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Wyniki wyszukiwania dla: IMPEDANCE SPECTROMETER
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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Determination of selenium by X-ray fluorescence spectrometry using dispersive solid-phase microextraction with multiwalled carbon nanotubes as solid sorbent
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Comprehensive two dimensional gas chromatography coupled with mass spectrometry as tool for characterization of the main pollutants present in atmospheric air in Gdansk
PublikacjaNowadays, the technique that is commonly used to identify and quantify the chemical compounds in gas sample is gas chromatography. The separation resolution in gas chromatography can be improved by applying the modulation technique. In this paper present is the most important information regarding the pollutants present in atmospheric air. The areas in which the tests were carried out are one of the largest industrial zones in...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part II: Gas-chromatography–mass spectrometry analysis
PublikacjaFlavouring compounds are an essential part of e-liquid products for cigarettes. In general, they are regarded as safe for ingestion, but they may have unrecognized risks when they are inhaled. In some cases, manufactures do not currently abide by the Tobacco Products Directive (2014/40/EU) and do not declare the detailed contents of e-liquids on their labels. To help evaluate the health impact of flavouring substances, there is...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublikacjaHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Determination of trace levels of eleven bisphenol A analogues in human blood serum by high performance liquid chromatography–tandem mass spectrometry
PublikacjaChemicals showing structural or functional similarity to bisphenol A (BPA), commonly called BPA analogues, have recently drawn scientific attention due to their common industrial and commercial application as a substitute for BPA. In the European Union, the use of BPA has been severely restricted by law due to its endocrine disrupting properties. Unfortunately, it seems that all BPA analogues show comparable biological activity,...
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A rapid and sensitive method for the quantitative analysis of ibuprofen and its metabolites in equine urine samples by gas chromatography-tandem mass spectrometry
PublikacjaIbuprofen is widely used in human and veterinary medicine for the treatment of chronic pain as well as rheumatic and musculoskeletal disorders. However, t he anal- gesic and anti-inflammatory properties of Ibuprofen have contributed to frequent drug abuse in equestr ian s ports. A sensitive and rapid gas chromatography with tandem mass spectrometry based method with a simple liquid-liquid extraction and deriva- tization requiring...
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Complementary Use of Multi-dimensional Gas Chromatography and Proton Transfer Reaction Mass Spectrometry for Identification of Rapeseed Oil Quality Indicators
PublikacjaThe change of concentration of various volatiles generated during frying may be an indicator of oil quality. Chemical compounds such as aldehydes, ketones, alcohols and carboxyl acids are the products of oxidation during thermal degradation of edible oils. Shown in this work is a complementary use of GC×GC-TOFMS and PTR-MS for the detection and determination of quality indicators of rapeseed oil. The former technique was used for...
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A rapid dispersive liquid–liquid microextraction of antimicrobial onion organosulfur compounds in animal feed coupled to gas chromatography-mass spectrometry
PublikacjaA rapid analytical procedure is proposed for determining two antimicrobial onion organosulfur compounds, propyl disulfide (PDS) and propyl propane thiosulfonate (PTSO), in animal feed. The use of PTSO as a natural ingredient in animal feed is allowed due to its antimicrobial activity against pathogenic organisms. Two analytical methodologies using gas chromatography coupled to mass spectrometry (GC-MS) are compared. After the extraction...
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublikacjaBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Analysis of chiral pharmaceutical residues in influent and effluent samples at racemic and enantiomeric level using liquid chromatography-tandem mass spectrometry
PublikacjaIn this work, two different chromatographic methods for seasonal monitoring of pharmaceutical residue in wastewater samples were developed. In the case of enantiomeric separation of selected compounds, LC-MS technique combining with vancomycin based chiral stationary phase was used. The performance of chiral analysis enabled to monitor the pharmaceutical contamination at the enantiomeric level. The d-SPE procedure was developed...
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Determination of robenidine in animal feeds by liquid chromatography coupled with diode-array detection and mass spectrometry after accelerated solvent extraction
PublikacjaRobenidyna (chlorowodorek 1,3-bis[(4-chlorobenzylideno)amino]guanidyny) jest stosowana w celu zapobiegania i leczenia kokcydiozy - pasożytniczej choroby układu pokarmowego wielu zwierząt hodowlanych (kozy, owce, króliki, drób) wywoływanej przez pierwotniaki należące do rzędu Eimeria tenella, E. Necatrix, E. Acervulina, E. Maxima, E. Brunetti, and E. Mivati. Robenidyna wykazuje stosunkowo wysoką skuteczność terapeutyczną, przy niewielkiej...
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Electrochemistry/mass spectrometry (EC/MS) for fast generation and identification of novel reactive metabolites of two unsymmetrical bisacridines with anticancer activity.
PublikacjaThe development of a new drug requires knowledge about its metabolic fate in a living organism, regarding the comprehensive assessment of both drug therapeutic activity and toxicity profiles. Electrochemistry (EC) coupled with mass spectrometry (MS) is an efficient tool for predicting the phase I metabolism of redox-sensitive drugs. In particular, EC/MS represents a clear advantage for the generation of reactive drug transformation...
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Linear impedance of V2O5 nanorods obtained at 903K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Linear impedance of 0.5Si3N4–99.5(40Na2O-20CaO-40P2O5) glass measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe linear electrical properties of 0.5Si3N4–99.5(40Na2O-20CaO-40P2O5) glass was measured by impedance spectroscopy method.
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Linear impedance of 1Si3N4–99(40Na2O-20CaO-40P2O5) glass measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe linear electrical properties of 1Si3N4–99(40Na2O-20CaO-40P2O5) glass was measured by impedance spectroscopy method.
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Linear impedance of V2O5 nanorods obtained at 913K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Linear impedance of V2O5 nanorods obtained at 893K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Impedance Evaluation of the Effect of Ru[sub 0.3]Ti[sub 0.7]O[sub 2] on Electrochemical Properties of Polymeric Conducting Electrodes Used in Cathodic Protection
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Electrochemical cell impedance spectra at Eoc+100mV
Dane BadawczeThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc+200mV
Dane BadawczeThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc-100mV
Dane BadawczeThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc-200mV
Dane BadawczeThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Linear impedance of 35P2O5-30Fe2O3-20Nb2O5-15TiO2
Dane BadawczeThe electrical properties of phosphate-iron glasses containing niobium and titanium were investigated. Glass samples of the composition of 35P2O5-30Fe2O3-20Nb2O5-15TiO2 (in %mol) were prepared by the conventional melt quenching technique. Appropriate amounts of reagents ((NH4)2HPO4 (≥99.9%, POCH), Fe2O3 (≥99.9%, POCH), Nb2O5 (≥99.9%, PLUKA AG) and TiO2...
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Nonlinear impedance of vanadate glasses containing BaTiO3
Dane BadawczeThe nonlinear impedance of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573...
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Linear impedance of 35P2O5-30Fe2O3-27.5Nb2O5-7.5TiO2
Dane BadawczeThe electrical properties of phosphate-iron glasses containing niobium and titanium were investigated. Glass samples of the composition of 35P2O5-30Fe2O3-27.5Nb2O5-7.5TiO2 (in %mol) were prepared by the conventional melt quenching technique. Appropriate amounts of reagents ((NH4)2HPO4 (≥99.9%, POCH), Fe2O3 (≥99.9%, POCH), Nb2O5 (≥99.9%, PLUKA AG) and...
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Linear impedance of vanadate glasses containing BaTiO3
Dane BadawczeThe linear impedance of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573...
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Linear impedance of V2O5 nanorods obtained at 923K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Nonlinear impedance of Bi2VO5.5 glass-ceramic annealed at 423 K was measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic annealed at 423 K was measured by impedance spectroscopy method.
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Linear impedance of 2Si3N4–98(40Na2O-20CaO-40P2O5) glass measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe linear electrical properties of 2Si3N4–98(40Na2O-20CaO-40P2O5) glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 50Bi2VO5.5-50SrB4O7 annealed glass at 593 K measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrcial properties of 50Bi2VO5.5-50SrB4O7 annealed glass was measured by impedance spectroscopy method.
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Linear impedance of 1SiO2–99(40Na2O-20CaO-40P2O5) glass measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe linear electrical properties of 1SiO2–99(40Na2O-20CaO-40P2O5) glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 40Bi2VO5.5-60SrB4O7 annealed glass at 593 K measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of 40Bi2VO5.5-60SrB4O7 glass annealed at 593 K was measured by impedance spectroscopy method.
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Ocena przydatności klasycznych metod pomiaru impedancji pętli zwarciowej do obwodów z wyłącznikami różnicowoprądowymi
PublikacjaW referacie przedstawiono wyniki badań zachowania się wyłączników różnicowoprądowych przy pomiarze impedancji pętli zwarciowej, wykonanym wybranymi miernikami. Badania przeprowadzono w obwodach z wyłącznikami różnicowoprądowymi o znamionowym prądzie różnicowym równym 30 mA, typu AC oraz typu A. Na podstawie przeprowadzonych badań i analiz zaproponowano sposób pomiaru impedancji pętli zwarciowej, który nie powoduje zbędnego zadziałania...
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Wpływ pomiaru dokładności napięć na wyznaczenie impedancji pętli zwarciowej metodą z przesunięciem y
PublikacjaMetoda z przesunięciem y to jedna z metod pomiaru impedancji pętli oparta na pomiarze składowych ortogonalnych napięcia umożliwiająca wyznaczenie wartości impedancji pętli znaczenie dokładniej niż metody klasyczne. Metoda ma posiada szereg zalet. Z racji tego poddawana jest ona ciągłym analizom metrologicznym pozwalającym na realizację modelu fizycznego miernika działającego w oparciu o tę metodę i odznaczającego się jeszcze lepszymi...
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Nowe rozwiązania pomiaru impedancji pętli zwarciowej przy odkształceniu krzywej napięcia w miejscu badania
PublikacjaW pracy przeanalizowano wpływ występujących w sieci czynników wpływających na błędy pomiaru, co umożliwiło ocenę, które znane metody i mierniki impedancji pętli zwarciowej mogą być stosowane w rzeczywistych układach elektroenergetycznych o wyraźnym odkształceniu krzywej napięcia. Przedstawiono nową metodę i przyrząd do pomiaru impedancji pętli zwarciowej oraz jej składowych ortogonalnych – rezystancji i reaktancji, która pozwala...
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STANY NIEUSTALONE TOWARZYSZĄCE POMIAROWI IMPEDANCJI PĘTLI ZWARCIA W OBWODACH WYJŚCIOWYCH ZASILACZY BEZPRZERWOWYCH UPS
PublikacjaW pracy przedstawiono metodykę i wyniki pomiarów stanów nieustalonych w zasilaczu bezprzerwowym (UPS) typu on - line. Do rejestracji zdarzeń po stronie zasilania i na wyjściu UPS wykorzystano dwa przyrządy do pomiaru jakości energii elektrycznej zsynchronizowane czasowo. Rejestratory kompresują uzyskane dane pomiarowe, co może wprowadzać dodatkowe błędy pomiaru wielkości mierzonych – napięć i prądów. Dodatkowe rejestracje oscyloskopem...
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Szacowanie standardowej niepewności złożonej pomiaru impedancji pętli zwarciowej wyznaczonej metodą z przesunięciem psi
PublikacjaW niniejszym artykule zaprezentowano wyniki szacowania standardowej niepewności złożonej pomiaru impedancji pętli zwarciowej wyznaczonej metodą z przesunięciem . Przeanalizowano wpływ niepewności rezystancji obciążenia pomiarowego, niepewności pomiaru napięć, niepewności pomiaru okresu oraz przesunięcia psi na dokładność pomiaru impedancji pętli zwarcia.
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Metody usuwania zakłóceń podczas pomiarów polowych widm Ramana
PublikacjaW pracy zostały scharakteryzowane źródła zakłóceń występujące podczas pomiarów widm Ramana w warunkach polowych oraz sposoby redukcji ich wpływu na jakość rejestrowanych widm. Zaprezentowano wpływ czasu integracji na jakość rejestrowanych widm w przypadkach, gdy szumy własne spektrometru mają składową typu 1/f, dominującą w zakresie małych częstotliwości. Przedstawiono także wyniki uzyskane podczas pomiarów z detekcją synchroniczną,...
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Comparison of peptide cancer signatures identified by mass spectrometry in serum of patients with head and neck, lung and colorectal cancers: Association with tumor progression
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Solid phase extraction with flame atomic absorption spectrometry for determination of traces of Ca, K, Mg and Na in quality control of white sugar
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Sensitive Determination of Cd in Small-Volume Samples by Miniaturized Liquid Drop Anode Atmospheric Pressure Glow Discharge Optical Emission Spectrometry
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Determination of mercury in mosses by novel cold vapor generation atmospheric pressure glow microdischarge optical emission spectrometry after multivariate optimization
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Development of direct-current, atmospheric-pressure, glow discharges generated in contact with flowing electrolyte solutions for elemental analysis by optical emission spectrometry
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Hanging drop cathode-atmospheric pressure glow discharge as a new method of sample introduction for inductively coupled plasma-optical emission spectrometry
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Determination of methylcyclopentadienyl-manganese tricarbonyl in gasoline and water via ionic-liquid headspace single drop microextraction and electrothermal atomic absorption spectrometry
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Boron-doped carbon nanowalls for fast and direct detection of cytochrome C and ricin by matrix-free laser desorption/ionization mass spectrometry
PublikacjaDetecting proteins via surface assisted laser desorption/ionization mass spectrometry (SALDI-MS) method is still highly challenging, and only few examples of nanomaterials have been demonstrated to perform such detection so far. In this study, carbon nanowalls (CNWs), vertically aligned graphene sheet-based materials, presenting specific morphology, dimensions, and boron doping levels have shown improved performances for both qualitative...
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Investigation of the Dynamism of Nanosized SOA Particle Formation in Indoor Air by a Scanning Mobility Particle Sizer and Proton-Transfer-Reaction Mass Spectrometry
PublikacjaTerpenes are VOCs of particular importance, since they are emitted from a wide range of indoor sources and are considered to be precursors of Secondary Organic Aerosol (SOA) formation. It has been proven that SOA particles, especially nanosized ones, pose a threat to human health. In this research, experiments with the application of an environmental chamber and real-time measurement techniques were carried out to investigate in...
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Carbon nanowalls: A new versatile graphene based interface for laser desorption/ionization-mass spectrometry detection of small compounds in real samples.
PublikacjaCarbon nanowalls, vertically aligned graphene nanosheets, attract attention owing to their tunable band-gap, high conductivity, high mechanical robustness, high optical absorbance and other remarkable properties. In this paper, we report for the first time, the use of hydrophobic boron-doped carbon nanowalls (CNWs) for laser desorption/ionization of small compounds and their subsequent detection by mass spectrometry (LDI-MS). The...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part I: Liquid chromatography-tandem mass spectrometry analysis
PublikacjaLiquid chromatography-tandem mass spectrometry with electrospray ionization (HPLC-ESI–MS/MS) methods were developed for the simultaneous determination of 42 flavouring compounds and nicotine in liquids for e-cigarettes. The chromatographic separation was performed using an Ace® Ultracore™ SuperC18™ (100 × 2.1 mm, 2.5 μm) column in both acidic and alkaline pH conditions to separate all the compounds. A simple “dilute & shoot” approach...