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Search results for: DESI
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Monitoring of volatile organic compounds (VOCs) in atmospheric air. Part I. On-line gas analyzers
PublicationThe paper reviews the subject literature concerning the analytical instruments routinely used for monitoring volatile organic compounds in atmospheric air. The analyzers are classified as stationary or mobile according to their ease of transport. Stationary DOAS (Differential Optical Absorption Spectroscopy) analyzer is characterized, as are MIMS (Membrane Introduction Mass Spectrometry), MESI (Membrane Extraction with Sorbent...
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Design and Configuration of Context-aware VoIP Telephony Systems
PublicationVoice over IP is a widely used concept with regard to a realization technology of different types of telephony systems, including those that are used in enterprises. Such systems of a call procesing component and a set of desk endpoints that are pervasove from a user perspective. Those andpoints are usually not mobile, but in result can deliver a much greater set of functions needed in an everyday office work. Those functions also...
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A distributed scheme for optimization of interdomain routing between collaborating domains
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Bezpieczeństwo i wydajność wybranych algorytmów kryptograficznych w systemie RSMAD
PublicationW artykule scharakteryzowano architekturę bezpieczeństwa Radiowego Systemu Monitorowania i Akwizycji Danych z Urządzeń Fotoradarowych (w skrócie RSMAD), ze szczególnym uwzględnieniem mechanizmów zapewniania poufności danych w tymże systemie. W pracy przedstawiono także szczegółowe wyniki badań w zakresie zgodności algorytmu AES-128 z kryterium SAC. Ponadto zaprezentowano analizę porównawczą wydajności algorytmów AES-128 oraz Triple-DES...
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Schweizerische Zeitschrift für Bildungswissenschaften/Revue suisse des sciences de l’éducation/Rivista svizzera di scienze dell’educazione
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CANADIAN JOURNAL OF INFORMATION AND LIBRARY SCIENCE-REVUE CANADIENNE DES SCIENCES DE L INFORMATION ET DE BIBLIOTHECONOMIE
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Koncert Pasyjny w Kościele Świętej Trójcy w Gdańsku
EventsPolitechnika Otwarta zaprasza na Koncert Pasyjny. Wystąpią: Akademicki Chór Politechniki Gdańskiej i Orkiestra Polskiej Filharmonii Kameralnej Sopot pod dyrekcją Mariusza Mroza. Na organach zagra Andrzej Szadejko.
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Expert systems in assessing the construction process safety taking account of the risk of disturbances
PublicationThe objective of the paper is to present the issue of safety manage-ment during the construction process. Threats in the form of disturb-ances may occur in the preparatory phase, during the execution of the construction project and also during its operational use. The arti-cle presents the concept of applying the methodology based, among others, on Learning Bayesian Networks, Artificial Neural Networks and Support Vector Machine,...
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To i-vote or not to i-vote: Drivers and barriers to the implementation of internet voting
PublicationThis paper investigates the drivers and barriers of internet voting and the implications of a global pandemic for the development of the respective technology. In contrast to the expected uptake in the early 2000s of internet voting, the technology is still rather seldomly used in election systems around the world. The paper at hand explores the different forces that drive or impede internet voting adoption from a political, social,...
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Decision Support in Selecting a Reliable Strategy for Sustainable Urban Transport Based on Laplacian Energy of T-Spherical Fuzzy Graphs
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Detection of stress corrosion cracking dynamics by dynamic electrochemical impedance spectroscopy.
PublicationKlasyczne badania korozji naprężeniowej nie dają precyzyjnych informacji o dynamice takiego procesu korozyjnego. Nowa technika dynamicznej elektrochemicznej spektroskopii impedanyjnej, która została opracowana w Katedrze Elektrochemii, Korozji i Inżynierii Materiałowej stwarza takie możliwości. Fakt ten związany z zastosowaną metodologią analizy umożliwiającą selektywną analizą czasowo-częstotliwościową danych pomiarowych.Praca...
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A Novel [4+2] Cycloaddition Reaction Involving Lawesson’s Reagent. Structure and Specific Fragmentations of a New Cyclic 1,2-Thiaphosphinane-4-one
PublicationA crude morpholine enamine of acetone treated with Lawesson’s reagent unexpectedly yielded a six-membered thiaphosphinane-4-one. This compound is the first example of a new class of heterocycles. It has been proven that it is formed from 4-methyl-2-morpholino-1,3-pentadiene which is usually present in crude morpholine enamine batches. A mechanism of this regioselective reaction was postulated and a characteristic chair-like conformation...
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Evidence for solid state electrochemical degradation within a small molecule OLED
PublicationAcridone derivative have been synthesised and used as OLED (Organic Light Emitting Diode) emitters which were found to be electroactive. Electrochemical investigations showed a side reaction takes place inside an active layer which diminished the overall device efficiency. By using a dopant and host active layer architecture, the formation of the by product was removed. The by-product was identified as a σ-dimer formed inside an...
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Kolalos Studi pubblicati dalla Sezione di storia antica del Dipartimento dei beni culturali dell'Università di Palermo
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Wykorzystanie dynamicznej elektrochemicznej spektroskopii impedancyjnej do badania procesu pękania warstwy pasywnej na austenitycznej stali wysokostopowej AISI 304L
PublicationCelem pracy było wykazanie, iż dynamiczna elektrochemiczna spektroskopia impedancyjna (DEIS) może być z powodzeniem wykorzystana do badania procesu pękania warstwy pasywnej na wysokostopowej stali AISI 304L w warunkach jednoczesnego działania naprężeń mechanicznych oraz agresywnego środowiska korozyjnego. W oparciu o przeprowadzone badania oraz uzyskane wyniki można uznać tą technikę za dobre narzędzie elektrochemiczne służące...
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Determination of pseudocapacitance chan ges of nickel oxide NiO electrode with use of dynamic electrochemical impedancje spectroscopy
PublicationThe electrochemical capacitors (ECs) are attractive energy storage devices which can be applied in many electronic products (e.g., cameras, laptops, cell phones) or hybrid electric vehicles (HEV). The energy storage in ECs is based on capacitive (the electrical double layer charging/discharging) and pseudocapacitive (additional charge provided by faradic reaction) phenomena. Considering the electrodes exhibiting pseudocapacitance,...
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Electrochemical simulation of metabolism for antitumor-active imidazoacridinone C-1311 and in silico prediction of drug metabolic reactions
PublicationThe metabolism of antitumor-active 5-diethylaminoethylamino-8-hydroxyimidazoacridinone (C-1311) has been investigated widely over the last decade but some aspects of molecular mechanisms of its metabolic transformation are still not explained. In the current work, we have reported a direct and rapid analytical tool for better prediction of C-1311 metabolism which is based on electrochemistry (EC) coupled on-line with electrospray...
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A Comprehensive Analysis of Impedance of the Electrochemical Cell
PublicationA comprehensive impedance characteristics of two electrodes electrochemical cell has been pre sented. In this method a multisinusoidal current excitation signal is used. The change of potential of both the electrodes are all registered as a function of time. The proposed method gives the possibility of determining the impedance of both electrodes individually as well as the impedance of a twoelectrode system. Additional application...
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Komputerowe wspomaganie procesu projektowania w dziedzinie architektury
PublicationGłówną zaletą zastąpienia deski kreślarskiej komputerem była możliwość szybkiej reprodukcji rysunków architektonicznych i ich ponownego wykorzystania. Wraz z rozwojem technik komputerowych powstawały nowe możliwości w projektowaniu. Możliwość wykonania trójwymiarowego modelu pozwoliła na sprawdzanie pewnych zależności bez konieczności tworzenia prototypów. Wykonany trójwymiarowy model mógł być także wykorzystany w różnego typu...
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Elektrochemiczna spektroskopia impedancyjna niestacjonarnych procesów elektrodowych.
PublicationCelem pracy było sprawdzenie przydatności Dynamicznej Elektrochemicznej Spektroskopii Impedancyjnej (DEIS) w analizie niestacjonarnych układów elektrodowych. Klasyczna elektrochemiczna spektroskopia impedancyjna może być stosowana tylko w przypadku, gdy badany układ jest w stanie stacjonarnym, w sensie termodynamicznym, podczas gdy większość układów elektrochemicznych tego wymagania nie spełnia. Istniejące ograniczenia narzucają...
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STARZENIE SIĘ LUDNOŚCI – PERSPEKTYWA LOKALNA
PublicationPostępujące starzenie się ludności determinuje zmiany społeczne i ekonomiczne. W literaturze przedmiotu ich charakter, przebieg i skutki najczęściej poddaje się analizie i ocenie w skali makro. Tymczasem zmiany demograficzne mają swoje istotne konsekwencje również w perspektywie lokalnych jednostek terytorialnych i stanowią wyzwanie dla działań władz lokalnych. Celem artykułu jest wskazanie szans i zagrożeń powodowanych postępującym...
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Udział społeczeństwa w procedurze planowania przestrzennego – analiza metod i technik konsultacji społecznych na przykładzie polskich małych i średnich miast w ramach projektu POWER
PublicationUdział społeczeństwa w procesie opracowywania aktów planowania przestrzennego w Polsce ma charakter informacyjny, a nie dialogiczny, co przyczynia się m.in. do jego konfliktogenności. W latach 2016–2021 zrealizowano ogólnokrajowy projekt POWER dofinansowany ze środków Unii Europejskiej, którego celem było m.in. przetestowanie angażujących metod i technik konsultacji społecznych, zwiększenie poziomu współdecydowania i poprawa metod...
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Multisine impedimetric monitoring with an in-depth distribution of relaxation times analysis of WE43 and AZ31 magnesium alloys corrosion
PublicationThis research aims to develop and utilize an impedance-based tool for monitoring non-stationary electrochemical processes, coupling the multisinusoidal perturbation signal approach and distribution of relaxation times (DRT) analysis for the first time. The approach was used to distinguish independent processes occurring at the surface of AZ31 and WE43 Mg alloys undergoing corrosion in Hank’s Balanced Salt Solution at 37 °C. We...
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Sport dla wszystkich w przestrzeni miasta. Przegląd rozwiązań przestrzennych i programów aktywizujących w wybranych krajach
PublicationNiniejsze opracowanie dotyczy identyfikacji współczesnych form aktywności fizycznej w przestrzeni miast, powiązanej infrastruktury (urządzeń, obiektów i terenów sportowych) oraz programów aktywizujących i włączających mieszkańców miast, przedstawienie dobrych praktyk i rozwiązań przestrzennych w wybranych krajach świata (m.in. Danii, Holandii, Wielkiej Brytanii, Kanadzie, Australii) oraz możliwości ich implementacji w warunkach...
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Night in a big city. Light festivals as a creative medium used at night and their impact on the authority, significance and prestige of a city
PublicationCities in times of global urbanization, are looking for completely new marketing methods, one such tool is the creative use of artificial light after dark, in the form of light festivals. This paper aims to introduce the historical development of the phenomenon and contemporary as well as contemporary illuminations / projects of illuminations of Fete des Lumieres festival in Lyon, Luminale in Frankfurt or on a smaller scale Lights...
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Cryptographic Protocols' Performance and Network Layer Security of RSMAD
PublicationW artykule omówiono architekturę bezpieczeństwa warstwy sieciowej Radiowego Systemu Monitorowania i Akwizycji Danych z urządzeń fotoradarowych (w skrócie RSMAD). Bezpieczeństwo w warstwie sieciowej tego systemu jest zapewniane przede wszystkim dzięki wykorzystaniu Virtual Private Network (w skrócie VPN). W tym celu zaimplementowano dwa protokoły IPsec i L2TP.Zastosowane mechanizmy ochrony danych, w tym typy i parametry VPNów zostały...
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L'economia mondiale dopo la guerra fredda
PublicationChe cosa è successo negli equilibri economici mondiali a partire dal 1989 e dalla dissoluzione del vecchio ordine sovietico? Dopo aver esaminato gli Usa e i suoi competitori asiatici, Giappone e Cina, il libro si concentra sull’Europa e sulle grandi trasformazioni portate dalla riunificazione tedesca, da Maastricht e dalla nascita dell’euro. Infine analizza, nell’ambito della globalizzazione, il ruolo dei BRICS, lo sviluppo economico...
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Chemiluminogenic acridinium salts: A comparison study. Detection of intermediate entities appearing upon light generation
PublicationThe nine derivatives of acridine-9-carboxylic acid (CMADs) capable for chemiluminescence (CL), representing various classes of compounds were isolated in a chemically pure state (assessed by RP-HPLC) and identified using high resolution mass spectrometry (ESI-QTOF) and magnetic resonance (1H NMR) techniques. Among them are aryl acridinium esters, containing certainly selected and located substituents in both aromatic systems, an...
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An integral-differential method for impedance determination of the hydrogen oxidation process in the presence of carbon monoxide in the proton exchange membrane fuel cell
PublicationThe impedance of a proton exchange membrane fuel cell powered by hydrogen contaminated with carbon monoxide, ranging from 150 to 300 ppb, is measured and discussed. The tested range of CO concentration complied with the fuel standard specified in the ISO standards. Studies of influence of CO contamination on operation of PEMFC are crucial for further development and commercialization of fuel cells for automotive applications. Based...
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Effect of cobalt addition on the corrosion behaviorof near equiatomic NiTi shape memory alloy in normal saline solution: electrochemical and XPS studies
PublicationThe electrochemical and corrosion (uniform and localized) behavior of a binary Ni52Ti48 shape memory alloy (SMA) and two ternary Ni52Ti48-xCox (x = 1.5 and 4.0 wt.%) SMAs were studied. Measurements were conducted in 0.9% NaCl solution at 37 oC employing various electrochemical methods. These include: linear polarization resistance (LPR), linear sweep voltammetry (LSV), chronoamperometry and dynamic electrochemical impedance spectroscopy...
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Smart Specializations as Innovative Ecosystems
PublicationIn the article it is showed that regional smart specializations that are currently the most important tool of the European innovation policy may be perceived, and if effective should constitute, innovative ecosystems. The article presents the concepts of smart specializations and innovative ecosystems. The concept of innovative ecosystem is, in the article, presented from the perspective of its foundation and relations to other...
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Anna Wałek dr
PeopleDr Anna Wałek, President of IATUL – International Association of University Libraries, director of the Gdańsk University of Technology Library. An experienced library manager, an expert in the field of Open Science, and organization and management of a scientific library. She conducts scientific research in data management in various scientific disciplines, metadata for research data, and data management support services - incl....
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Determination of sex hormone concentration in wastewater samples.
Open Research DataConcentration levels of five selected steroid hormones in influent and effluent waters from wastewater treatment plant were determined using SPE(C18)-HPLC-ESI/MS/MS method. Sex hormones like: estradiol, estriol, estrone, 17-α-ethynyloestradiol, progesterone were present in all influent wastwater samples.
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Fiber-optic biosensors with metal-oxide ALD coatings
ProjectsProject realized in Department of Metrology and Optoelectronics according to PPN/BFR/2019/00005/U/00001 agreement from 2019-12-19
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Theorie und Praxis des Theaters / Teoría y Práctica del Teatro / Theory and Practice of Theatre / Théorie et Pratique du Théâtre
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Kazimierz Market Place. Akwarela 38x56cm
PublicationL'acquerello in Alessandria, la mostra internazionale patrocinata dal Comune e dalle Provincia di Alessandria, dalla Regione Piemonte e dal Comune di Vignale e organizzata dall'Associazione italiana acquerellisti. L'esposizione, circa 150 acquerelli dei socie Aia e di artisti provenienti da Australia, Belgio, Brasile Polonia e Spagna per presentare le principali tecniche dell'acquerelli e le diverse concezioni artistiche e stilistiche...
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Pesticide residues levels in honey from apiaries located of Northern Poland
PublicationConcentration levels of 30 pesticide residues were measured in honey samples collected from apiaries in northern part of Poland (Pomerania) using method based on the QuEChERS extraction followed by liquid chromatography-tandem mass spectrometry with electron spray ionization (LC-ESI-MS/MS). In 29% of the samples were found positive for at least some of the target compounds. Concentration of bifenthrin, fenpyroximate, methidathion,...
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Piotr Zygmunt Kowalski mgr
PeopleW 2009 r. ukończył studia magisterskie na kierunku Ochrona Dóbr Kultury (specjalność: Konserwatorstwo) na Wydziale Sztuk Pięknych Uniwersytetu Mikołaja Kopernika w Toruniu.
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Typology of the Black Tents Architecture between Iranian nomad tribes
PublicationEvidence of the past shows variation in human settlements. Nomadic house the” Black Tent” shows relationship between humans and the natural environment surrounding them. Black Tents are made of natural materials consistant with environmental conditions. This paper discusses nomadic living space of some Iranian tribes located in different regions to show their unique architecture and culture. Rediscovering different architecture...
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The profiles and spectrum of aqua solution of tannic acid by HPLC-DAD-MS analysis.
Open Research DataThe profiling of tannic acid is determined by examining the content and proportion / ratio of gallotannins [Aras et al. 2016, Clifford et al. 2007, Gauri et al. 2012, Nishizawa et al. 1982]. In order to check the ion mass distribution (TIC) in an aqueous solution of commercial tannic acid, a direct sample injection (TA) was performed into the mass spectrometer....
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Bedload transport and temporal variation of non-uniform sediment in a seepage-affected alluvial channel
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Advances in mass spectrometry for iron speciation in plants
PublicationIron is an important nutrient essential for plants and critical for human health. The state-of-the art of methods for iron speciation in cereal grains and plant fluids is critically reviewed. Particular attention is given to the latest developments in the coupling of HPLC with the parallel ICP MS and electrospray ionization (ESI) MS/MS detection, usually QTOF MS or Q-Orbitrap MS, for the identification and quantification of iron...
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Organic and conventional kiwifruit, myths versus reality: antioxidant, antiproliferative and helth effects
PublicationComparison between organic and conventional kiwifruit cultivars 'Hayward' and 'Bidan', which was done by four radical scavenging assays, ESI-MS, and DSC measurements, showed significant differences between the cultivars. Such results were not estimated in kiwifruit growing under organic and conventional conditions. The extraction of bioactive compounds was done by two different methods: sequential extraction with ethyl acetate...
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The Use of Sustainability Reporting Instruments in the Global Airline Industry in Financial Year 2019
Open Research DataThis dataset provides an overview of the GRI topic-specific disclosures global passenger airline companies reported in their 2019 financial year sustainability reports and the specific SDGs they addressed. Additionally, it includes information on the frequency of application of other well-known SR instruments (i.e., SASB, IIRC, CDSB, CDP, UNGC, ISO...
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Instrumentalne metody badania struktury i aktywności biomolekuł
e-Learning Courses1. Analiza kinetyki denaturacji białka przy użyciu różnicowej kalorymetrii skanningowej.2. Zastosowanie średniociśnieniowej chromatografii cieczowej do izolacji i charakterystyki biomakromolekuł.3. Wykorzystanie HPLC do izolacji substancji naturalnych i badania czystości antybiotyków.4. Wyznaczanie masy cząsteczkowej białka z zastosowaniem spektroskopii MS-ESI.5. Spektroskopia FTIR w badaniu struktury drugorzędowej białek.6. Określanie...
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Kreowanie wartości publicznej przez wykorzystanie wolnego i otwartego oprogramowania GNU Health
PublicationGłównym celem pracy jest prezentacja roli, potencjału i funkcjonalności oprogramowania GNU Health. Ten zaawansowany i dojrzały, wysokiej jakości produkt - opracowany i nieustannie rozwijany w ramach projektu wolnego i otwartego oprogramowania - jest z sukcesem wdrażany w placówkach ochrony zdrowia w wielu krajach. Jego zastosowanie przyczynia się nie tylko do usprawnień w zarządzaniu praktyką medyczną lecz również odgrywa ważną...
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Experimental and Quantum Chemical Evaluation of 8-Hydroxyquinoline as a Corrosion Inhibitor for Copper in 0.1 M HCl
PublicationThe corrosion inhibition properties of 8-hydroxyquinoline (8-HQ) in 0.1 M HCl for copper have been investigated by using experimental (electrochemical impedance spectroscopy (EIS), dynamic electrochemical impedance spectroscopy (DEIS), and potentiodynamic polarization) and theoretical methods complemented by surface morphological examination with the aid of scanning electron microscopy (SEM) and electron dispersive X-ray spectroscopy...
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Merging Proline:Xylitol Eutectic Solvent in Crosslinked Chitosan Pervaporation Membranes for Enhanced Water Permeation in Dehydrating Ethanol
PublicationThe scope of this research aims at merging a new deep eutectic mixture (DES) into a biopolymer-based membrane for a pervaporation application in dehydrating ethanol. Herein, an L-proline:xylitol (at 5:1) eutectic mixture was successfully synthesized and blended with chitosan (CS). A complete characterization of the hybrid membranes, in terms of morphology, solvent uptake, and hydrophilicity, has been conducted. As part of their...
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Understanding the origin of high corrosion inhibition efficiency of bee products towards aluminium alloys in alkaline environments
PublicationVarious bee products were found to be efficient corrosion inhibitors of aluminium in different environments. In particular, bee pollen was found to be highly effective in alkaline electrolytes, yet its highly complex composition and possible synergistic interactions hinder determination of the compounds acting as active corrosion inhibitors. The main purpose of the following work is to investigate the effect of solvents used for...
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Investigation of the electrochemical behaviour of AA1050 aluminium alloy in aqueous alkaline solutions using Dynamic Electrochemical Impedance Spectroscopy
PublicationThe paper presents the electrochemical behaviour of aluminium alloy AA1050 in aqueous alkaline media in the pH range 14–8.5. Electrochemical study was applied in order to obtain comprehensive information on the mechanism and kinetics of the process of anodic dissolution of aluminium, supplemented by monitoring of surface topography using an electron microscope. The corrosion rate of AA1050 increases with increasing concentration...