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Search results for: SYMPLEKS BAUERA
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Ion Chromatography with Pulsed Amperometric Detection for Determining Cyanide in Urine and Meconium Samples
PublicationThe parents’ addictions and eating habits have a significant influence on the child’s growth. The first stool of a newborn baby provides a large amount of information about xenobiotics transmitted by the mother’s body. The analytical technique used in the study is ion chromatography with pulsed amperometric detection (IC-PAD). The biological samples, which were obtained from women staying in a maternity ward and their partners,...
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MECONIUM SAMPLES USED TO ASSESS INFANT EXPOSURE TO THE COMPONENTS OF ETS DURING PREGNANCY
PublicationThe aim of the study was to use meconium samples to assess fetal exposure to compounds present in environmental tobacco smoke (ETS). Material and Methods: In order to assess fetal exposure to toxic tobacco smoke compounds, samples of meconium from the offspring of women with different levels of tobacco smoke exposure, and the samples of saliva from the mothers were analyzed. Thiocyanate ion as a biomarker of tobacco smoke exposure,...
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New Trends in Sample Preparation Techniques for the Analysis of the Residues of Pharmaceuticals in Environmental Samples
PublicationPharmaceutical residues in the environment is a field of special interest due to the adverse effects to either human health or aquatic and soil environment. Pharmaceuticals have been already detected in underground, surface and wastewaters, soils, manure and sediments. The growing awareness of environmental pollution arising from human activity forces the need for their comprehensive determination. Environmental samples are complex...
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Determination of Metals Content in Wine Samples by Inductively Coupled Plasma-Mass Spectrometry
PublicationKnowledge about the metal content of wine is very important, for many reasons. Depending on the element, its quantity varies in wine from ng/L to mg/L. Despite the fact that metals are not directly connected to the taste and aroma of the wine, their content should be determined and controlled, because excess is undesirable, and in some cases prohibited, due to potential toxicity. Several analytical procedures for metal determination...
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Complementary use of GCxGC–TOF–MS and statistics for differentiation of variety in biosolid samples
PublicationFormation of biosolid cakes, which are one of the main wastes generated in wastewater treatment plants, is connected with emission of many hazardous chemical compounds, including odoriferous ones. To optimize particular processes of biosolid cake processing, it is necessary to assess chemical composition of the gas mixtures containing the compounds released from the cakes. The paper proposes application of two-dimensional gas chromatography...
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An analytical hierarchy process for selection of the optimal procedure for resveratrol determination in wine samples
PublicationThe study shows the application of analytical hierarchy process (AHP) in ranking the analytical procedures, that are applied for resveratrol determination in wine samples. 19 different analytical methodologies are described by metrological, economic and environmental criteria, that are further divided into 10 subcriteria. Before AHP application, the amount of input data is decreased with cluster analysis. The first run of AHP is...
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Direct determination of cadaverine in the volatile fraction of aerobically stored chicken breast samples
PublicationTo supplement the currently used methods for poultry meat shelf life assessment, it might be necessary to develop a technique for rapid headspace analysis of volatiles with no prior sample preparation step. Biogenic amines, in particular cadaverine, are considered meat spoilage indicators. Described in this article are the results of a preliminary investigation of the applicability of proton transfer reaction mass spectrometry...
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Determination of cyanide in urine and saliva samples by ion chromatography with pulsed amperometric detection
PublicationCommonly known as a highly toxic chemical, cyanide is also an essential reagent for many industrial processes. It naturally occurs in plant seeds as a cyanogenic glycosides. Another relatively common mode of cyanide exposure is inhalation of environmental tobacco smoke. This study concerns importance to determine cyanide ion in human biological samples. Urine and saliva samples were collected healthy volunteers exposed to tobacco...
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Determination of MDPBP in postmortem blood samples by gas chromatography coupled with mass spectrometry
PublicationMDPBP (1-(3,4-methylenedioxyphenyl)-2-(1-pyrrolidinyl)-1-butanone) is a new psychoactive substance sold on the black market. It has been a controlled drug of abuse in Poland and China since 2015 as some toxic and fatal cases connected with use of synthetic cathinone derivatives were observed. The fatal case outlined here concerns a 19 year-old man, who was found dead with an envelope containing white powder lying nearby the cadaver....
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Determination of Volatile Organic Compounds in indoor air in the Gdansk area using permeation passive samplers.
PublicationDozymetria pasywna, znana od wielu lat, jest użytecznym narzędziem w monitoringu poziomu zanieczyszczeń. Do określenia jakości powietrza wewnętrznego w 22 pomieszczeniach mieszkalnych, zlakoalizowanych na terenie Gdańska, wykorzystano dozymetry pasywne typu permeacyjnego na etapie pobierania próbek analitów. Uzyskane wyniki porównano z wynikami uzyskanymi przy wykorzystaniu matedy dynamicznej. Podjęto również próbę identyfikacji...
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Determination of Volatile Organic Compounds in Indoor Air in the Gdansk Area Using Permeation Passive Samplers
PublicationPassive dosimetry — known for over a hundred years — is still a useful tool in monitoring air pollutants. In this work, permeation passive samplers were used to determine indoor air quality in 22 apartments located in the Gdansk area in the northern part of Poland. The results obtained by the passive sampling technique were compared to those obtained by dynamic sampling. Attempts were also made to identify indoor sources of...
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Static renewal and continuous-flow calibration of two types of passive samplers for the monitoring of pharmaceuticals in wastewater
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Limitations of Integrative Passive Samplers as a Tool for the Quantification of Pharmaceuticals in the Environment – A Critical Review with the Latest Innovations
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Sense of Purpose in Life and Escape from Self as the Predictors of Quality of Life in Clinical Samples
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New sorbent materials for selective extraction of cocaine and benzoylecgonine from human urine samples
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The simultaneous detection of food dyes from different samples in a 96-well plate by spectrophotometry
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A fully validated HPLC–UV method for determination of sulthiame in human serum/plasma samples
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Selected analytical challenges in the determination of pharmaceuticals in drinking/marine waters and soil/sediment samples
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Comparison of different digestion methods for proteomic analysis of isolated cells and FFPE tissue samples
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Application of the Least Squares Method to the approximation of equally spaced samples in frequency measurement approach
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Nested PCR for the detection of Aspergillus species in maxillary sinus samples of patients with chronic sinusitis
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Determination of hormones in water samples using liquid chromatography coupled with tandem mass spectrometry
PublicationOver the past few years, many synthetic (ethinylestradiol) and natural (estradiol,estriol, estrone) compounds present in the environment have been affecting the hormonalbalance of humans and animals. Steroid hormones are very often used for medical purposesand have high estrogenic activity what makes them endocrine disrupters. Most hormonalcompounds are released into the water as a result of their incomplete removal in wastewatertreatment...
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Application of Immunological Techniques (from Vaccination to FinalMeasurements) in Determination of Pharmaceutical Residues in Environmental Samples
PublicationWiele biologicznie aktywnych związków wytwarzanych przez człowieka trafia ostatecznie do środowiska. Ich los środowiskowy pozostaje nadal wyzwaniem dla analityków środowiskowych i osób odpowiedzialnych za szacowanie ryzyka. Artykuł przedstawia przegląd jednej z najszerszych i bezpośrednich metod analiz środowiskowych - immunoanalitykę - ze szczególnych uwzględnieniem jej zastosowania do oznaczania jakościowego i ilościowego pozostałości...
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Comparison of Ion Chromatography and Isotachophoresis for the Determination of selected Anions in Atmospheric Wet Deposition Samples
PublicationW pracy przedstawiono porównanie wyników oznaczenia zawartości wybranych anionów w próbkach opadów atmoferycznych z zastosowaniem technik izotachoforezy i chromatografii jonowej. Na podstawie otrzymanych wyników można stwierdzić, że technika chromatografii jonowej charakteryzuje się niższymi wartościami granic wykrywalności i oznaczalności, szerokim zakresem pomiarowym i możliwością oznaczania analitów w próbkach o róznym składzie...
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Oznaczanie herbicydów kwasowych w próbkach wodnych. Determination of acidic herbicides in aqueous samples
PublicationPrzedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy fenoksykwasów i fenoli w próbkach wodnych. Przedyskutowano zalety i wady izolacji i wzbogacania analitów za pomocą ekstrakcji ciecz-ciecz, ekstrakcji do fazy stałej, mikroekstrakcji do fazy stacjonarnej oraz ekstrakcji za pomocą płynu w stanie nadkrytycznym. Ze względu na złożoność próbki środowiskowej, w analizie końcowej stosuje się wysokorozdzielcze...
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SYNTHETIZED MEMBRANES FOR ULTRASOUND-ASSISTED SOLVENT EXTRACTION OF POROUS MEMBRANE PACKED SOLID SAMPLES.
PublicationMembranes are becoming more and more popular in analytical chemistry, which is why they are used, among others, in extraction processes. Therefore, this work focuses on the process of synthesis PVDF membranes and its optimization. The obtained membranes were used as bags for the phthalate extraction in disposable diapers for babies. Extraction was accomplished by method ultrasound-assisted solvent extraction of porous PVDF membrane...
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Methods of assaying volatile oxygenated organic compounds in effluent samples by gas chromatography—A review
PublicationThe paper is a review of the procedures for the determination of volatile and semivolatile oxygenated organic compounds (O-VOCs) in effluent samples by gas chromatography. Current trends and outlook for individual steps of the procedure for the determination of O-VOCs in effluents are discussed. The available sample preparation techniques and their limitations are described along with GC capillary columns used for O-VOCs separation...
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Determination of cyanide ion in urine samples using ion chromatography with pulsed amperometric detection.
PublicationCyanides are widely applied in industrial activity, including gold and silver mining and the production of organic chemicals. HCN is also formed directly from fossil fuel combustion sources from gasoline and diesel vehicles. In natural environment, in plants seeds for example an apple seed, it exists as a cyanogenic glycosides. The amount of cyanide ions originating from food products is however rather small. Larger concentrations...
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Direct Analysis of Samples of Various Origin and Composition Using Specific Types of Mass Spectrometry
PublicationOne of the major sources of error that occur during chemical analysis utilizing the more conventional and established analytical techniques is the possibility of losing part of the analytes during the sample preparation stage. Unfortunately, this sample preparation stage is required to improve analytical sensitivity and precision. Direct techniques have helped to shorten or even bypass the sample preparation stage; and in this...
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New, fast and cheap prediction tests for BRCA1 gene mutations identification in clinical samples.
PublicationDespite significant progress in cancer therapy, cancer is still the second cause of mortality in the world. The necessity to make quick therapeutic decisions forces the development of procedures allowing to obtain a reliable result in a quick and unambiguous manner. Currently, detecting predictive mutations, including BRCA1, is the basis for effectively treating advanced breast cancer. Here, we present new insight on gene mutation...
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Preliminary studies on DNA retardation by MutS applied to the detection of point mutations in clinical samples
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Application of the chromatographic retention index system for the estimation of the calibration constants of permeation passive samplers with polydimethylsiloxane membranes
PublicationThe paper presents the results of research on the calibration of permeation passive samplers equipped with polydimethylsiloxane (PDMS) membranes using the physico-chemical properties of the analytes. Strong correlations were found between the calibration constants of the samplers and the linear temperature-programmed retention indices of the analytes determined on columns coated with pure PDMS (r2 = 0.914). These correlations...
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Kompleks niesprostania we wczesnej twórczości prozatorskiej Adolfa Rudnickiego na przykładzie „Szczurów” i „Niekochanej”
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Sample preparation for gas chromatographic determination of halogenated volatile organic compounds in environmental and biological samples
PublicationPodstawowym elementem przygotowania próbek środowiskowych i biologicznych do analizy jest etap izolacji i/lub wzbogacania polegający na przeniesieniu analitów z matrycy pierwotnej charakteryzującej się złożonym i często zmiennym składem (próbka oryginalna) do matrycy wtórnej z równoczesnym usunięciem substancji przeszkadzających (izolacja)i zwiększeniem stężenia analitów do poziomu powyżej granicy oznaczalności stosowanego przyrządu...
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An inter-laboratory validation of methods of lipid peroxidation measurement in UVA-treated human plasma samples
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Selective determination of cocaine and its metabolite benzoylecgonine in environmental samples by newly developed sorbent materials
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Efficient recovery of electrophoretic profiles of nucleoside metabolites from urine samples by multivariate curve resolution
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Determination of carbamazepine in urine and water samples using amino-functionalized metal–organic framework as sorbent
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Application of a smartphone based spectrophotometer for rapid in-field determination of nitrite and chlorine in environmental water samples
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Construction and Validation of Simulation Models of Samples Made from 316L Steel by Applying Additive Technique
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Comparison of dry and living Sphagnum palustre moss samples in determining their biocumulative capability as biomonitoring tools
PublicationPorównano właściwości suchych i żyjących mchów Sphagnum palustre poprzez wyznaczenie ich zdolności biokumulacyjnych jako narzędzia przy biomonitoringu. Zastosowano dwie formy mchów w celu porównania ich wad i zalet i wybraniu najlepszej. Badania przeprowadzono na terenie zurbanizowanym w celu wyznaczenia głównych źródeł zanieczyszczeń. Przeprowadzono analizę klasterową oraz analizę głównych składowych w celu zidentyfikowania profilu...
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Development of New UV–vis Spectroscopic Microwave-Assisted Method for Determination of Glucose in Pharmaceutical Samples
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Simultaneous determination of non-steroidal anti-inflammatory drugs and oestrogenic hormones in environmental solid samples
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Transmission vs. Diffuse Transmission in Circular Dichroism: What to Choose for Probing Solid-State Samples?
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Measuring radioactive powder samples on the highresolution powder diffraction beamline at the European Synchrotron Radiation Facility
PublicationThis laboratory note describes a new sample preparation technique to enable high-resolution powder diffraction experiments at the European Synchrotron Radiation Facility on radioactive samples. The sample preparation involves setting the active material in resin and several layers of encapsulation suitable for measurement at the beamline. This has allowed low-temperature measurements on very small quantities of samples, providing...
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Application of magnetic nanoparticles for magnetic solid-phase extraction in preparing biological, environmental and food samples
PublicationThe need to obtain meaningful results as the basis for determining the content of trace amounts of analytes has become the driving force behind the development of modern analytical techniques, including sample-preparation techniques, such as solid-phase extraction (SPE). Recently, great interest was aroused in the use of magnetic nanoparticles (MNPs) in SPE. These materials exhibit high selectivity, and, in small amounts, can provide...
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The use of selected analytical techniques for pollutants determination in the environmental samples collected from the Arctic regions
PublicationThe paper concern importance of the use of analytical techniques for pollutants determination in the Arctic based on the example of total organic carbon, phenolsandformaldehyde determinationandmeasurementofpHand electrical conductivity parameters in surfacewater samples collected fromthe Revelva catchment.
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Arctic as a reservoir for polycyclic aromatic hydrocarbons and polychlorinated biphenyls- water samples from Foxfonna glacier
PublicationPolycyclic aromatic hydrocarbons and polychlorinated biphenyls are groups of stable compounds, hard to biodegrade, potentially toxic. Their presence in Arctic environment may have a big impact on natural balance, fauna and flora. Although Arctic areas should be unpolluted, some amounts of pollutants are transferred from lower latitudes with sea currents and air masses. This paper presents the amounts of selected persistent organic...
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Developments in ultrasound-assisted microextraction techniques for isolation and preconcentration of organic analytes from aqueous samples
PublicationThe great potential of ultrasonic assistance in sample preparation, especially extraction, is being recognized. In this review, we discuss the applications of ultrasonic radiation in assisting microextraction. Topics covered include ultrasound-assisted emulsification microextraction, ultrasound-assisted-emulsification-dispersive liquid-liquid microextraction, and ultrasound-assisted hollow-fiber liquid-phase microextraction with...
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‘Green’ multi - residue methods for the determination of high importance currently used pesticides in environmental samples
PublicationThe purpose of the research has been to develop and apply ‘green’ analytical methodologies to control and monitor the level of currently used pesticides from different chemical groups in aqueous samples. For extraction of analytes solid - phase microextraction (SPME) and dispersive liquid - liquid microextraction (DLLME) have been applied and compared. For SPME, commonly used materials for coating fibers include: polydimethylsiloxane...