Search results for: FILTRY GM-LC
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The potential of LC–MS technique in direct analysis of perfume content
PublicationPerfumes are products that consist of a wide range of natural and synthetic compounds. Due to complex composition, the determination of their ingredients is a difficult task. Most of the perfume components are either volatile or semi-volatile; however, most of the attention has been paid to volatile ones, and thus, gas chromatography or electronic noses are generally used. Nevertheless, in this study, liquid chromatography coupled...
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Filtry Kalmana i sterowanie w warunkach losowych
e-Learning CoursesPrzedmiot omawia podstawy filtracji Kalmana oraz zasady sterowania obiektami, na które działają zakłócenia losowe.
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Zwierzęce szczątki kostne z dawnego grodu w Dusinie, stanowisko 1, gm. Gostyń
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GM Crops & Food-Biotechnology in Agriculture and the Food Chain
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Determination of free tyrosine in equestrian supplements by LC–MS/MS and comparison of its quantity with total free amino acids content in view of doping control
PublicationThe reports on the probable beneficial impact of tyrosine (TYR) supplementation on performance enhancement have contributed to the growth of interest in TYR in equestrian sports field and related industries, such as the manufacture of dietary and nutritional supplements. In this study, the first attempt to the assessment of horses exposure to TYR during nutritional supplementation was demonstrated by quantification of unbound TYR...
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A method for a comprehensive lipidomic analysis of flaxseed (Linum usitatissimum) with the use of LC–Q-TOF-MS and dispersive micro-solid-phase (μDSPE) extraction
PublicationFlaxseed (FS) is one of the richest sources of α-linolenic acid oil and lignans, and it is suggested that the consumption of flaxseed may contribute to the prevention of certain chronic diseases such as many types of cancer, diabetes, cardiovascular diseases and cerebrovascular stroke. Here, we demonstrate a new method for comprehensive FS lipidome profiling with the use of LC–Q-TOF-MS and dispersive micro-solid-phase extraction....
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LC-ESI-MS profiling of Potentilla norvegica and evaluation of its biological activities
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublicationGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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Association between Breastmilk LC PUFA, Carotenoids and Psychomotor Development of Exclusively Breastfed Infants
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Identification of antioxidant polyphenolics from Jasione montana based on a preliminary LC-MS profiling
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Wpływ parametrów filtra wejściowego lc pojazdu na stabilność trakcyjnego układu zasilania
PublicationW referacie przedstawiono wpływ zmiany parametrów elektrycznych filtra na stabilność układu zasilania trakcji elektrycznej. Zaprezentowano ogólne założenia teoretyczne problemu oraz zaproponowano nowy współczynnik pozwalający na wstępne określenie stabilności sys-temu dla przyjętych parametrów filtra wejściowego. Przedstawiono wyniki analizy symula-cyjnej wykonanej w programie PSpice przy wykorzystaniu opracowanych modeli poszcze-gólnych...
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Development and validation of an LC–MS/MS method for the determination of biogenic amines in wines and beers
PublicationBiogenic amines are group of organic, basic, nitrogenous compounds that naturally occur in plant, microorganism, and animal organisms. Biogenic amines are mainly produced through decarboxylation of amino acids. They are formed during manufacturing of some kind of food and beverages such as cheese, wine, or beer. Histamine, cadaverine, agmatine, tyramine, putrescine, and b-phenylethylamine are the most common biogenic amines found...
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A Robust Method for Sample Preparation of Gastrointestinal Stromal Tumour for LC/MS Untargeted Metabolomics
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Analysis of urinary nucleosides as potential cancer markers determined using LC–MS technique
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Dielectric response of electric-field distortions of the twist-bend nematic phase for LC dimers
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublicationThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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Determining the true content of quercetin and its derivatives in plants employing SSDM and LC–MS analysis
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LC–MS/MS analysis, antioxidant and anticholinergic properties of galanga (Alpinia officinarum Hance) rhizomes
PublicationGalanga (Alpinia officinarum Hance) is a pungent and aromatic rhizome, which is a member of the ginger family (Zingiberaceae). The rhizomes of this plant have been used as a traditional medicine in far east countries for relieving stomach ache, invigorating the circulatory system, treating colds, and reducing swelling. The aim of this study was to investigate antioxidant and anticholinergic properties of galanga. For this purpose,...
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Generalized adaptive notch filters with frequency debiasing for tracking of polynomial phase systems
PublicationGeneralized adaptive notch filters are used for identification/tracking of quasi-periodically varying dynamic systems and can be considered an extension, to the system case, of classical adaptive notch filters. For general patterns of frequency variation the generalized adaptive notch filtering algorithms yield biased frequency estimates. We show that when system frequencies change slowly in a smooth way, the estimation bias can...
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An LC-MS/MS Method for a Comprehensive Determination of Metabolites of BTEX Anaerobic Degradation in Bacterial Cultures and Groundwater
PublicationBTEX (benzene, toluene, ethylbenzene, and the different xylene isomers), known for carcinogenic and neurotoxic effects, are common environmental contaminants. The first step for the development of the bioremediation technologies is the detection of intense microbial degradation in contaminated waters in the quest for the most active bacterial strains. This requires the multispecies analysis for BTEX metabolites which are considered...
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Quantification of methadone and its metabolites: EDDP and EMDP determined in autopsy cases using LC‐MS/MS
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Analysis of bisphenols and their derivatives in infant and toddler ready-to-feed milk and powdered milk by LC MS/MS
PublicationReady-to-feed milk and powdered milk packed in different types of packaging lined with resin are chosen as the primary or complementary diet for infants and toddlers. An HPLC–MS/MS method was established and validated for the determination of nineteen bisphenols and their derivatives in such samples. The recoveries were from 31% to 120%, while the values of limit of detection and quantification were in the range of 0.24–0.40 and...
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Jarosław Guziński prof. dr hab. inż.
PeopleJaroslaw Guzinski received M.Sc., Ph.D. and D.Sc. degrees from the Electrical Engineering Department at Technical University of Gdansk, Poland in 1994, 2000 and 2011 respectively. Since 2016 he is Associate Professor at Gdansk University of Technology. Currently he is the head of the Department of Electric Drives and Energy Conversion. From 2006 to 2009 he was involved in European Commission Project PREMAID Marie Curie, ‘Predictive...
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Adjustable fractional-delay filters utilizing the Farrow structure and multirate techniques. [Przestrajalne filtry o opóźnieniu ułamkowym wykorzystujące strukturę Farrowa i techniki wieloszybkościowe]
PublicationDo efektywnej realizacji ułamkowo opóźniających, przestrajalnych filtrów FIR (o skończonej odpowiedzi impulsowej) można wykorzystywać strukturę Farrowa. Jednakże, niezależnie od efektywności w porównaniu z innymi strukturami, jej złożoność implementacyjna szybko rośnie ze wzrostem szerokości pasma filtru. Celem zredukowania złożoności numerycznej, zaproponowano podejście wieloszybkościowe. W tym podejściu sygnał wejściowy jest...
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Zastosowanie chromatografii cieczowej w odwróconym układzie faz (RP-LC) w rozdzielanie i oznaczaniu polifenoli i naftochinonów w materiałach roslinnychreversed = Phase liquid chromatography (RP-LC) for separation and quantitative determination of polyphenols and naphtoquinones in plant materials
PublicationW pracy przedstawiono przegląd metod rozdzielania i oznaczania naftochinonów i polifenoli pochodzących z materiału roślinnego, z wykorzystaniem technik chromatograficznych w układzie faz odwróconych - RP-TLC (Reversed-Phase Thin Layer Chromatography) oraz RP-HPLC (Reversed-Phase High Performance Liquid Chromatography). Przeanalizowano procedury przygotowania próbki, etap rozdzielania, a także kontroli czystości zbieranych frakcji....
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Filtry Kalmana i sterowanie w warunkach losowych - sem. zim. 2022/2023
e-Learning CoursesWykład dotyczy metod projektowania filtrów Kalmana oraz sterowania obiektami dynamicznymi w warunkach losowych.
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Filtry Kalmana i sterowanie w warunkach losowych - sem. zim. 2023/2024
e-Learning CoursesWykład dotyczy metod projektowania filtrów Kalmana oraz sterowania obiektami dynamicznymi w warunkach losowych.
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Lipidomic characteristics of three edible cold-pressed oils by LC/Q-TOF for simple quality and authenticity assurance
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LC-PDA-MS and GC-MS Analysis of Scorzonera hispanica Seeds and Their Effects on Human Breast Cancer Cell Lines
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Urine metabolic fingerprinting using LC–MS and GC–MS reveals metabolite changes in prostate cancer: A pilot study
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Metabolic Evaluation of Urine from Patients Diagnosed with High Grade (HG) Bladder Cancer by SPME-LC-MS Method
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Zastosowanie techniki LC-MS/MS oraz biotestów w analityce próbek środowiskowych w celu oznaczenia ich potencjału endokrynnego i zawartości wybranych związków endokrynnych
PublicationWyniki wielu badań prowadzonych w przeciągu ostatnich lat mogą stanowić podstawę do stwierdzenia, że zanieczyszczenia emitowane do środowiska ze źródeł antropogennych mogą stanowić kolejny rodzaj zagrożenia, z którego nie zdawano sobie sprawy wcześniej. Zanieczyszczeniami takimi są substancje z grupy EDC definiowane jako jakikolwiek czynnik, który wpływa na syntezę, wydalanie, transport, wiązanie, działanie lub wydalanie hormonów...
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Collective filter evaluation of an FSD filter-based resampling algorithm. [online] W: Online Symposium for Electronics Engineers. Techonline Bedford, Massachusetts, USA. [Dostęp: 15 stycznia**2002]. Dostępny w World Wide Web: http://www.techonline.com/community/ed_resource/feature_article/14917/[6 s. 5 rys.] Badanie algorytmu zmiany szybkości próbkowania realizowanego w oparciu o filtry FSD za pośrednictwem analizy filtru zbiorczego.
PublicationW pracy przedstawiono koncepcję filtru zbiorczego dla potrzeb oceny jakościalgorytmu zmiany szybkości próbkowania realizowanego w oparciu o filtry u-łamkowo-opóźniające (FSD). W przypadku takiego algorytmu przepróbkowania dowyznaczania każdej próbki wyjściowej potrzebny jest filtr FSD o innm opóź-nieniu ułamkowym. Z kolei jakość takiego filtru zależy właśnie od jego opóź-nienia, co stwarza problemy w ocenie jakości samego...
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Molecular interaction sensors: a new detector platform for separation methods
PublicationPotencjometria jest nową metodą detekcji dla chromatografii cieczowej (LC)i elektroforezy kapilarnej (CE). Zastosowanie potencjometrii dla chromatograficznych technik wynika z faktu, że sygnał z detektora jest zależny od stanu rozdzielenia analitów nad pokryciem sensora i od rodzaju eluentu. Rozdzielenie analitu powoduje zmiany potencjału, a zmiany te można zaklasyfikować jako potencjometryczne. Do opisu ilościowego potrzebny jest...
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Determining pesticide contamination in honey by LC-ESI-MS/MS - Comparison of pesticide recoveries of two liquid-liquid extraction based approaches
PublicationHoney, a valuable food product, may be contaminated by xenobiotics during its production and/or harvest. The determination of trace levels of contaminants in a complex matrix like honey still presents a challenge to analytical chemists. The aim of this work was to assess and compare the extraction efficiencies of 30 pesticide residues (acaricides, insecticides, herbicides, fungicides), belonging to over 15 different chemical classes....
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Extraction and Analysis of Bisphenols and Their Derivatives in Infant and Toddler Ready-to-feed Meals by Ultrasound-assisted Membrane Extraction Followed by LC MS/MS
PublicationThis research developed an ultrasound-assisted membrane extraction coupled with liquid chromatography-tandem mass spectrometry method for the determination of nineteen bisphenols and their derivatives in infant and toddler ready-to-feed meals. The calibration curves for all analytes were linear in the tested range, and the limit of detection and limit of quantitation were in the range 0.27 to 0.79 ng/g and 0.80 to 2.4 ng/g, respectively....
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Developments in Green Chromatography
PublicationGreen analytical chemistry is a widely recognized concept that has led to the development of new analytical methods with reduced environmental impact and minimized analyst occupational exposure. Achievements include the development of microextraction, ultrasound-assisted extraction (UAE), and microwave-assisted extraction (MAE) techniques. Research towards greener separation processes focuses on the elimination of toxic solvents...
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Concentration of Potentially Bioactive Compounds in Italian Extra Virgin Olive Oils from Various Sources by Using LC-MS and Multivariate Data Analysis
PublicationHigh quality extra virgin olive oils represent an optimal source of nutraceuticals. The European Union (EU) is the world’s leading olive oil producer, with the Mediterranean region as the main contributor. This makes the EU the greatest exporter and consumer of olive oil in the world. However, small olive oil producers also contribute to olive oil production. Beneficial effects on human health of extra virgin olive oil are well...
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Plant-based meat substitute analysis using microextraction with deep eutectic solvent followed by LC-MS/MS to determine acrylamide, 5-hydroxymethylfurfural and furaneol
PublicationFor the analysis of plant-based meat substitutes and the determination of Maillard reaction products such as acrylamide, 5-hydroxymethylfurfural and furaneol, a novel and effective procedure based on hydrophobic natural deep eutectic solvent and liquid chromatography coupled with tandem mass spectrometry was developed for the first time. The 49 compositions of the deep eutectic solvents were designed and screened to select the...
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Agata Kot-Wasik prof. dr hab. inż.
PeopleAgata Kot-Wasik, born in 1964 in Siedlce, graduated in 1988 from the Faculty of Chemistry, Gdańsk University of Technology in Industrial and Technical Analysis. In 1988-1992 she was employed in the Department of Organic Chemistry. In 1990, she completed postgraduate studies "Instrumental techniques in the traces analysis and Environmental Protection" at GUT, and in 1992 began PhD Studies at the Faculty of Chemistry, GUT, which...
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Preparation and evaluation of 1,3-alternate 25,27-bis[p-nitrobenzyloxy]-26,28-bis[3-propyloxy]-calix[4]arene-bonded silica gel stationary phase for LC
PublicationPrzeprowadzono syntezę nowej fazy stacjonarnej na bazie sililowej pochodnej 25,27-bis[p-nitrobenzyloksy]-26,28-bis-[3-propyloksy]kaliks[4]arenu zablokowanego w konformacji 1,3-naprzemianległej. Zbadano selektywność i sprawność fazy w stosunku do szeregu klas związków organicznych techniką wysokosprawnej chromatografii cieczowej.
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Selectivity Tuning by Natural Deep Eutectic Solvents (NADESs) for Extraction of Bioactive Compounds from Cytinus hypocistis—Studies of Antioxidative, Enzyme-Inhibitive Properties and LC-MS Profiles
PublicationIn the present study, the extracts of Cytinus hypocistis (L.) L using both traditional solvents (hexane, ethyl acetate, dichloromethane, ethanol, ethanol/water, and water) and natural deep eutectic solvents (NADESs) were investigated in terms of their total polyphenolic contents and antioxidant and enzyme-inhibitive properties. The extracts were found to possess total phenolic and total flavonoid contents in the ranges of 26.47–186.13...
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Krzysztof Nyka dr hab. inż.
PeopleKrzysztof Nyka, received MSc (1986) PhD (2002) and DSc (2020) degrees in telecommunication and electrical engineering from the Faculty of Electronics, Telecommunications and Informatics (ETI) of Gdańsk University of Technology (GUT), Poland. He is currently an Associate Professor at the Department of Microwaves and Antenna Engineering, Faculty of ETI, GUT. Before his academic career, he worked for the electronic industry (1984-1986). Research...
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Rapid and simple multi-analyte LC–MS/MS method for the determination of benzodiazepines and Z-hypnotic drugs in blood samples: Development, validation and application based on three years of toxicological analyses
PublicationBenzodiazepines (BZDs) and Z-drugs have been particularly important treatments for sleeping and anxiety disorders for many years. However, recently, a number of new benzodiazepines (named designer benzodiazepines, DBZDs) were synthesised, but some of them have never been used in the clinic; they reached the black drug market as new psychoactive substances and are used for recreational purposes. The abuse of these substances has...
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Profile and Content of Phenolic Compounds in Leaves, Flowers, Roots, and Stalks of Sanguisorba officinalis L. Determined with the LC-DAD-ESI-QTOF-MS/MS Analysis and Their In Vitro Antioxidant, Antidiabetic, Antiproliferative Potency
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Jacek Stefański prof. dr hab. inż.
PeopleJJacek Stefański received M.Sc., Ph.D. and D.Sc. degrees in telecommunications engineering from Gdansk University of Technology (GUT), Poland, in 1993, 2000 and 2012, respectively. Awarded title of Professor by the President of Poland in 2020. Currently, he works as a professor at the Department of Radio Communication Systems and Networks (DRCSN) in GUT. From 2005 to 2009, he worked as an assistant professor in the National Institute...
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Analogowe filtry CMOS OTA-C czasu ciągłego realizowane w strukturach pro- gramowalnych.**2002, s. 7-113, 95 rys. 12 tab. maszyn. Rozprawa doktorska ( 22.10.2002 ) PG Wydz. Elektr. Telekom. i Informat. Promotor: prof. dr hab. inż. Michał Białko
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OZNACZANIE POZOSTAŁOŚCI PESTYCYDÓW W ORGANIZMACH PSZCZELICH ORAZ W MIODZIE Z WYKORZYSTANIEM PROCEDURY OPARTEJ NA ZASTOSOWANIU CHROMATOGRAFÓW SPRZĘŻONYCH Z TANDEMOWYMI SPEKTROMETRAMI MAS (GC-MS/MS i LC-MS/MS)
PublicationPestycydy to bardzo liczna grupa różnorodnych związków chemicznych stosowa-nych w rolnictwie. Ze względu na swoją trwałość gromadzą się w różnych elementach środowiska i mogą występować w obszarze, na którym nigdy nie zostały użyte. Zachodzi także proces ich bioakumulacji w tkankach oraz narządach zwierząt i roślin. Stosowane w rolnictwie środki ochrony roślin (szczególnie w okresie wzmożonych zabiegów agro-technicznych wiosną...
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Optymalizacja parametrów obciążenia generatora magnetokumulacyjnego
PublicationW pracy przedstawiono wyniki symulacji komputerowej generatora magnetokumulacyjnego (GM) obciążonego cewką indukcyjną. Badania symulacyjne przeprowadzono w celu optymalizacji parametrów cewki obciążenia generatora dla wybranej konstrukcji modelu GM. Badano wpływ indukcyjność i rezystancji obciążenia na współczynnik wzmocnienia prądu w układzie oraz na energię pola magnetycznego zgromadzoną w obciążeniu.
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Daniel Załuski dr hab. inż. arch.
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