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Search results for: SPEKTROMETRIA MAS (MS)
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Non-volatile molecular composition and discrimination of single grape white of chardonnay, riesling, sauvignon blanc and silvaner using untargeted GC–MS analysis
PublicationThis study developed and applied a GC–MS method aiming at molecular fingerprinting of 120 commercial single grape white wines (Chardonnay, Riesling, Sauvignon Blanc and Silvaner) for possible authentication according to grape variety. The method allowed detection of 372 peaks and tentative identification of 146 metabolites including alcohols, organic acids, esters, amino acids and sugars. The grape variety effect explained 8.3%...
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The use of RP-HPLC–Q-TOF–MS as a powerful tool for wastewater composition profiling and selection of water pollution marker specific to wastewater contamination
PublicationLimited drinking water resources and water pollution are one of the main worldwide problems. To reduce the consumption of fresh water resources, the use of treated wastewater has been proposed. The farmlands have been irrigated with wastewater for centuries, but the composition of used sewage has changed over the years. Recent research has revealed the presence of hundreds of new organic contaminants in many environmental waters,...
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A Robust Method for Sample Preparation of Gastrointestinal Stromal Tumour for LC/MS Untargeted Metabolomics
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Analysis of urinary nucleosides as potential cancer markers determined using LC–MS technique
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New approach in determination of urinary diagnostic markers for prostate cancer by MALDI-TOF/MS
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Identyfikacja i diagnostyka procesu oczyszczania ścieków przy użyciu metody MS-PCA
PublicationPołączenie algorytmu PCA z dekompozycją falkową pozwala na wiarygodną identyfikację i diagnostykę procesu z wieloma skalami czasu. Niniejszy artykuł pokazuje jak przy pomocy wspomianego narzedzia określić stan pracy obiektu oraz odpowiednio szybko wykryć uszkodzenia (np. czujników pomiarowych) lub stany awaryjne obiektu jakim jest oczyszczalnia ścieków. Przedstawiony jest przykład detekcji błędów pomiarowych (stężenie tlenu w komorze...
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The chromatographic analysis of extracts from poplar (Populus sp.) - Laying program GC-MS
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Endogenous oxidative DNA base modifications analysed with repair enzymes and GC/MS technique
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Identification of antioxidant polyphenolics from Jasione montana based on a preliminary LC-MS profiling
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublicationGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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Marzena Grygiel, WFTi MS, Nanotechnologia, 1 st, 3sem, 2022/23 z
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Marzena Grygiel, WFTi MS, Nanotechnologia, 1 st, 4sem, 2022/ 23 l
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublicationOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublicationThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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GC-MS-based untargeted metabolomics of plasma and urine to evaluate metabolic changes in prostate cancer
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Determining the true content of quercetin and its derivatives in plants employing SSDM and LC–MS analysis
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Validated GC–MS method for determination of bisphenol a and its five analogues in dietary and nutritional supplements
PublicationBisphenol A (BPA) and its analogues showing structural and functional similarity to BPA are commonly applied in various industrial applications and thus are becoming ubiquitous in the environment. At the same time there is increasing scientific evidence that exposure to these chemicals may lead to adverse health effects in human and wildlife. In recent years dietary and nutritional supplements dedicated for athletes have become...
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Characteristics of Cucumis metuliferus, Actinidia deliciosa and Musa paradisica fragrance profiles using a comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometric detection (GC×GC-TOF MS)
PublicationComprehensive two-dimensional gas chromatography with time-of-flight mass spectrometric detection (GC×GC-TOF-MS) is a modern analytical technique used in many fields. This technique enables an effective separation of volatile chemical compounds [1]. In recent years, the topic of healthy food and healthy living has become very popular. For this reason, more and more scientific publications related to the analysis of food products...
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Metodologia pracy zespołowe - S, MS, sem.06, letni 21/22 (M:31707W0)
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Analiza danych biznesowych z wykorzystaniem MS Excel – Power BI i Power Query
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Metodologia pracy zespołowej, W, MS, sem.06, letni 21/22 (M:31707W0)
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Phyloproteomic study by MALDI-TOF MS in view of intraspecies variation in a significant homogenous phytopathogen Dickeya solani
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The application of isotopically labeled analogues for the determination of small organic compounds by GC/MS with selected ion monitoring
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GC-MS analysis, antidiabetic and antioxidant activity of methanolic extract of pluteus cervinus: an in vitro and in silico approach
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Method development and validation for optimized separation of the major polyphenolics in propolis extracts using GC-MS method
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Flowers and Leaves Extracts of Stachys palustris L. Exhibit Stronger Anti-Proliferative, Antioxidant, Anti-Diabetic, and Anti-Obesity Potencies than Stems and Roots Due to More Phenolic Compounds as Revealed by UPLC-PDA-ESI-TQD-MS/MS
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Determination of PCBs in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry -method validation
PublicationOpracowano procedurę oznaczania wybranych analitów z grupy PCB w próbkach osadu dennego z wykorzystaniem techniki przyspieszonej ekstrakcji za pomocą rozpuszczalnika (PLE) w połączeniu z chromatografią gazową z detektorem spektrometrii mas. Opracowana procedura analityczna została wykorzystana do analizy próbek morskiego osadu dennego, które stanowiły przedmiot badań międzylaboratoryjnych organizowanych przez Comité Consultatif...
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Impact of Cluster Zone Leaf Removal on Grapes cv. Regent Polyphenol Content by the UPLC-PDA/MS Method
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Ekspertyza dotycząca przyczyn pęknięcia rurociągu 8”-096-P1059, zamówienie nr WU/0402/2020/MS
PublicationWykonano badania nieniszczące i niszczących próbek materiału rurociągu wraz z przygotowaniem próbek do badań z materiału rodzimego.
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Metabolic Evaluation of Urine from Patients Diagnosed with High Grade (HG) Bladder Cancer by SPME-LC-MS Method
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Verification of the homogeneity of the matrix/analyte mixture on sample plate using MALDI-MS technique and new ionic liquid matrices
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DNA methylation analysis with methylation‐sensitive high‐resolution melting (MS‐HRM) reveals gene panel for glioma characteristics
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The potential role of fatty acids in prostate cancer determined by GC–MS analysis of formalin-fixed paraffin-embedded tissue samples
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Dynamics of hepatitis B virus quasispecies heterogeneity in association with nucleos(t)ide analogue treatment determined by MALDI-TOF MS
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Simultaneous determination of individual isothiocyanates in plant samples by HPLC-DAD-MS following SPE and derivatization with N-acetyl-l-cysteine
PublicationThe procedure for the isothiocyanates (ITCs) determination that involves derivatization with N-acetyl-l-cysteine (NAC) and separation by HPLC was developed. Prior to derivatization, plant ITCs were isolated and purified using solid-phase extraction (SPE). The optimum conditions of derivatization are: 500 μL of isopropanolic eluate obtained by SPE combined with 500 μL of derivatizing reagent (0.2 M NAC and 0.2 M NaHCO3 in water)...
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Method for the simultaneous determination of monoaromatic and polycyclic aromatic hydrocarbons in industrial effluents using dispersive liquid-liquid microextraction with GC-MS
PublicationWe present a new method for simultaneous determination of 22 monoaromatic and polycyclic aromatic hydrocarbons in postoxidative effluents from the production of petroleum bitumen using dispersive liquid-liquid microextraction coupled to gas chromatography and mass spectrometry. The eight extraction parameters including the type and volume of extraction and disperser solvent, pH, salting out effect, extraction and centrifugation...
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Study of effect of phosphate and uranium ions on the thermal properties of surfactant-modified natural red clay using TG–FTIR–MS techniques
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Concentration of Potentially Bioactive Compounds in Italian Extra Virgin Olive Oils from Various Sources by Using LC-MS and Multivariate Data Analysis
PublicationHigh quality extra virgin olive oils represent an optimal source of nutraceuticals. The European Union (EU) is the world’s leading olive oil producer, with the Mediterranean region as the main contributor. This makes the EU the greatest exporter and consumer of olive oil in the world. However, small olive oil producers also contribute to olive oil production. Beneficial effects on human health of extra virgin olive oil are well...
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KONSULTACJE / SDW-MS, WMI-W, PB-W / Wydział Inżynierii Mechanicznej i Okrętownictwa / sem. zimowy 2021/2022 (PG)
e-Learning CoursesKONSULTACJE PRZEZNACZONE SĄ DLA STUDENTÓW: - SZKOŁY DOKTORSKIEJ WDROŻENIOWEJ - PG: Mechanika Stosowana (W) - STUDIÓW INZYNIERSKICH I STOPNIA - MiBM, MTR, ZiIP - WIMiO: WMI (W) - STUDIÓW INŻYNIERSKICH I STOPNIA - MiBM st. niestacj. - WIMiO - WMI (W) - STUDIÓW MAGISTERSKICH II STOPNIA - TKiS - WIMiO - Pojazdy Bezzałogowe (W) KONSULTACJE ODBYWAJĄ SIĘ ZDALNIE w CZWARTEK w godz. 15.00-17.00
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Determination of pharmaceutical residues in drinking water in Poland using a new SPE-GC-MS(SIM) method based on Speedisk extraction disks and DIMETRIS derivatization
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Wpływ stopowania laserowego z użyciem nanorurek węglowych stopu Ti13Nb13Zr do zastosowań biomedycznych na jego wybrane własności mechaniczne
PublicationDo eksperymentu użyto stopu tytanu Ti13Nb13Zr, który ze względu na swój skład chemiczny i właściwości mechaniczne stanowi materiał do zastosowań w inżynierii medycznej. Celem pracy była ocena wpływu stopowania laserowego stopu Ti13Nb13Zr z powłoką z wielościennych nanorurek węglowych na jego właściwości mechaniczne (chropowatość, nanotwardość, moduł Younga). Do wytworzenia powłoki węglowej wykorzystano metodę osadzania elektroforetycznego (EDP)....
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Phenolic composition and antioxidant properties of polish blue-berried honeysuckle genotypes by HPLC-DAD-MS, HPLC postcolumn derivatization with ABTS or FC, and TLC with DPPH visualization
PublicationIn this study, different Polish cultivars of blue-berried honeysuckles (Lonicera caerulea L.), wild and bog bilberry, were analyzed for bioactive compounds. The chemical properties verified included composition of anthocyanins and other polyphenols, antioxidant activity, and profiles of antioxidants by HPLC postcolumn derivatization or TLC. The antioxidant activities of different blue-berried honeysuckle cultivars were similar...
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Selectivity Tuning by Natural Deep Eutectic Solvents (NADESs) for Extraction of Bioactive Compounds from Cytinus hypocistis—Studies of Antioxidative, Enzyme-Inhibitive Properties and LC-MS Profiles
PublicationIn the present study, the extracts of Cytinus hypocistis (L.) L using both traditional solvents (hexane, ethyl acetate, dichloromethane, ethanol, ethanol/water, and water) and natural deep eutectic solvents (NADESs) were investigated in terms of their total polyphenolic contents and antioxidant and enzyme-inhibitive properties. The extracts were found to possess total phenolic and total flavonoid contents in the ranges of 26.47–186.13...
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Optymalizacja projektu montażu obiektu MS-4/B realizowanego w ramach zadania „Budowa drogi ekspresowej S7 na odc. Miłomłyn-Olsztynek, Pododcinek Ostróda Północ - Ostróda Południe, w ciągu drogi S7 wraz z budową obwodnicy Ostródy w ciągu DK 16 (Pododcinek "B")” wraz z uzgodnieniami z nadzorem autorskim i nadzorem naukowym
PublicationCelem opracowania jest przeprowadzenie optymalizacji projektu montażu obiektu MS-4/B realizowanego w ramach zadania „Budowa drogi ekspresowej S7 na odc. Miłomłyn-Olsztynek, Pododcinek Ostróda Północ - Ostróda Południe, w ciągu drogi S7 wraz z budową obwodnicy Ostródy w ciągu DK 16 (Pododcinek "B")” oraz uzgodnienie wprowadzonych zmian z Nadzorem Autorskim (NA).
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Christian Jungnickel dr hab.
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Sebastian Wilczewski dr inż.
PeoplePhD. Sebastian Wilczewski is employed as an Assistant Professor in the Department of Applied Informatics in Management, Faculty of Management and Economics. Additionally, he has been working in IT companies for over 20 years, where he held positions from an system engineer and consultant, through the position of Project Manager, Portfolio Manager and Process Owner to the position of Team Leader for a team of about 30 IT analysts. Areas...
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A survey on network resiliency methodologies against weather-based disruptions
PublicationDue to the increasing dependence on network services of our society, research has recently been concentrating on enhancing traditional protection strategies to withstand large-scale failures, as in case of disaster events. The recently-formed EU-funded RECODIS project aims at coordinating and fostering research collaboration in Europe on disaster resiliency in communication networks. In particular, the Working Group (WG) 2 of the...
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Can matrix solid phase dispersion (MSPD) be more simplified? Application of solventless MSPD sample preparation method for GC–MS and GC–FID analysis of plant essential oil components
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Wykorzystanie technik GC×GC-TOF-MS i olfaktometrii terenowej do oceny uciążliwości zapachowej powietrza atmosferycznego na obszarach przyległych do terenu składowiska odpadów komunalnych
PublicationUciążliwość zapachowa jest poważnym problemem środowiskowym i jednym z powodów skarg ludności dotyczących złej jakości powietrza atmosferycznego. Źródłem emisji nieprzyjemnych zapachów do środowiska (odorów) są obiekty gospodarki komunalnej, w tym składowiska odpadów komunalnych. Ze względu na negatywny wpływ emisji substancji zapachowych na zdrowie i życie człowieka, konieczne jest stosowanie odpowiednich narzędzi analitycznych...
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Jaromir Durkiewicz mgr
PeopleJaromir Durkiewicz is a research assistant at Department of Applied Informatics in Management, Faculty of Management and Economics, Gdańsk University of Technology. He holds a double master's degree in Informatics and Econometrics and Political Science (University of Gdańsk). His professional career includes a few years of work in IT sector. Since 2017 - PhD student at Faculty of Management and Economics, where he cooperates with...