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Wyniki wyszukiwania dla: facts extraction
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Micro-cloud point extraction for preconcentration of Aspirin in commercial tablets prior to spectrophotometric determination
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Application of a Novel Micro-Cloud Point Extraction for Preconcentration and Spectrophotometric Determination of Azo Dyes
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Optimized procedure of extraction, purification and proteomic analysis of nuclear proteins from mouse brain
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Extraction, Optimization, and Characterization of Neem Seed Oil via Box-Behnken Design Approach
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Micro-Cloud Point Extraction for Preconcentration of Aspirin in Commercial Tablets Prior to Spectrophotometric Determination
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Statistical evaluation of the effectiveness of different extraction techniques for determining robenidyne levels in poultry feed.
PublikacjaPoprzez zastosowanie testu Kruskala-Wallisa i chemometrycznej techniki analizy podobieństwa porównano efektywność sześciu różnych technik ekstrakcji (wytrząsanie, ekstrakcja w aparacie Soxhleta, w aparacie Soxteca, wspomaganej ultradźwiękami, wspomaganej promieniowaniem mikrofalowym oraz przyspieszonej ekstrakcji rozpuszczalnikiem) na podstawie wyników odzysku robenidyny z próbek paszy dla ptaków. W zależności od zastosowanej techniki...
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Extraction of antenna pattern from near field antenna measurements distorted by undesired emission
PublikacjaIn this paper authors present experimental correction of antenna pattern obtained from near field measurements when they are distorted by determined electromagnetic emission. Such situation may be met e.g. when feeding or supply subsystem interacts with antenna radiation pattern due to self-emission. Presented results of experiments show effectiveness of extraction of antenna pattern utilizing near field antenna measurements.
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Web component for automatic extraction of ontological information from informal description of web services
PublikacjaThis article treats about usage possibilities of Web Services and cooperation in development that leads to constant improvement of these components. It describes the semantic methods which can beused to create the description that is comprehensible for computers. It also presents the two models supporting the automatic generation of the semantic description based on informal description. Thepaper draws upon the comparison of two...
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Diethyl carbonate as a green extraction solvent for chlorophenol determination with dispersive liquid–liquid microextraction
PublikacjaThe principles of green analytical chemistry indicate that the search for greener organic solvents for extraction applications is crucial. In this study diethyl carbonate (DEC) is proved to be a green solvent, as it is relatively nontoxic, obtainable from renewable resources and biodegradable. Here it is applied as an extraction solvent for chlorophenol determination in water samples with dispersive liquid–liquid microextraction....
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Effect of the ionic liquids on extraction of aromatic and sulfur compounds from the model petrochemical stream
PublikacjaSuitability of a imidazolium ionic liquids (ILs) as solvents in dearomatization and desulfurization in the ternary systems and in a model multicomponent systems has been analyzed. With this aim, ternary liquid-liquid phase equilibrium data (LLE) have been obtained for ternary mixtures of {IL + benzene, or toluene, or thiophene, or 2-butanethiol + hexane}, or {IL + benzene + 2-methylpentane} at T = 298.15 K and ambient pressure,...
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SYNTHETIZED MEMBRANES FOR ULTRASOUND-ASSISTED SOLVENT EXTRACTION OF POROUS MEMBRANE PACKED SOLID SAMPLES.
PublikacjaMembranes are becoming more and more popular in analytical chemistry, which is why they are used, among others, in extraction processes. Therefore, this work focuses on the process of synthesis PVDF membranes and its optimization. The obtained membranes were used as bags for the phthalate extraction in disposable diapers for babies. Extraction was accomplished by method ultrasound-assisted solvent extraction of porous PVDF membrane...
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A New Adaptive Method for the Extraction of Steel Design Structures from an Integrated Point Cloud
PublikacjaThe continuous and intensive development of measurement technologies for reality modelling with appropriate data processing algorithms is currently being observed. The most popular methods include remote sensing techniques based on reflected-light digital cameras, and on active methods in which the device emits a beam. This research paper presents the process of data integration from terrestrial laser scanning (TLS) and image data...
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Up-to-date strategies and future trends towards the extraction and purification of Capsaicin: A comprehensive review
PublikacjaBackground According to the current need of manufacturing healthier products, food companies are seeking specific biomolecules that may offer additional added value (i.e., biological activities) to the new food formulations. Capsaicin, as the pungent ingredient of chili peppers, has become so far one of the target biomolecules explored since the 1950s. There is evidence demonstrating that capsaicin exhibits important biological...
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Signals Features Extraction in Radioisotope Liquid-Gas Flow Measurements using Autocorrelation Function
PublikacjaKnowledge of the two-phase flow structure is essential for the proper conduct of industrial processes. Description of liquid-gas flow regimes is possible by using of data analysis in time, frequency, or state-space domain. In this research studies, the autocorrelation function is applied for analysis of signals obtained for liquid-gas flow by use gamma-ray absorption. The experiments were carried out on the laboratory hydraulic...
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Buried Object Characterization by Data-Driven Surrogates and Regression-Enabled Hyperbolic Signature Extraction
PublikacjaThis work addresses artificial-intelligence-based buried object characterization using FDTD-based electromagnetic simulation toolbox of a Ground Penetrating Radar (GPR) to generate B-scan data. In data collection, FDTD-based simulation tool, gprMax is used. The task is to estimate geophysical parameters of a cylindrical shape object of various radii, buried at different positions in the dry soil medium simultaneously and independently...
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Signals features extraction in radioisotope liquid-gas flow measurements using wavelet analysis
PublikacjaKnowledge of the structure of a flow is significant for the proper conduct of a number of industrial processes. In this case, a description of a two-phase flow regimes is possible by use of the time-series analysis in time, frequency and state-space domain. In this article the Discrete Wavelet Transform (DWT) is applied for analysis of signals obtained for water-air flow using gamma ray absorption. The presented method was illustrated...
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Polyethylene glycol-coated solid-phase microextraction fibres for the extraction of polar analytes-A review
PublikacjaThe article discusses the merits and limitations of commercially available solid-phase microextraction (SPME) fibres and compares them with the new type of extraction coatings, in particular those containing polyethylene glycol as sorbent, as well as the methods of the preparation of the latter. It also analyses their possible application for the extraction of a broad spectrum of analytes, with particular emphasis on the sampling...
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Collective excitations in the hubbard model with intrasite attraction
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Bilateral power supply of the traction network as a first stage of Smart Grid technology implementation in electric traction
PublikacjaSince 2001, trolleybus system in Gdynia has been involved in many activities related to the reduction of power consumption, both in terms of implementation and research and development. In PKT, in cooperation with SESTO company, started applications of Smart Grid technologies in supply network: the bilateral supply. The paper presents results of this this novel investment.
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Trolleybus with traction batteries for autonomous running
PublikacjaIn 2009 the transport company of city Gdynia (Poland) introduced in the operation trolleybuses fitted with traction batteries. This solution was designed for emergency situations, such as: damage of overhead lines or power loss. Transport company also considering the use of batteries in regular use. The article presents the operational experiences gained during the current operation. Furthermore, there are presented new trends...
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Trolleybuses with traction batteries for autonomous running
PublikacjaIn 2009 the transport company of city Gdynia (Poland) introducet in the operation trolleybuses fitted with traction batteries. This solution was designed for emergency situations, such as: damage of overhead lines or power loss. Transport company also considering the use of batteries in regular use. The article presents the operational experiences gained during the current operation. Furthermore, there are presented new trends...
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Glycerolic Licorice Extracts as Active Cosmeceutical Ingredients: Extraction Optimization, Chemical Characterization, and Biological Activity
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Synthesis and structural properties of carbon/alumina composites: Practical application in solid phase extraction of explosives
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Continuous Monitoring of Thermooxidative Degradation Products of Polystyrene by Membrane Extraction with Sorbent Interface and Gas Chromatography
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Application of a magnetically separable Zr-MOF for fast extraction of palladium before its spectrophotometric detection
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Hydrophobic deep eutectic solvents as “green” extraction media for polycyclic aromatic hydrocarbons in aqueous samples
PublikacjaThe paper presents novel nonionic and hydrophobic deep eutectic solvents which were synthesized from natural compounds, i.e., thymol, ±camphor, decanoic and 10-undecylenic acids. Fundamental physicochemical properties of the synthesized deep eutectic solvents were determined, followed by their application as extractants in ultrasound-assisted dispersive liquid-liquid microextraction to isolate and enrich polycyclic aromatic hydrocarbons...
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Modeling and MANOVA studies on toxicity and endocrine potential of packaging materials exposed to different extraction schemes
PublikacjaThe stability of the linings of packaging that is in contact with the goods stored has been of major concern during decades of the development of packaging materials. In this work, an attempt was undertaken to assess the applicability of using two bioassays (Microtox® and XenoScreen YES/YAS) in estimating the stability of packaging (cans, caps, multilayer material) and the impact of their degradation on the toxicity of some simulated media....
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Supercritical fluid extraction of algae enhances levels of biologically active compounds promoting plant growth
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The Copper(II) Ions Solvent Extraction with a New Compound: 2,6-Bis(4-Methoxybenzoyl)-Diaminopyridine
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Device characteristics extraction by low frequency noise measurements; Someresults on the state-of-the-art MOSFET´s
PublikacjaPrzedstawiono wyniki pomiarów i analizy szumów tranzystorów MOSFET z izolatorem bramki wykonanym z SiO2 i HfO2. Wyniki pomiarów wykorzystano do oszacowania gęstości aktywnych stanów na powierzchni użytego tlenku i porównano z wynikami otrzymanymi metodą charge-pumping.
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Determination of pesticides in water using new solid phase extraction technique - speedisk and speedisk column.
PublikacjaW publikacji opisano zastosowanie nowych narzędzi do ekstrakcji do fazy stałej: szybkie dyski i szybkie kolumienki (speedisk i speedisk column). Zaprezentowano ich zastosowanie do ekstrakcji pestycydów z próbek wody, przy zastosowaniu różnych rozpuszczalników.
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ANALYSIS OF THE IMPACT OF MASS FLOW EXTRACTION ON THE CHANGE OF PARAMETERS IN A LABYRINTH SEAL USING THE STODOLA METHOD
PublikacjaLabyrinth seals are an important element of a steam turbine set design. The use of diagnostic extraction makes it possible to control the operation of a seal by providing information on the thermodynamic parameters along the length of the seal. Diagnostic extraction has a considerable impact on the change of the parameters, the amount of the extracted mass. This article describes the dependence of pressure in the clearance downstream...
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Extraction and evaluation of gas-flow-dependent features from dynamic measurements of gas sensors array
PublikacjaGas analyzers based on gas sensors are the devices which enable recognition of various kinds of volatile compounds. They have continuously been developed and investigated for over three decades, however there are still limitations which slow down the implementation of those devices in many applications. For example, the main drawbacks are the lack of selectivity, sensitivity...
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ANALYSIS OF THE IMPACT OF MASS FLOW EXTRACTION ON THE CHANGE OF PARAMETERS IN A LABYRINTH SEAL USING THE STODOLA METHOD
PublikacjaLabyrinth seals are an important element of a steam turbine set design. The use of diagnostic extraction makes it possible to control the operation of a seal by providing information on the thermodynamic parameters along the length of the seal. Diagnostic extraction has a considerable impact on the change of the parameters, the amount of the extracted mass. This article describes the dependence of pressure in the clearance downstream...
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Small signal admittance spectroscopy applied for extraction of charge carrier mobility in thin organic layers
PublikacjaPraca przedstawia nowy sposób wyznaczania ruchliwości nośników ładunku w cienkich warstwach organicznych w oparciu o pomiary widm małosygnałowej admitancji.
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Application of magnetic nanoparticles for magnetic solid-phase extraction in preparing biological, environmental and food samples
PublikacjaThe need to obtain meaningful results as the basis for determining the content of trace amounts of analytes has become the driving force behind the development of modern analytical techniques, including sample-preparation techniques, such as solid-phase extraction (SPE). Recently, great interest was aroused in the use of magnetic nanoparticles (MNPs) in SPE. These materials exhibit high selectivity, and, in small amounts, can provide...
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Deep eutectic solvents in analytical sample preconcentration Part B: Solid-phase (micro)extraction
PublikacjaOne of the key challenges of modern analytical chemistry is the monitoring of trace amounts of contaminants using sensitive and selective instrumental techniques. Due to the variety and complexity of some samples, it is often necessary to properly prepare a sample and to perform a preconcentration of trace amounts of analytes. In line with the principles of Green Analytical Chemistry (GAC), it is important for an analytical procedure...
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Assessment of particular abdominal aorta section extraction from contrast-enhanced computed tomography angiography
PublikacjaThe aim of this work is to improve the accuracy of extraction of a particular abdominal aorta section and to reduce the distortion in three-dimensional Computed Tomography Angiography (CTA) images. Imaging modality and quality plays crucial role in the medical diagnostic process, thus ensuring high quality of images is essential at every stage of acquisition and processing.Noise is defined as a disturbance of the image quality...
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Development of SPME fiber coatings with tunable porosity for physical confinement of ionic liquids as an extraction media
PublikacjaExtending the use of ionic liquids in sample preparation techniques remains a challenge. This paper presents procedures enabling the easy application of ionic liquids to the SPME technique. For this purpose, two approaches for producing a porous silica coating on a metal rod were investigated. Two silica precursor and porogen systems were used in the research: K2SiO3 + Formamide and Tetramethyl-orthosilicate + Polyethylene oxide....
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Green energy extraction for sustainable development: A novel MPPT technique for hybrid PV-TEG system
PublikacjaThe Photovoltaic (PV) module converts only a small portion of irradiance into electrical energy. Most of the solar energy is wasted as heat, resulting in a rise in PV cell temperature and a decrease in solar cell efficiency. One way to harvest this freely available solar thermal energy and improve PV cell efficiency is by integrating PV systems with thermoelectric generators (TEG). This cogeneration approach of the hybrid PV-TEG...
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Giant Reed (Arundo donax L.) Fiber Extraction and Characterization for Its Use in Polymer Composites
PublikacjaThis work describes an extraction method for giant reed fibers from stems and leaves based on chemical soaking and crushing through a rolling mill. Obtained fibers, together with the shredded plant (stems + leaves), are characterized in terms of chemical composition, thermal stability, morphology, and crystallinity. Mechanical properties of fibers have also been assessed (single fiber tensile tests). The results show that the proposed...
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New achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix
PublikacjaWithout any doubt, the monitoring of compounds present in samples at trace or ultra-trace level usually requires a preliminary step of isolation and/or enrichment of analytes due to the fact that majority of analytical techniques are not sensitive enough for direct determination of trace compounds. On the other hand, sample preparation is considered as crucial part of whole analytical procedures, in particular in samples characterized...
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublikacjaA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...
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Understainding solid-phase microextraction: key factors influencing the extraction process and trends in improving the technique
PublikacjaAnalytical chemists are faced with the daunting challenges of accurately monitoring the state of the environment and the processes taking place in it and of determining an enormous range of analytes often present in trace and ultratrace amounts in sample matrixes with complex or variable compositions. Further challenges are presented by the need to introduce new methodologies into current analytical practice and equipment to comply...
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Charakterystyka wybranych tłuszczów użytych w gastronomii do głębokiego smażenia. Characteristics of selected fats used in catering industry for deep frying of food stuffs.
PublikacjaW wybranych losowo próbach tłuszczów smażalniczych z gastronomii oznaczono skład kwasów tłuszczowych, Liczbę Kwasową, Liczbę Anizydynową, Liczbę Nadtlenkową oraz zawartość i skład frakcji polarnej. Nie znaleziono korelacji pomiędzy stopniem nienasycenia badanych tłuszczów smażalniczych (LJ) i badanymi wyróżnikami jakości.
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Application of polyethylene glycol-coated iron oxide nanoparticles for magnetic solid phase extraction of copper from seawater samples and its determination by graphite furnace atomic absorption spectrometry using response surface methodology for optimization of extraction
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Collective Excitations in the Extended Hubbard Model with Intrasite Attraction
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Mutual Attraction: Siemens Activities in Italy 1855-1968
PublikacjaThe chapter deals with Siemens investments in Italy between 1855 and 1968. The contribution shows how the two war influenced the strategies of the company
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Application of additional factors supporting the microextraction process
PublikacjaDue to the fact that green analytical chemistry is of high importance, the past two decades have witnessed a rapid growth in the sample preparation area with special emphasis on simplification, miniaturization and automation of extraction procedures. In addition, to accelerate the extraction processes and to improve the separation of analytes, several enhanced parameters are applied. These factors include, ultrasounds, microwaves,...
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Enhanced photocatalytic activity of accordion-like layered Ti3C2 (MXene) coupled with Fe-modified decahedral anatase particles exposing {1 0 1} and {0 0 1} facets
PublikacjaNew composites consisting of decahedral anatase particles exposing {001} and {101} facets coupled with accordion-like layered Ti3C2 with boosted photocatalytic activity towards phenol and carbamazepine degradation were investigated. The photocatalysts were characterized with X-ray diffraction (XRD), diffuse reflectance spectroscopy (DR/UV–Vis), Brunauer-Emmett-Teller (BET) specific surface area, Raman spectroscopy, scanning electron...