as deionise water and alcohol and also to study the various structural formation when nanodiamond solution is placed on silicon surface. The purpose of this research project is divided into two parts to configure the measurement units for examining modified nanodiamond particles, examination...
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Studies on the complex formation between lactams and thiolactams of sparteine with copper(II) cation
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Kinetic and equilibrium studies of the reaction of 2,4-dinitrophenyl-2,4,6-trinitrophenylmethane with cryptands in acetonitrile
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Studies of the complex formation between some proton sponges and Cu(II) cations
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Potentiometric and AM1d studies of a new class of Tr-podands–silver(I) complexes
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In Search of Panacea—Review of Recent Studies Concerning Nature-Derived Anticancer Agents
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Edible Flowers Extracts as a Source of Bioactive Compounds with Antioxidant Properties—In Vitro Studies
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New supervised alignment method as a preprocessing tool for chromatographic data in metabolomic studies
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Experimental and theoretical studies of the spectroscopic properties of simple symmetrically substituted diphenylacetylene derivatives
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Conformational studies of cyclic enkephalin analogues withL- orD-proline in position 3
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Control Theory Education in the Distance Education B.Eng. Studies at Warsaw University of Technology
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Synthesis, biological activity and molecular modelling studies of tricyclic alkylimidazo-, pyrimido- and diazepinopurinediones
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Crystallographic and spectroscopic studies of 5-arylidene-2-amino-imidazol-4-ones
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Cyclic Dipeptides as Building Units of Nano- and Microdevices: Synthesis, Properties, and Structural Studies
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Complementarity of electronic and vibrational circular dichroism based on stereochemical studies of vic-diols
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In situ optical studies of thermal stability of iodine-doped polyazomethine thin films
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Studies of Transport Properties of Single Layer Devices Based on the Polyazomethine Thin Films
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Time Projection Chamber (TPC) detectors for nuclear astrophysics studies with gamma beams
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Polyphenol-Enriched Composite Bone Regeneration Materials: A Systematic Review of In Vitro Studies
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Increasing the conductivity of V2O5 -TeO2 glass by crystallization: structure and charge transfer studies
PublikacjaIn the present paper, V2O5-TeO2 glass...
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Guided wave propagation in structures. Modelling, experimental studies and application to damage detection
PublikacjaCelem niniejszej pracy są eksperymentalne i numeryczne analizy propagacji prowadzonych fal sprężystych w stalowych konstrukcjach prętowych, belkowych, ramowych, tarczowych i płytowych. W szczególności praca poświęcona jest: (a) modelowaniu propagacji fal z uwzględnieniem zjawiska dyspersji; (b) budowie modeli obliczeniowych w formalizmie metody elementów spektralnych; (c) eksperymentalnej weryfikacji zaproponowanych modeli; (d)...
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The influence of the substrate temperature on the preparation of DNA films for studies under vacuum conditions
PublikacjaPrzeanalizowano wpływ temperatury na formowanie warstw DNA. Sprawdzono wpływ stabilizatorów na jakość otrzymanych próbek. Stwierdzono, że optymalnymi warunkami przygotowywania filmów do badań w warunkach próżniowych jest - 10 st. C przy minimalnej zawartości NaOH.
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Mechanical, structural and diffusion studies of hydrogel polyurethane nanocomposites containing modified montmorillonite
PublikacjaW pracy zaprezentowano wyniki badań hydrożeli poliuretanowych zawierających poli(tlenek etylenu) oraz montmorylonit. Otrzymane układy scharakteryzowano z użyciem technik XRD, DMA, badań mechanicznych oraz wyznaczono chłonność wody i parametry dyfuzji.
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Kościół grodowy w Gdańsku. Studium z pogranicza historii i architektury
PublikacjaW części pierwszej artykułu przedstawiony został zarys dziejów kościoła grodowego, noszącego wezwanie mariackie. Powstał on ok. poł. XII w. i istniał aż do końca lat dwudziestych XIV w. W XIII w. lokowana była przy nim grupa kanonicka pełniąca pełniąca funkcje kancelaryjne przy księciu Świętopełku II i Warcisławie II. Kościół przetrwał zniszczenie Gdańska przez Krzyżaków i był przez nich użytkowany aż do rozpoczęcia budowy zamku...
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Synthesis, spectroscopy and computational studies of some biologically important hydroxyhaloquinolines and their novel derivatives
PublikacjaA series crystalline compounds of methyl and phosphinyl derivatives of 2-methylquinolin-8-ol (1a) and related 5,7-dichloro-2-methylquinolin-8-ol (1b) were quantitatively prepared and characterized by microanalysis, IR, UV-vis and multinuclear NMR spectroscopy. Five of them have been characterized by single crystal X-ray diffraction method. The known compounds, 8-methoxy-2-methylquinoline (2a) and 8-methoxyquinoline (2d), were synthesised...
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Threshold photoelectron studies of isoxazole over the energy range 9.9-30 eV
PublikacjaThe threshold photoelectron spectrum of the isoxazole molecule, C3H3NO has been measured over the photon energy range 9.9-30 eV with the use of synchrotron radiation. In the 9.9-10.8 eV range, corresponding to photoionization from the highest occupied molecular orbital 3a"(π3), seven well resolved vibrational series have been observed and their modes are tentatively assigned. A strong adiabatic ionization, with an energy of 11.132...
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Studies on the influence of technological variants of finishing machining on flow of parts in flexible manufacturing
PublikacjaIn the article below the problems of influence of variants of finishing processing on flow of machining parts in flexible manufacturing system were presented. The investigations were carried out the technological processes for piston rods and rams of hydraulic cylinders. There were also presented model variants of technological processes for piston rods finished with the burnishing. In these studies the influence of technological...
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Synthesis, spectroscopy and computational studies of some novelphosphorylated derivatives of quinoline-5,8-diones
PublikacjaThe neutral phosphorus nucleophiles such as R2P(=Y)M allowed the radical addition to 2-methyl-5,8-dioxo-5,8-dihydroquinoline-7-amine and N-(2-methyl-5,8-dioxo-5,8-dihydroquinolin-7-yl)acetamide giving exclusively O-phosphorylated products. All products were quantitatively prepared and characterized by microanalysis, and multinuclear NMR spectroscopy. Seven of them, have been characterized by single crystal X-ray diffraction method....