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Sustainable synthesis of cyclic carbonates from bio‐based polyether polyol: the structure characterization, rheological behaviour and thermal properties
PublicationThe cycloaddition of CO2 to epoxides represents a green efficient method to form bis(cyclic carbonate)s. The main purpose of the work reported in this paper was to examine the effect of the gas flow rate (20, 40, 60 and 100 mL min–1) during carbonation on the conversion yield, chemical structure, rheological behaviour and thermal properties of the prepared compounds. A series of new bis(cyclic carbonate)s was obtained from bio‐based...
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Towards Computer-Aided Graphene Covered TiO2-Cu/(CuxOy) Composite Design for the Purpose of Photoinduced Hydrogen Evolution
PublicationIn search a hydrogen source, we synthesized TiO2-Cu-graphene composite photocatalyst for hydrogen evolution. The catalyst is a new and unique material as it consists of copper-decorated TiO2 particles covered tightly in graphene and obtained in a fluidized bed reactor. Both, reduction of copper from Cu(CH3COO) at the surface of TiO2 particles and covering of TiO2-Cu in graphene thin layer by Chemical Vapour Deposition (CVD) were...
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Charge dependence of fragmentation process induced by ion collisions with furan molecule
PublicationThe goal of this work is to describe the system evolution after ion-molecule interaction. We combine different quantum chemistry and statistical mechanics approaches in order to give extended description of the process. Herein we report on a recent study of the fragmentation mechanism of neutral, singly- and doubly-ionized furan molecule in the gas phase.
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Public Participation practice versus economic pressure: transformation of the Gdansk Coastal Strip
PublicationThe paper focuses on the issue of public participation in the areas that are particularly sensitive to the transformation processes based on the case study of Gdańsk Coastal Strip. Moreover the article presents the outcome of an innovative attempt at promotion of public participation introduced in university education that was built on the experiences gathered during elaboration of the pro publico bono project of the Coastal Strip...
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Nanostructure of the laser-modified transition metal nanocomposites for water splitting
PublicationAlthough hydrogen is considered by many to be the green fuel of the future, nowadays it is primarily produced through steam reforming, which is a process far from ecological. Therefore, emphasis is being put on the development of electrodes capable of the efficient production of hydrogen and oxygen from water. To make the green alternative possible, the solution should be cost-efficient and well processable, generating less waste...
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Assessment and design of greener deep eutectic solvents – A multicriteria decision analysis
PublicationDeep eutectic solvents (DES) are often considered as green solvents because of their properties, such as negligible vapor pressure, biodegradability, low toxicity or natural origin of their components. Due to the fact that DES are cheaper than ionic liquids, they have gained many applications in a short period of time. However, claims about their greenness sometimes seem to be exaggerated. Especially, bearing in mind lots of data...
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Application of molecularly imprinted polymers in analytical chiral separations and analysis
PublicationOver the last two decades the process of development and application of a new types of molecular imprinted polymer (MIP) sorbents in the field of analytical chemistry have been widely described in the literature. One of the new trends in analytical chemistry practice is the use of new types of MIP sorbents as specific sorption materials constituting the stationary phase in advanced separation techniques. The following review paper...
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Cognitive network model dedicated to transport system telematics
PublicationThe paper defines the concept of cognitive radio, in the context of transport systems, with particular emphasis on modern ecological concept of “green cognitive radio”. In addition, in the paper a modified cognitive network model dedicated to transport system telematics is proposed and presented. Algorithms to support the functioning of the cognitive radio are discussed. Sensors necessary to use the network to support cognitive...
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Lithuania inland waterways and its prospects
PublicationInland waterways have some traditions in Lithuania and in neighbor Countries, but during last 50 years other modes of transport move out inland waterway transport from real economical activity. In the same time inland waterways is the main green and sustainable transport system. In this article are presented analysis situation, methodology for the ships optimal using in inland waterways, forecasting of the possible cargo and passenger...
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer Du-145 cells
Open Research DataThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer Du-145 cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to normal MRC-5 cells
Open Research DataThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to normal MRC-5 cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...
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Analysis of arsenic species in environmental samples
PublicationMany analytical methods for determining arsenic in various forms in environmental samples have been developed in recent years. The main objective of this review article is the presentation and comparison of the three principal techniques for the determination arsenic compounds, namely: hydride generation (HG), voltammetry and chromatography (liquid chromatography including high-performance liquid chromatography (HPLC), and gas...
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Lead(II) coordination polymers with imidazole-4- and pyrazole-3-carboxylate isomeric linkers: Structural diversity and luminescence properties
PublicationUsing 1H-imidazole-4-carboxylic acid (4imCOOH) and 1H-pyrazole-3-carboxylic acid (3pyrCOOH) coordination polymers [Pb(4imCOO)2(H2O)]n (1) and [Pb2(3pyrCOO)4]n (2) were constructed. Obtained polymers were characterized via FT-IR, X-ray, PL and TG methods. The coordination polyhedron around Pb(II) in 1 is described as distorted pentagonal pyramid with hemidirected coordination sphere (based on DFT calculations). Compound 2 consists...
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Fluorine ions in photocatalysts’ synthesis: an obstacle or an ally? The investigation of photocatalysts in Ti-O-F system
PublicationTitanium(IV) oxide (TiO2) is one of the most promising photocatalysts, which is expected to be applied in the photocatalytic degradation of xenobiotics. For sustainable development and green chemistry approach recently, much effort has been paid to enhance TiO2 photocatalytic activity in UV-vis light by modifying its structure. The photocatalytic process’s complexity cannot be simply described as electron-hole pairs generations...
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Microscopy analysis of A549 and H460 cells' mitochondria after exposure to TXT2 and TXT4
Open Research DataThe data set contains live-cell imaging of A549 and H460 cells' mitochondria after exposure to TXT2 and TXT4. Cells were exposed for 6 h to the tested compounds at their IC90 concentration or to DMSO. Then, mitochondrial labelling was performed by incubating the cells with a MitoTracker Green FM probe (Thermo Fisher Scientific) and Hoechst 33342 (Thermo...
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SEM micrographs of aluminium corrosion in alkaline media with various bee products as corrosion inhibitors
Open Research DataThis dataset contains various scanning electron microscopy (SEM) micrographs of AA5754 aluminum alloy samples exposed to the corrosive alkaline environment without and with the addition of various bee products to act as green corrosion inhibitors. The products are bee pollen, honey, and putty. They were investigated in bicarbonate buffer (pH =10 or...
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Nowe substancje psychoaktywne Cz. III. Syntetyczne katynony-charakterystyka, metody oznaczania i wyzwania analitycznje
PublicationSyntetyczne katynony to druga co do liczebności (po syntetycznych kannabinoidach) grupa nowych substancji psychoaktywnych będących składnikiem dopalaczy zabezpieczanych przez policję w nielegalnym handlu. Substancje te po raz pierwszy wykryto w Europie w 2004 r., a do końca roku 2015 zidentyfikowano aż 103 nowe związki z tej grupy. Możliwość wprowadzania dodatkowych grup funkcyjnych w strukturę katynonu pozwala na niezwykle wiele...
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Dopants and gas modifiers in ion mobility spectrometry
PublicationThe ion mobility techniques, including the most commonly used drift-tube ion mobility spectrometry (IMS) and differential mobility spectrometry (DMS), are used successfully for the detection of a wide range of organic compounds in the gas phase. In order to improve detection quality, admixtures are added to gas streams flowing through the detector. Dopants mostly prevent the ionization of interfering chemicals however, better detection...
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Oleksandr Melnychenko dr hab.
PeopleOleksandr Melnychenko works as a professor in a group of research and teaching staff at the Department of Finance of the Faculty of Management and Economics, the Gdańsk University of Technology; is a sworn translator of the Ukrainian language in Poland; an entrepreneur with many years of experience in running his own business and managing the companies' finances; has experience working in a commercial bank in a position dealing...
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The possibility of use by-products for synthesis of emulsifiers
PublicationIn the last years the interest in use of materials originated from natural sources, e.g. vegetables to produce attractive products still grows. According to that, also the synthesis of these products should be adequate to the green chemistry requirements. The typical example observed in recent years focuses on utlization of bioglycerol - the by - product of global biodiesel manufacturing. The still growing production of biodiesel...
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Novel fast analytical method for indirect determination of MCPD fatty acid esters in edible oils and fats based on simultaneous extraction and derivatization
PublicationA novel method for indirect determination of MCPD esters levels in lipid samples has been developed. The method is based on combination of extraction and derivatisation in the same sample preparation step. It is achieved by the application of diethyl ether as extraction solvent for isolation of released from esterified forms analytes from water phase and dilution solvent for solid PBA – derivatisation agent. It is a noteworthy...
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Deep eutectic solvents microbial toxicity: Current state of art and critical evaluation of testing methods
PublicationDeep eutectic solvents (DESs) were described at the beginning of 21st century and they consist of a mixture of two or more solid components, which gives rise to a lower melting point compared to the starting materials. Over the years, DESs have proved to be a promising alternative to traditional organic solvents and ionic liquids (ILs) due to their low volatility, low inflammability, easy preparation, and usually low cost of compounds...
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Deep eutectic solvents – A new platform in membrane fabrication and membrane-assisted technologies
PublicationDeep eutectic solvents (DESs) are a new class of solvents that can offset some of the primary drawbacks of typical solvents and ionic liquids (ILs). Since DESs fall into the guidelines of “Twelve Principles of Green Chemistry”, their implementation in several types of applications has exponentially increased over the last years. The usage of DESs has been directed to the designing, manufacture and purification of new materials...
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Monitoring and analytics of semivolatile organic compounds (SVOCs) in indoor air
PublicationThis paper reviews literature information on the behaviour of semivolatile organic compounds (SVOCs) in the indoor environment, as well as the most likely emission sources. The consecutive stages of analytical procedures used for monitoring SVOCs in indoor environments are described. The most common approaches used for collecting samples from the gas and particulate phases are mentioned. The paper discusses and compares various...
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Amyloidosis - Male, 94 - Tissue image [5300730025896341]
Open Research DataThis is the histopathological image of TONSIL tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Amyloidosis - Male, 94 - Tissue image [5300730025898061]
Open Research DataThis is the histopathological image of TONSIL tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Impact of Urbanization on Stormwater Runoff from a Small Urban Catchment: Gdańsk Małomiejska Basin Case Study
PublicationThis paper deals with the impact of different forms of urbanization on the basin outflow. The influence of changes in land cover/use, drainage system development, reservoirs, and alternative ways of stormwater management (green roofs, permeable pavements) on basin runoff was presented in the case of a small urban basin in Gdańsk (Poland. Seven variants of area development (in the period of 2000-2012) – three historical and four...
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Silver nanoparticles incorporated with superior silica nanoparticles-based rice straw to maximize biogas production from anaerobic digestion of landfill leachate
PublicationTreating hazardous landfill leachate poses significant environmental challenges due to its complex nature. In this study, we propose a novel approach for enhancing the anaerobic digestion of landfill leachate using silver nanoparticles (Ag NPs) conjugated with eco-friendly green silica nanoparticles (Si NPs). The synthesized Si NPs and Ag@Si NPs were characterized using various analytical techniques, including transmission electron...
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Sintering Parameter Investigation for Bimetallic Stainless Steel 316L/Inconel 718 Composite Printed by Dual-Nozzle Fused Deposition Modeling
PublicationFused deposition modeling (FDM) nowadays offers promising future applications for fabricating not only thermoplastic-based polymers but also composite PLA/Metal alloy materials, this capability bridges the need for metallic components in complex manufacturing processes. The research is to explore the manufacturability of multi-metal parts by printing green bodies of PLA/multi-metal objects, carrying these objects to the debinding...
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Chromatographic and Spectroscopic Identification and Recognition of Natural Dyes, Uncommon Dyestuff Components, and Mordants: Case Study of a 16th Century Carpet with Chintamani Motifs
PublicationA multi-tool analytical practice was used for the characterisation of a 16th century carpet manufactured in Cairo. A mild extraction method with hydrofluoric acid has been evaluated in order to isolate intact flavonoids and their glycosides, anthraquinones, tannins, and indigoids from fibre samples. High-performance liquid chromatography coupled to spectroscopic and mass spectrometric detectors was used for the identification of...
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CLAY MINERALS – MINERALOGY AND PHENOMENON OF CLAY SWELLING IN OIL & GAS INDUSTRY
PublicationAmong the minerals found in the earth's crust, clay minerals are of the widest interest. Due to the specific properties such as plasticity, absorbing and catalytic properties clay minerals are used in many industries (oil & gas, chemistry, pharmacy, refractory technology, ceramics etc.). In drilling, a phenomenon of swelling clays is frequently observed. It has an important impact on the cementing quality. During the last few decades...
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Nowoczesne koncepcje integracji usług w systemie BeesyCluster
PublicationOpisano funkcje aktualnej wersji systemu BeesyCluster jakowarstwy pośredniej w dostępie do rozproszonych zasobów wraz podsystemami integracji usług, wyboru usług oraz ich wykonania. Zaprezentowano rozszerzenia podsystemu integracji usług zorientowane na green computing. Omówiono problemy inteligentnego wyszukiwania usług, wykorzystanie GPU, współpracę z urządzeniami mobilnymi oraz przetwarzanie w przestrzeniach inteligentnych.Dodatkowo...
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Ultrasound assisted solvent extraction of porous membrane-packed samples followed by liquid chromatography-tandem mass spectrometry for determination of BADGE, BFDGE and their derivatives in packed vegetables
PublicationThe problem of the presence of trace organic pollutants in food is of growing importance due to increasing awareness about their impact on newborns, infants and adults of reproductive age. Despite the fact that packaged food products offer many advantages, packaging can be a source of contamination for stored food. Thus, monitoring such pollution in food is of high importance. In this work, a novel methodology based on the solvent...
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Turmeric nanofiber-encapsulated natural product formulation act as a phytogenic feed additive—A study in broilers on growth performance, biochemical indices of blood, and E. coli in cecum
PublicationA phytogenic feed additive (PFA) formulation was prepared with bioactive molecules—curcuminoids, gingerol, and carvacrol by encapsulating in nanofiber isolated from turmeric spent (turmeric nanofiber, TNF). This formulation was completely characterized by scanning electron microscope, ultra performance liquid chromatography, and gas chromatography and evaluated for its efficacy. PFA-encapsulated TNF (PFA@TNF) considerably increased...
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PULSE and ECG measurement from the hand with single fingers - elbows resting on the armrests of the chair - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows in the air - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Second Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with single fingers - elbows resting on the armrests of the chair - Second Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows in the air - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with single fingers - elbows resting on the armrests of the chair - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Second Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows to the body - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows in the air - Second Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Second Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...