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Search results for: 1,4,7,10-TETRAAZACYKLODODEKAN
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Rekonstrukcja ewolucji układu przestrzennego średniowiecznego miasta i portu Szczecin Reconstruction of the Spatial Evolution of the Medieval City and Port of Szczecin
PublicationPraca rekonstruuje ewolucję układu osadniczego Szczecina w okresie od połowy VIII w. do początku XIV w., w oparciu o interpretację dostępnej literatury naukowej dotyczącej historii i archeologii Szczecina oraz metodę analizy planistycznej. Bardzo istotnym elementem opisu struktury urbanistycznej wczesnośredniowiecznego Szczecina było określenie roli i położenia portu. W wyniku analizy zmian układu przestrzennego miasta w omawianym...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Comparing some convolution-based methods for creation of surround sound. W: [CD-ROM] Collected papers. First Pan-American/Iberian Meeting on Acoustics. 144 Meeting of the Acoustical Society of America. III Iberoamerican Cong- ress of Acoustics. 9o Mexican Congress of Acoustics. Cancun, Q. R. Mxico, 2-6 Dec. 2002. [B.m.:ASA]**2002 paper 2pPP22, 7 s. 8 rys. 1 tab. bibliogr. 12 poz. system nagrań dźwięku dookólnego z wykorzystaniem splotu odpowiedzi impul- sowej sali.
PublicationW referacie przedstawiono eksperymenty związane z symulacją dźwięku dookól-nego w sali koncertowej. W tym celu wykorzystano splot odpowiedzi impulsowejz danego wnętrza (wielokanałowe nagrania odpowiedzi impulsowej) z nagraniamiz komory bezechowej. Uzyskany w ten sposób sygnał został następnie przypisa-ny do odpowiednich kanałów w systemie dookólnym. Uzyskane w ten sposób nag-rania były następnie porównywane w testach subiektywnych...
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Structural Variety of Cobalt(II), Nickel(II), Zinc(II), and Cadmium(II) Complexes with 4,4′-Azopyridine: Synthesis, Structure and Luminescence Properties
PublicationSelf-assembled bi- and polymetallic complexes of CoII, NiII, ZnII, and CdII were obtained by the reaction of 4,4′-azopyridine (azpy) with metal tri-tert-butoxysilanethiolates (Co, 1; Cd, 2), acetylacetonates (Ni, 3; Zn, 4), and acetates (Cd, 5). All compounds were characterized by single-crystal X-ray structure analysis, elemental analysis, FTIR spectroscopy, and thermogravimetry. Complexes 1, 2 and 4, 5 exhibit diverse structural...
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Wykonanie pomiarów wraz z opracowaniem opinii naukowo-technicznej dotyczącej geometrii rotundy palmiarni wykonanej w ramach zadania: Rewitalizacja i przebudowa kompleksu budynku palmiarni w ogrodzie botanicznym w Parku Oliwskim im. Adama Mickiewicza w Gdańsku-Oliwie"
PublicationCelem opracowania jest wykonanie skanu laserowego konstrukcji rotundy palmiarni realizowanej w ramach zadania „Rewitalizacja i przebudowa kompleksu budynku palmiarni w ogrodzie botanicznym w Parku Oliwskim im. Adama Mickiewicza w Gdańsku Oliwie”, ocena zgodności geometrii konstrukcji z dokumentacją projektową oraz wydanie opinii nt dalszego postępowania z konstrukcją. Zakres opracowania obejmuje: 1) analizę dokumentacji obiektu; 2)...
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Complexation of amino acids derivatives in water by calix[4]arene phosphonic acids
PublicationSeries of the calix[4]arene phosphonic acids with various substituents at the lower rim was synthesized. Complexing properties of these receptors towards methyl esters of six amino acids strongly depended on the calix[4]arene conformation flexibility. The complex formation processes were monitored using 1H NMR spectroscopy (deuterated phosphate buffer at pD 7.3, 22 oC) and association constant values were evaluated. Inherently...
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Lower rim substituted tert-butylcalix[4]arenes.Part 8: Calix[4]arenes with dialkoxyphosphoryl functions. Synthesis and complexing properties
PublicationW pracy przedstawiono syntezę i charakterystykę otrzymanych związków (1, 2), pochodnych alkoksyfosforylowych p-tert-butylokaliks[4]arenu: 5,11,17,23-tetra-tert-butylo-25,26,27,28-tetrakis(3-diizopropoksyfosforylopropoksy)kaliks[4]arenu (1) oraz 5,11,17,23-tetra-tert-butylo-25,26,27,28-tetrakis(3-methoksyetoksyfosforylopropoksy)kaliks[4]arenu (2). Zbadano właściwości jonoforowe związków 1 i 2 w membranie elektrod jonoselektywnych,...
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Polityczne, prawne i ekonomiczne aspekty ustawy o języku polskim
PublicationW artykule omówiono proces przyjmowania przez Sejm i Senat RP ustawy o języku polskim z 7 października 1999 r. oraz jej nowelizacji z 4 marca 2004 r. Przestawiono aspekty polityczne, prawne i ekonomiczne tej ustawy oraz wybrane komentarze prasowe.
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New 2-[(4-Amino-6-N-substituted-1,3,5-triazin-2-yl)methylthio]-N-(imidazolidin-2-ylidene)-4-chloro-5-methylbenzenesulfonamide Derivatives, Design, Synthesis and Anticancer Evaluation
PublicationIn the search for new compounds with antitumor activity, new potential anticancer agents were designed as molecular hybrids containing the structures of a triazine ring and a sulfonamide fragment. Applying the synthesis in solution, a base of new sulfonamide derivatives 20–162 was obtained by the reaction of the corresponding esters 11–19 with appropriate biguanide hydrochlorides. The structures of the compounds were confirmed...
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Solubility of Carbon Dioxide in Deep Eutectic Solvents Based on 3-Amino-1-Propanol and Tetraalkylammonium Salts at Low Pressure
PublicationDeep eutectic solvents (DESs) became an object of a great interest as an alternative to ionic liquids (ILs) and commonly used in CO2 capture amine solutions. In the present study, five different DESs based on 3-amino-1-propanol as physical-chemical CO2 absorbents were used. The composition was chosen in order to estimate the effects of hydrogen bond acceptor:hydrogen bond donor (HBA:HBD) molar ratio, anion type and length of alkyl...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec in order to examine the fast fluctuations of sample temperature during charging - discharging...
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Janusz Rachoń prof. dr hab. inż.
PeopleSprawował urząd rektora w latach 2002-2008 Urodził się 11 sierpnia 1946 r. w Nowym Sączu. Studia wyższe ukończył w 1969 r. na Wydziale Chemicznym Politechniki Gdańskiej, uzyskując tytuł magistra inżyniera chemika. W 1969 r. rozpoczął pracę na Wydziale Chemicznym Politechniki Gdańskiej, na którym uzyskał w 1975 r. doktorat, a w 1985 r. habilitację. Na stanowisko docenta został powołany w 1989 r., na stanowisko profesora nadzwyczajnego...
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The Usefulness of Cyclic Diamidines with Different Core-substituents as Antitumor Agents
PublicationA series of related polycationic compds. has been screened for potential antitumor activity by the NCI's in vitro testing (one dose primary anticancer assay and the NCI-60 full panel screening). The GI50 values of triazines 3 and 4 are on av. 1.9 μM and 2.4 μM, resp. Furan 8 deserves mention too (1.9 μM). The biol. test results showed that carbazole 10 possessed cytotoxic activity in the nanomolar range, much better than...
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Invasive breast carcinoma of no special type - Female, 62 - Tissue image [5020730020706971]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Invasive breast carcinoma of no special type - Female, 62 - Tissue image [5020730020704211]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Myxofibrosarcoma - Male, 70 - Tissue image [9270729565548921]
Open Research DataThis is the histopathological image of CONNECTIVE, SUBCUTANEOUS AND OTHER SOFT TISSUES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Invasive breast carcinoma of no special type - Female, 62 - Tissue image [5020730020705271]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Invasive breast carcinoma of no special type - Female, 62 - Tissue image [5020730020704571]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Myxofibrosarcoma - Male, 70 - Tissue image [9270729565544131]
Open Research DataThis is the histopathological image of CONNECTIVE, SUBCUTANEOUS AND OTHER SOFT TISSUES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Invasive breast carcinoma of no special type - Female, 62 - Tissue image [5020730020705251]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Myxofibrosarcoma - Male, 70 - Tissue image [9270729565549431]
Open Research DataThis is the histopathological image of CONNECTIVE, SUBCUTANEOUS AND OTHER SOFT TISSUES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Myxofibrosarcoma - Male, 70 - Tissue image [9270729565547311]
Open Research DataThis is the histopathological image of CONNECTIVE, SUBCUTANEOUS AND OTHER SOFT TISSUES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Coupling of Blood Pressure and Subarachnoid Space Oscillations at Cardiac Frequency Evoked by Handgrip and Cold Tests: A Bispectral Analysis
PublicationThe aim of the study was to assess blood pressure–subarachnoid space (BP–SAS) width coupling properties using time–frequency bispectral analysis based on wavelet transforms during handgrip and cold tests. The experiments were performed on a group of 16 healthy subjects (F/M; 7/9) of the mean age 27.2 ± 6.8 years and body mass index of 23.8 ± 4.1 kg/m². The sequence of challenges was first handgrip and then cold test. The handgrip...
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Przesnięcie (w 1967r.) wartowni nr 1 na Westerplatte w Gdańsku
PublicationOmówiono znaczenie wartwni nr 1 podczas obrony Westerplatte w dniach od 1 do 7 września 1939r. Wskazano na historyczne znaczenie tego obiektu budowlanego. Omówiono technologie jego przesunięcia o około 80 m podczas rozbudowy morskiego portu w Gdańsku w 1967 roku.
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Determination of Sodium Ion Diffusion Coefficient in Tin Sulfide@Carbon Anode Material Using GITT and EIS Techniques
PublicationThe electroanalytical behavior of SnSx (x = 1, 2) encapsulated into a carbon phase was studied using the galvanostatic intermittent titration technique (GITT) and electrochemical impedance spectroscopy (EIS). These techniques are widely utilized in battery systems to investigate the diffusion of alkali metal cations in anode and cathode materials depending on the concentration of ions in the host material. Here, we report different...
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Insightful studies of AuCu nanostructures deposited on Ti platform: Effect of rapid thermal annealing on photoelectrochemical activity supported by synchrotron radiation studies
PublicationIn this work, we present the influence of annealing atmospheres during rapid thermal annealing (40◦C/s) on nanostructured Ti platforms modified by 10 nm layer of AuCu alloy obtained via magnetron sputtering. The AuCu/Ti platform annealed under hydrogen atmosphere exhibits the best photoelectrochemical activity under visible light, i.e. 27 times higher photocurrent than for pure Ti dimpled platform, and the lowest reflectance with minimum...
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Badania stabilności biologicznej wody w wybranych systemach wodociągowych
PublicationW pracy przedstawiono wyniki badań mikrobiologicznych wody powierzchniowej i wód podziemnych z rejonu Trójmiasta, które zasilają systemy dystrybucji charakteryzujące się nikim stosunkiem powierzchni kontaktu do objętości przesyłanej wody (≈0,65) w aspekcie ich stabilności biologicznej. Dokonano oceny skuteczności zastosowanych procesów uzdatniania w usuwaniu ogólnej liczby bakterii (OLB), a w badaniach laboratoryjnych określono...
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The Optical Coherence Tomography and Raman Spectroscopy for Sensing of the Bone Demineralization Process
PublicationThe presented research was intended to seek new optical methods to investigate the demineralization process of bones. Optical examination of the bone condition could facilitate clinical trials and improve the safety of patients. The authors used a set of complementary methods: polarization-sensitive optical coherence tomography (PS-OCT) and Raman spectroscopy. Chicken bone samples were used in this research. To stimulate in laboratory...
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Analysis of pounding between adjacent buildings founded on different soil types
PublicationEarthquake-induced pounding was experienced in many previous earthquakes and it was found to be a critical issue. This study investigates the effect of pounding between buildings founded on the same and different soil types. Three 3-D buildings with 4, 6 and 8 storeys were considered in this study. Three pounding scenarios were taken into account, i.e. pounding between 4-storey and 6-storey buildings, between 4-storey and 8-storey...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 534 mA. Sample J53, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 534 mA. Sample J53, experiment run #1. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 420 mA. Sample 103, run#1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #1. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,8 V at 241 mA. Sample 24, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,8 V and discharged to 10 mV by constant current 241 mA, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 250 mA. Sample 23, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 250 mA. Sample 23, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 241 mA. Sample 24, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 241 mA, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,1 V at 561 mA. Sample 71, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,1 V and discharged to 10 mV by constant current 561 mA. Sample 71. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 204 mA. Sample 51, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 204 mA. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 561 mA. Sample 71, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 561 mA. Sample 71, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 560 mA. Sample 42, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 560 mA. Sample 42. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 306 mA. Sample 51, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 306 mA. Experiment run #1. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 102 mA. Sample 51, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 102 mA. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 168 mA. Sample 115, run#1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 168 mA. Sample 115. Experiment rum #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,1 V at 290 mA. Sample 82, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,1 V and discharged to 10 mV by constant current 290 mA. Sample 82. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 290 mA. Sample 82, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 290 mA. Sample 82. Experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Synthesis and steroid sulfatase inhibitory activities of N-alkanoyl tyramine phosphates and thiophosphates
PublicationA series of phosphate and thiophosphate analogs based on the frameworks of N-alkanoyl tyramines have been synthesized and biologically evaluated. Their binding modes have been modeled using docking techniques. The inhibitory effects of the synthesized compounds were tested on STS isolated from the human placenta as well as the MCF-7, MDA-MB-231 and SkBr3 cancer cell lines. Most of the new STS inhibitors possessed potent activity...
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Phospholipid-functionalized gold electrode for cellular membrane interface studies - interactions between DMPC bilayer and human cystatin C
PublicationThis work describes the electrochemical studies on the interactions between V57G mutant of human cystatin C (hCC V57G) and membrane bilayer immobilized on the surface of a gold electrode. The electrode was modified with 6-mercaptohexan-1-ol (MCH) and 1,2-dimyristoyl-sn-glycero-3-phosphocholine (DMPC). DMPC was used as a membrane mimetic for monitoring electrochemical changes resulting from the interactions between the functionalized...
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Flow maldistribution and its mitigation in mini heat exchangers
PublicationIn the present paper, a detailed numerical investigation has been carried out to analyze the flow maldistribution in 50 parallel 1 mm x 1 mm rectangular minichannels and 1 mm depth minigap section with rectangular, trapezoidal, triangular or concave mani-folds in Z-type flow configuration (16 different cases). The working medium was ethanol and the mass flow rate was 5×10-4 kg/s. Both sections was heated from the bottom side. Heat...
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Microwave-assisted synthesis of a TiO2-CuO heterojunction with enhanced photocatalytic activity against tetracycline
PublicationA microwave method was used for the synthesis of TiO2-CuO oxide systems. A detailed investigation was made of the effect of the molar ratio of components (TiO2:CuO=9:1, 7:3, 5:5, 3:7, 1:9) on the crystalline structure and morphology. Transmission electron microscopy (TEM) confirmed the presence of octahedral and rod-shaped titania particles and sheet copper(II) oxide particles; moreover, HRTEM analysis indicated the presence of...
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Understanding the kinetics and atmospheric degradation mechanism of chlorotrifluoroethylene (CF2=CFCl) initiated by OH radicals
PublicationThe atmospheric degradation of chlorotrifluoroethylene (CTFE) by OH˙ was investigated using density functional theory (DFT). The potential energy surfaces were also defined in terms of single-point energies derived from the linked cluster CCSD(T) theory. With an energy barrier of −2.62 to −0.99 kcal mol−1 using the M06-2x method, the negative temperature dependence was determined. The OH˙ attack on Cα and Cβ atoms (labeled pathways...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #2. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #3. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...