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Search results for: meldrum's acid
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Preliminary Microbiological Tests of S-Carvone and Geraniol and Selected Derivatives of These Compounds That May Be Formed in the Processes of Isomerization and Oxidation
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Nowa technologia pomiarów deformacji materiału T-S. XII Krajowa Konferencja Mechaniki Gruntów i Fundamentowania.
PublicationW artykule przedstawiono treściwy opis wybranych elementów nowego stanowiska badawczego dla materiału Taylor-Schneebeli (T-S) w warunkach płaskiego stanu odkształcenia. Omówiono wykorzystywane systemy pomiarowe, w tym nowy oparty na rejestracji zdjęć cyfrowych. Analiza pomiarów związana jest z metodami cyfrowej interpretacji obrazów, co umożliwia śledzenie pola przemieszczania i obrotów cząstek materiału modelowego.
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Analiza słonecznego ogrzewania wody. Instalacje Sanitarne**2002 nr 3 s. 30-32, 6 rys.
PublicationPrzedstawiono studium parametryczne oceny ekonomicznej efektywności insta-lacji slonecznego ogrzewania wody, wykorzystującej zmodyfikowaną do potrzebenergetyki słonecznej metodę ''Zaktualizowanej Wartości Netto'' -NPVW. Stwier-dzono istnienie znacznych obszarów opłacalności słonecznego ogrzewania wodyw okresie 25-letniego horyzontu czasowego. Jest jednak konieczna pomoc rządowa w zakresie inwestowania na instalację słoneczną.
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Gry bardzo serio. CXO Nowy Magazyn Kadry Zarządzającej.**2002 nr 12 s.26-28.
PublicationGry symulacyjne Lean są typem symulacji społecznej, której zasady są opartenie na współzawodnictwie, ale na wypracowaniu zespołowej taktyki działania.Celem symulacji jest wzmacnianie u uczących się umiejętności współdziałania,negocjowania, osiągania kompromisu, wypracowania wspólnej strategii Leanprzez wszystkich uczestników zespołu reprezentujących różne interesy. Arty-kuł przedstawia rodzaje gier symulacyjnych, sposoby...
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Plan zagospodarowania przestrzennego województwa, jakie oczekiwania? Przes- trzeń**2002 nr 15 s. 29-30.
PublicationPrzedstawiono doświadczenia w planowaniu zagospodarowania przestrzennego,programowaniu rozwoju województwa i koordynowaniu planowania miejscowego wwojewództwie pomorskim. Określono oczekiwania wobec planu zagospodarowaniaprzestrzennego województwa jako elementu planowania regionalnego i elementuprowadzenia gospodarki przestrzennej.
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Heterojunction of (P, S) co-doped g-C3N4 and 2D TiO2 for improved carbamazepine and acetaminophen photocatalytic degradation
PublicationNovel photocatalysts of phosphorus and sulfur co-doped graphitic carbon nitride incorporated in 2D TiO2 structure were successfully fabricated and applied for solar-driven degradation of emerging pollutants from the group of pharmaceuticals not susceptible to biodegradation. The hybrid photocatalysts with different loadings of (P, S)-doped g-C3N4 were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR),...
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Ochrana před úrazem elektrickým proudem při použití proudových chráničů v obvodech s měniči frekvence
PublicationObwody zawierające przemienniki częstotliwości charakteryzują się tym, że kształt prądu ziemnozwarciowego zależy od miejsca zwarcia. Prądy ziemnozwarciowe mogą mieć różną częstotliwość oraz być mocno odkształcone, a także, w zależności od zastosowanego układu prostownikowego, mogą być jednokierunkowe o małym lub dużym tętnieniu. Kształt i częstotliwość prądu znacząco wpływa na poprawne działanie wyłączników różnicowoprądowych....
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The role of hydrogen bonding on tuning hard-soft segments in bio-based thermoplastic poly(ether-urethane)s
PublicationThis work describes the preparation of bio-based thermoplastic poly(ether-urethane)s (TPU) via a prepolymer method and investigates the effect of varying the interphase hydrogen-bonding (H-bonding) on physicochemical, thermal and mechanical properties. This was achieved by varying the glycol type and molar ratio of [NCO]/[OH] groups used during the prepolymer chain extending step. The TPUs’ chemical structure was analyzed by Fourier...
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Synergistic effects in micellization and surface tension reduction in nonionic gemini S-10 and cationic RTAB surfactants mixtures
PublicationMixtures of nonionic gemini surfactant S-10 (α,α′-[2,4,7,9-tetrametyl-5-decyne-4,7-diyl]bis[ω-hydroxy -polioxyetylene] with cationic alkyltrimethylammonium bromides of different alkyl chain length (RTAB) were investigated. Basing on surface tension measurements the cmc values and other adsorption parameters were found. The Clint, Rubing’s and Rosen theories were applied for evaluation of the synergistic effects in mixed films and...
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Problemy planowania rozwoju systemu transportowego w obszarach metropolitalnych – przykład Obszaru Metropolitalnego G-G-S
PublicationProblemy rozwoju systemów transportowych w metropoliach wynikają ze specyfiki tych obszarów, ich skali i struktury przestrzennej. Obszary te charakteryzują się dużą wewnętrzną integracją funkcjonalną oraz dobrze rozwiniętą siecią transportową. Dynamicznie rozwijające się obszary metropolitalne mają odrębne systemy zarządzania finansami, rozwią- zania prawne oraz administrację, a także własne organy planowania i zarządzania, które...
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Synthesis, structure and properties of poly(ether-urethane)s synthesized using a tri-functional oxypropylated glycerol as a polyol
PublicationThe main aim of this work was to obtain poly(ether-urethane)s using tri-functional polyoxyalkylene polyol (Rokopol G1000), which introducing the chemical cross-links into the structure of polyurethanes. Poly(ether-urethane)s were prepared using two-step method, called prepolymer method, which involves in the first step the reaction of 4,4'-diphenylmethane diisocyanate (MDI) and tri-functional polypropylene glycol glycerol triether...
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Prebiotic Potential of Oligosaccharides Obtained by Acid Hydrolysis of α-(1→3)-Glucan from Laetiporus sulphureus: A Pilot Study
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Efficacy of tranexamic acid supplemented with local infiltration analgesia in reducing blood loss in patients undergoing unicompartmental knee arthroplasty
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Efficacy of tranexamic acid supplemented with local infiltration analgesia in reducing blood loss in patients undergoing unicompartmental knee arthroplasty.
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Molecular Heteroconjugation Equilibria in (n-Butylamine + Acetic Acid) Systems in Binary (Dimethyl Sulfoxide + 1,4-Dioxane) Solvent Mixtures
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Bimodal Nd-Doped LuVO4 Nanoprobes Functionalized with Polyacrilic Acid for X-Ray Computed Tomography and NIR Luminescent Imaging
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Proline, glutamic acid, and leucine rich protein 1 (PELP1) expression in deep paravertebral muscles in idiopathic scoliosis girls
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Exploring ion-ion preferences through structure-property correlations: amino acid-derived, bis(guanidinium) disiloxane salts
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The type of blood used to feed Aedes aegypti females affects their cuticular and internal free fatty acid (FFA) profiles
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Raman and surface-enhanced Raman spectroscopy investigation of vasopressin analogues containing 1-aminocyclohexane-1-carboxylic acid residue
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Application of hollow mesoporous carbon nanospheres as an high effective adsorbent for the fast removal of acid dyes from aqueous solutions
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Ibotenic acid lesion of the ventral hippocampus differentially affects dopamine and its metabolites in the nucleus accumbens and prefrontal cortex in the rat
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Enhanced Activity and Sustained Release of Protocatechuic Acid, a Natural Antibacterial Agent, from Hybrid Nanoformulations with Zinc Oxide Nanoparticles
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Investigation of OH radicals formation on the surface of TiO2/N photocatalyst at the presence of terephthalic acid solution. Estimation of optimal conditions
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Molecular and structural basis of inner core lipopolysaccharide alterations in Escherichia coli: incorporation of glucuronic acid and phosphoethanolamine in the heptose region.
PublicationIt is well established that lipopolysaccharide (LPS) often carries nonstoichiometric substitutions in lipid A and in the inner core. In this work, the molecular basis of inner core alterations and their physiological significance are addressed. A new inner core modification of LPS is described, which arises due to the addition of glucuronic acid on the third heptose with a concomitant loss of phosphate on the second heptose. This...
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Cations of amino acid alkyl esters conjugated with an anion from the group of NSAIDs – As tunable pharmaceutical active ionic liquids
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Molecular heteroconjugation equilibria in (n-butylamine + acetic acid) systems in binary (dimethyl sulfoxide + 1,4-dioxane) solvent mixtures
PublicationWyznaczono stałe kwasowe Ka(HA), Ka(BH+) oraz stałe równowagi KAHA-, KBHE+ i KAHB, w układach (n-butyloamina + kwas octowy) bez przeniesienia protonu w binarnych mieszaninach rozpuszczalników (DMSO + 1,4-dioksan). Wartości stałych wyznaczono z wykorzystaniem metody miareczkowania potencjometrycznego przy stałej sile jonowej. Stwierdzono, iż stałe heterokoniugacji molekularnej w badanych mieszaninach rozpuszczalników są liniowo...
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Supramolecular structures of bis-thionooxalamic acid esters derived from (±)-cyclohexane-1,2-diamine and (±)-1,2-diphenylethylenediamine
PublicationZsyntezowano dwa racemiczne estry kwasu bis(tiooksamowego) i zbadano ich sposób upakowania w sieci krystalicznej. Analiza rentgenograficzna monokryształów badanych związków wykazała, że organizują się one w jednowymiarowe struktury, które tworzone są przez molekuły o przeciwnej chiralności, połączone za pomocą trójcentrowych wiązań wodorowych C=S...NH...O=C. Powstające agregaty są dodatkowo stabilizowane przez słabe oddziaływania...
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Cold plasma treatment of tannic acid as a green technology for the fabrication of advanced cross-linkers for bioactive collagen/gelatin hydrogels
PublicationTannic acid (TA) is a natural compound studied as the cross-linker for biopolymers due to its ability to form hydrogen bonds. There are different methods to improve its reactivity and effectiveness to be used as a modifier for biopolymeric materials. This work employed plasma to modify tannic acid TA, which was then used as a cross-linker for fabricating collagen/gelatin scaffolds. Plasma treatment did not cause any significant...
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Influence of hydrochloric acid concentration and type of nitrogen source on the electrochemical performance of TiO2/N-MoS2 for energy storage applications
PublicationIn this work, nitrogen-doped molybdenum sulfide was directly deposited on titanium dioxide nanotubes substrate (TiO2/N-MoS2) during hydrothermal synthesis. The study focuses on the influence of hydrochloric acid concentration used for the synthesis, with the results indicating its essential role in thioacetamide hydrolysis and thus in the effectiveness of the N-MoS2 deposition. The electrode material itself is characterized by...
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No Evidence for Sex-specificity in Vitamin C, E and Fatty Acid Content of Human Milk from Healthy Polish Mothers
PublicationHuman milk (HM) is a complex fluid that meets the nutritional needs of infants. Its composition idrfs associated with environmental, maternal, and foetal variables. It provides nutrients and bioactive substances, including cytokines, immunoglobulins, and constituents with antioxidative properties. Boys are reportedly more susceptible to oxidative stress. This study aimed to determine the relationship between infant sex and the...
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Overcoming carboxylic acid inhibition by granular consortia in high-load liquefied food waste fermentation for efficient lactate accumulation
PublicationGranular sludge, a self-aggregating spherical biofilm, possesses better stability compared to flocculent sludge under extreme conditions. This study compared the ability of anaerobic granular sludge (AnGS) and flocculent waste activated sludge (WAS) to convert food waste (FW) into highly-valuable optically active lactic acid (LA), a central and versatile intermediate platform molecule. Different loadings (30–60 g volatile suspended...
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Comparison and Optimization of Saccharification Conditions of Alkaline Pre-Treated Triticale Straw for Acid and Enzymatic Hydrolysis Followed by Ethanol Fermentation
PublicationThis paper concerns the comparison of the efficiency of two-stage hydrolysis processes, i.e., alkaline pre-treatment and acid hydrolysis, as well as alkaline pre-treatment followed by enzymatic hydrolysis, carried out in order to obtain reducing sugars from triticale straw. For each of the analyzed systems, the optimization of the processing conditions was carried out with respect to the glucose yield. For the alkaline pre-treatment,...
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Plasma free amino acid profiling as metabolomic diagnostic and prognostic biomarker in paediatric cancer patients: a follow‑up study
PublicationAmino acids (AAs) play a crucial role in cancer cell metabolism. Levels of 22 plasma AAs at the time of diagnosis and after treatment were established among 39 pediatric cancer patients and 33 healthy children. Glutamic acid levels decreased and tryptophan levels increased during treatment. Cancer patients presented significantly lower levels of glutamine and leucine post-treatment while levels of 12 other AAs were higher comparing...
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Ammine(2-ethylpyridine-κN)bis(tri-tert-butoxysilanethiolato-κS)cobalt(II)
PublicationTytułowy związek [Co(C12H27O3SSi)2(C7H9N)(NH3)] został otrzymany w reakcji dimerycznego amoniakalnego tri-tert-butoksysilanotiolanu kobaltu(II) z 2-etylopirydyną. Atom kobaltu w otrzymanym związku jest koordynowany przez dwa atomy siarki, jedną resztę 2-etylopirydyny i jedną cząsteczkę amoniaku. Dzięki specyficznemu przestrzennemu ustawieniu ligandów, dodatkowo tworzy się wiązanie wodorowe wewnątrz cząsteczkowe N-H - S
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Identification and characterization of the Indian Yellow dyestuff and its degradation products in historical oil paint tube by liquid chromatography mass spectrometry
PublicationAn analytical protocol for identification of dyes using reversed phase liquid chromatography-mass spectrometry with atmospheric pressure electrospray ionization (LC-ESI/MS) is presented. The developed method has been successfully applied in identification of euxanthic acid and euxanthone, the main components of the Indian Yellow dye in a historical oil paint tube produced by Richard Ain`es, a recognizable French company supplying...
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Occurrence and Determination of Volatile Fatty Acids in Wastewater of Different Origin
PublicationOpracowano metodykę oznaczania krótkołańcuchowych alifatycznych kwasów monokarboksylowych w ściekach rożnego pochodzenia stosując ekstrakcję za pomocą eteru metylo-tert-butylowego na etapie przygotowania próbek i chromatografię gazową z kolumną kapilarną Stabilwax-DA i Rtx-624, natomiast na etapie detekcji stosowano spektrometr mas.
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α-Amino Acids In Water: A Review Of VCD And ROA Spectra
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Peroxidative metabolism of fatty acids in the course of tick-borne encephalitis
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Applicability of phenolic acids as effective enhancers of cocrystals solubility of methylxanthines
PublicationApplicability of phenolic acids as potential cocrystal formers for methylxanthine derivatives was analyzed both in terms of cocrystallization probabilities and solubility advantage. The cocrystal formation abilities were evaluated using mixing enthalpy estimated within the conductor like screening model for real solvents (COSMO-RS) framework. The solubility improvement of potential cocrystals was estimated by formulation of the...
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Recent advances in extraction and analysis procedures of natural chlorogenic acids
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Calibration of POCIS and PASSIL passive samplers – influence of humic acids
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Capillary Electrophoresis in Determination of Low Molecular Mass Organic Acids
PublicationThis paper presents overviews the capabilities of capillary electrophoretic techniques to determine low molecular mass organic acids in a variety of aqueous, gas and solid samples. It mainly focuses on short - chain carboxylic acids containing one or more carboxylic groups and possibly some other functional groups (hydroxyl, keto-, amino- etc.). Finally the procedures applied to the determine the acids in different matrices are...
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Occurrence and Determination of Volatile Fatty Acids in Landfill Leachate and Gas
PublicationIn landfills containing biological matter volatile fatty acids (VFAs) are generated at high rate at the early stage of waste disposal and their content in leachate is high as compared to the leachate from old parts of landfill since they are converted to methane gas. Monitoring of the leachate for the content of VFAs can help determine the processes occurring in waste and possible effect of the leachate on the environment in the...
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Occurrence and Determination of Volatile Fatty Acids in Landfill Leachate and Gas
PublicationIn landfills containing biological matter volatile fatty acids (VFAs) are generated at high rate at the early stage of waste disposal and their content in leachate is high as compared to the leachate from old parts of landfill since they are converted to methane gas. Monitoring of the leachate for the content of VFAs can help determine the processes occurring in waste and possible effect of the leachate on the environment in the...
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Green Analytical Chemistry in Determination of Volatile Fatty Acids in Wastewater
PublicationCharakterystyka metodyk oznaczania lotnych kwasów tłuszczowych w próbkach wodnych, opierających się na Zasadach Zielonej Chemii. Opis zastosowania techniki bezpośredniego dozowania próbki wodnej do chromatografu gazowego, techniki analizy fazy nadpowierzchniowej oraz techniki mikroestrakcji do fazy stacjonarnej.
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Hydrogen and chalcogen bonds in crystals of chalcogenadiazolecarboxylic acids – competition or cooperation?
PublicationThis article presents crystal structures of chalcogenadiazolecarboxylic acids bearing both a hydrogen and a chalcogen bond donor. The selected molecules varied in the size of the aromatic unit, the chalcogen atom and/or the position of the carboxyl group in the core structure. The most common synthons in their lattice are "R" _"2" ^"2" (8) self-complementary acid dimers or four-membered [Ch···N]2 rings. Supramolecular synthons...
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Composition of fatty acids in selected sorts of biscuits, offered for children
PublicationThe fatty acid (FA) composition, especially total trans-fatty acids (TFA) content in 12 assortments of biscuits offered for children, produced by four different companies, were determined by gas chromatography. Total fat content of the biscuit samples ranged from 2.2 to 22.8 g/100 g of product. The major FAs were palmitic C16:0, oleic C18:1, and linoleic C18:2 acids. Depending on the biscuit type, the total saturated fatty acids...
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The Role of Electron Transfer in the Fragmentation of Phenyl and Cyclohexyl Boronic Acids
PublicationIn this study, novel measurements of negative ion formation in neutral potassium-neutral boronic acid collisions are reported in electron transfer experiments. The fragmentation pattern of phenylboronic acid is comprehensively investigated for a wide range of collision energies, i.e., from 10 to 1000 eV in the laboratory frame, allowing some of the most relevant dissociation channels to be probed. These studies were performed in...
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Determination and identification of organic acids in wine samples. Problems and challenges.
PublicationFor long time, organic acids were underestimated. However, during last two decades there is an increasing interest of natural compounds having antioxidant, antimicrobial and anti-inflammatory properties thus organic acids are very preferable. Wine stands as one of the sources of organic acids since they are responsible for its organoleptic and aestethic character. Nevertheless, it is important to not exceed acceptable level of...