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Search results for: KALORYMETRIA DSC
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Efficient optimization approaches for microwave assisted extraction of high-quality antioxidant compounds from Salvia officinalis L.: UHPLC-HRMS differential analysis of phenolic profiles obtained by ultrasound and microwave extraction
PublicationThe study aims to optimize MAE of total phenolic compounds (TPC) and antioxidant capacity from Salvia officinalis L. leaves using a definitive screening design (DSD) and I-optimal design. UHPLC-HRMS analysis was used to identify and compare the composition of MAE and UAE optimal extracts. The results showed that DSD and I-optimal design were successfully applied for the optimization of MAE targeting phenolics and other antioxidants...
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Comparison of hydrochemistry and organic compound transport in two non-glaciated high Arctic catchments with a permafrost regime (Bellsund Fjord, Spitsbergen)
PublicationAn increase in air temperature related to climate change results in the retreat of glaciers, the degradation of permafrost, and the expansion of glacier-free areas in the polar regions. All these processes lead to changes in the Arctic landscape. They influence the hydrochemistry of streams and rivers fed by glaciers and thawing permafrost. In this study, we examine eighty two water samples from two non-glaciated catchments with...
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Measurements and calculations of the width of the fracture process zones on the surface of notched concrete beams
PublicationArtykuł omawia wyniki pomiaru i analizy numerycznej szerokości strefy pękania w belkach betonowych z nacięciem. Do pomiarów zastosowano metodę DIC. Do symulacji zastosowano model sprężysto - plastyczny i model z degradacją sztywności. Oba modele zostały rozszerzone o nielokalne osłabienie. Wyniki symulacji porównano z doświadczeniami.
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Stanisław Barański
PeopleStanisław Barański received BSc in 2019 and MSc in 2020 in informatics at Gdańsk University of Technology. Currently, he is a PhD candidate at the Department of Computer Architecture, Faculty of Electronics, Telecommunications and Informatics, Gdansk University of Technology. His research interests include blockchains and cryptography, especially the issue of blockchain-based internet voting and mitigation of content poisoning...
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AutoCAD - DC Edukacja
e-Learning CoursesAutoCAD DC Edukacja
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Charakterystyka frakcji oleju palmowego otrzymanych na drodze wielostopniowej krystalizacji
PublicationPrzeprowadzono wielostopniową frakcjonowaną krystalizację oleju palmowego z acetonu. Stosując temperatury krystalizacji od 25 do 0C, otrzymano siedem frakcji znacznie różniących się budową chemiczną i właściwościami fizycznymi. We frakcjach oznaczono skład kwasów tłuszczowych metodą GLC oraz zawartość triacylogliceroli metodą HPLC. Zbadano też właściwości fizyczne otrzymanych frakcji. Oznaczono zawartości fazy stałej metodą pulsacyjnego...
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Towards sugar-derived polyamides as environmentally friendly materials
PublicationAs part of our ongoing study investigating isohexide-based polyamides, we have synthesized isosorbide(bis(propan-1-amine)) (DAPIS) and studied its reactivity in the polymerization towards fully biobased polyamides. Polycondensation of nylon salts with various contributions of DAPIS afforded a family of homo- and copolyamides, which were characterized using complementary spectroscopic techniques. The chemical structure of the materials...
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Cure Index demonstrates curing of epoxy composites containing silica nanoparticles of variable morphology and porosity
PublicationAn image was taken by Cure Index on curability of epoxy with silica nanoparticles having variable morphology and porosity. Three kinds of silica nanoparticles with non-porous curved-rod, non-porous spherical, and mesoporous spherical microstructures were synthesized and characterized by Fourier-transform infrared spectroscopy, scanning electron microscopy (SEM) and Brunauer–Emmett–Teller analyses. Epoxy nanocomposites containing...
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The Physicochemical and Antibacterial Properties of Chitosan-Based Materials Modified with Phenolic Acids Irradiated by UVC Light
PublicationThis paper concerns the physicochemical properties of chitosan/phenolic acid thin films irradiated by ultraviolet radiation with wavelengths between 200 and 290 nm (UVC) light. We investigated the preparation and characterization of thin films based on chitosan (CTS) with tannic (TA), caffeic (CA) and ferulic acid (FA) addition as potential food‐packaging materials. Such materials were then exposed to the UVC light (254 nm) for...
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Impedimetric sensing of α-amino acids driven by micro-patterned 1,8-Diazafluoren-9-one into titania- boron- doped maze-like nanocarbons
PublicationThe development of impedimetric, non-faradaic label-free sensors for the detection of α-amino acids constitutes a trailblazing technology for the fast and inexpensive quantification of such biomarkers. Since α-amino acids, such as glycine and sarcosine, are basic constituents in biological processes, a variation in their concentration may be an indicator of cardiovascular diseases and metabolic disorders or neurological conditions....
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Rate performance of the V2O5 nanocrystals as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanocrystals obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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Cyclic voltammetry curves of the V2O5 nanorods (Li-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanocrystals obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Li/Li+ at a scan rate of 1 mV/s. The results show that in the subsequent cycles,...
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Cyclic voltammetry curves of the V2O5 nanocrystals (Li-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanocrystals obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Li/Li+ at a scan rate of 1 mV/s. The results show that in the subsequent cycles,...
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Rate performance of the V2O5 nanorods as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanorods obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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Static analysis of thin-walled beams and frames with stiffeners.
PublicationPraca zawiera pełną treść referatu wygłoszonego na Konferencji w Wilnie.Referat przedstawia problem numerycznej analizy belek i ramstalowych zbudowanych z bi-symetrycznych profili cienkościennychze stężeniami. Wyniki analizy przeprowadzonej według koncepcji superelementu jednowymiarowego porównano z wynikami obliczeń przy zastosowaniu gęstej siatki elementów powłokowych QUAD4 programu MSC NASTRAN.
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Periodic stick-slip deformation of granular material under quasi-static conditions
PublicationArtykuł omawia wyniki porównawcze między doświadczeniami z użyciem metody korelacji obrazów cyfrowych (DIC) a symulacjami z użyciem metody elementów dyskretnych (DEM) dla problemu przesuwającej się sztywnej ścianki w piasku. W doświadczeniach zaobserwowano w piasku deformację typu slip-stick, która nie została odtworzona w obliczeniach DEM..
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Właściwości elektryczne i magnetyczne szkła Fe2O3 – SiO2 – PbO
PublicationSzkło Fe2O3–SiO2–PbO wydaje się być obiecującym materiałem do zastosowań w urządzeniach elektrycznych takich jak rdzenie cewek, czujniki pola magnetycznego oraz mikrotransformatory. Jest to spowodowane korzystnymi właściwościami takimi jak stosunkowo wysoka rezystywność oraz w miarę duża przenikalność magnetyczna. Pierwsza wymieniona cecha skutkuje brakiem strat energii na prądy wirowe. Natomiast druga cecha oznacza potencjalną...
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Electrochemical cell impedance spectra at Eoc+100mV
Open Research DataThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc+200mV
Open Research DataThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc-100mV
Open Research DataThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc
Open Research DataThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Electrochemical cell impedance spectra at Eoc-200mV
Open Research DataThe dataset presents impedance spectrum of electrochemical cell filled with 3% NaCl solution presented in the figure below. This cell was used measured using Atlas-Sollich 0531 impedance analyser with built-in potentiostat. When changing the DC polarisation of the cell the non-linear phenomena could be observed. The impedance spectrum frequency range...
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Broken Rotor Symptons in the Sensorless Control of Induction Machine
PublicationInverter fed sensorless controlled variable speed drives with induction machine are widely used in the industry applications, also in wind power generation and electric vehicles. On-line self diagnostic systems implementation is needed for early stage fault detection and avoiding a critical fault. Diagnostic algorithms in modern DSP-based controllers can operate simultaneously with control system functions. In the closed-loop controlled...
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Investigating BiMeVOx compounds as potential photoelectrochemical and electrochemical materials for renewable hydrogen production
PublicationIn this study, BiMeVOx compounds (where Me: Co, Mo, Ce, Zr) were synthesized and characterized as potential photoelectrochemical materials for solar water splitting, the hydrogen evolution reaction (HER), and oxygen evolution reaction (OER). The analysis confirmed the successful formation of phase BiMeVOx compounds with the desired crystal structure. Among the tested materials, BiCoVOx(800) showed the highest photocurrent density...
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Rafał Hein dr hab. inż.
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Przekształtniki dwukierunkowe ze zwrotem energii do sieci
PublicationW artykule przedstawiono stanowisko eksperymentalne oraz badania porównawcze napędu jednokierunkowego i dwukierunkowego z silnikami indukcyjnymi o mocy 22kW. Następnie przedstawiono wyniki wdrożenia napędu dwukierunkowego w Spółdzielni Mleczarskiej "Maćkowy" w Gdańsku, gdzie napęd dwukierunkowy wykorzystano przy modernizacji wirówki do produkcji twarogu DSC1 z silnikiem o mocy 18,5kW.
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Przekształtniki dwukierunkowe ze zwrotem energii do sieci
PublicationW artykule przedstawiono stanowisko eksperymentalne oraz badania porównawcze napędu jednokierunkowego i dwukierunkowego z silnikami indukcyjnymi o mocy 22kW. Następnie przedstawiono wyniki wdrożenia napędu dwukierunkowego w Spółdzielni Mleczarskiej "Maćkowy" w Gdańsku, gdzie napęd dwukierunkowy wykorzystano przy modernizacji wirówki do produkcji twarogu DSC1 z silnikiem o mocy 18,5kW.
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Fruit Pomace as a Component Shaping the Content of Bioactive Compounds and Nutritional, Health-Promoting (Anti-Diabetic and Antioxidant) of Shortcrust Pastries Sweetened with Sucrose and Erythritol
Open Research DataIn this study, an attempt was made to develop shortcrust pastries containing different amounts of chokeberry, apple and blackcurrant pomace (0%, 10%, 30%, 50%), modulating their degree of sweetness via the application of sucrose or erythritol. The obtained products were assessed for their nutritional value (energy value, protein, fats, dietary fibre,...
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Dual drive control under SVPWM, experimental results
Open Research DataThe dataset contains the experimental results of the project: A universal algorithm of space vector pulse width modulation for three-level three and multi-phase NPC inverters with DC-link voltage balancing. The analysis includes the behaviour of the drive system, examining the dynamic system response to speed and angle changes, and encompassing data...
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Diamine derivatives of dimerized fatty acids and bio-based polyether polyol as sustainable platforms for the synthesis of non-isocyanate polyurethanes
PublicationA series of environmentally friendly non-isocyanate polyurethanes (NIPUs) were successfully prepared via the polyaddition reaction of bio-based polyether polyol-based cyclic carbonate with diamine derivative of dimerized fatty acids. The syntheses of NIPUs were realized by the three-step method in the absence of toxic solvents and, importantly, the process of carbonation did not require the use of elevated pressure. The effect...
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Structure and Molecular Dynamics in Renewable Polyamides from Dideoxy-Diamino Isohexide
PublicationThe chemical structure, the conformation, andthe flexibility of the polymer chain fragments present in thepolyamides synthesized from 2,5-diamino-2,5-dideoxy-1,4;3,6-dianhydrosorbitol, 1,4-diaminobutane, and either sebacic orbrassylic acid have been studied by liquid-state 2D NMRspectroscopy viz. correlation spectra (COSY) and heteronuclearmultiple-bond correlation spectra (gHMBC), by 13Ccross-polarization/magic-angle spinning...
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Synthesis and characterisation of polyurethane elastomers with semi-products obtained from polyurethane recycling
PublicationIn this work polyurethane elastomers were synthesised by using different mixtures of a petrochemical and glycerolysate polyols and 4,4-diphenylmethane diisocyanate (MDI). Glycerolysate polyol was produced from polyurethane foam decomposition using crude glycerine as a decomposition agent. The structure and thermal properties of obtained semi-product were similar to the polyol used in the synthesis of original foam. Glycerolysate...
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Wpływ kolejności dozowania surowców oraz sił ścinających na właściwości mieszanin polietylen dużej gęstości/miał gumowy, wytwarzanych przy użyciu współbieżnej wytłaczarki dwuślimakowej
PublicationKompozycje termoplastyczne polietylenu dużej gęstości (PE-HD) z udziałem 50 % mas. miału gumowego (GTR), wytwarzano przy użyciu współbieżnej wytłaczarki dwuślimakowej. Scharakteryzowano wpływ kolejności dozowania surowców oraz sił ścinających generowanych podczas intensywnego mieszania na parametry pracy wytłaczarki, wartości masowego wskaźnika szybkości płynięcia, statyczne właściwości mechaniczne (wytrzymałość na rozciąganie,...
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Water Solubilization Using Nonionic Surfactants from Renewable Sources in Microemulsion Systems
PublicationIn this study the effect of temperature, NaCl andoils (hydrocarbons: C8-C16) on the formation and solubilizationcapacity of the systems of oil/monoacylglycerols(MAG):ethoxylated fatty alcohols (CEO20)/propylene glycol(PG)/water was investigated. The effects of the surfactantmixture on the phase behavior and the concentration ofwater or oil in the systems were studied at three temperatures(50, 55, 60 C) and with varied NaCl solutions...
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Curing epoxy with ethylenediaminetetraacetic acid (EDTA) surface-functionalized Co Fe3-O4 magnetic nanoparticles
PublicationIn this work, the bulk and surface composition of Fe3O4 supermagnetic nanoparticles were modified for efficient epoxy curing. The bare, ethylenediaminetetraacetic acid (EDTA) capped, and cobalt (Co)-doped EDTA capped Fe3O4 nanoparticles were synthesized electrochemically. The crystalline structure and phase information, surface capping, morphology and magnetization behavior of nanoparticles were studied by X-Ray diffraction (XRD),...
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Surface active fatty acid ILs: Influence of the hydrophobic tail and/or theimidazolium hydroxyl functionalization on aggregates formation
PublicationNine structurally-related fatty acid ionic liquids have been prepared and their thermal behavior as well as their ability to self-assemble in water has been investigated. The thermal properties were studied by thermal gravimetric analysis (TGA) and differential scanning calorimetry (DSC), while the aggregation behavior was analyzed by tensiometry, isothermal titration calorimetry (ITC), conductometry, dynamic light scattering (DLS),...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublicationA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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From Structure to Luminescent Properties of B2O3-Bi2O3-SrF2 Glass and Glass-Ceramics Doped with Eu3+ Ions
PublicationGlass-ceramics with the composition B2O3 -Bi2O3 -SrF2 were synthesized by the conventional melt-quenching technique and subsequent crystallization of the parental glasses. The temperature at which the ceramization was carried out was selected based on differential scanning calorimetry (DSC) analysis. The structure of the studied materials and the formation of SrF2 nanocrystals were confirmed by the Fourier-transform infrared spectroscopy...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublicationA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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Investigation on Filaments for 3D Printing of Nasal Septum Cartilage Implant
PublicationSeptoplasty is a widely used method in treating deviated septum. Although it is successfully implemented, there are problems with excessive bleeding, septal perforation, or infections. The use of anatomically shaped implants could help overcome these problems. This paper focuses on assessing the possibility of the usage of a nasal septum cartilage implant 3D printed from various market-available filaments. Five different types...
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CAD. Integrated Architectural Design, MSc Arch (2022/2023)
e-Learning CoursesThe programme will provide students with a solid grounding in BIM (Building Information Modelling) using Autodesks Revit Architecture. Students will review the advanced features of Revit for Architecture, a tool to support BIM (Building Information Modelling) and delivery of 3D digital models and related documentation. The lesson plans will specifically introduce students to common workflows and problem-solving skills while creating...
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Elective Project I ENG sem. MSc (23/24)
e-Learning CoursesThe elective project I class is dedicated to daylight analysis within the built environment.
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Construction Project (BSc, sem. VI, spring/summer 2024)
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Diploma consultations (BSc, sem. VIII, spring/summer 2024)
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CAD Integrated Architectural Design, MSc Arch (2023-24)
e-Learning CoursesDetailed understanding of optimizing the design process using parametric BIM (Building Information Modeling) in the Autodesk Revit Architecture program. Practical design exercises included familiarize students with methods of integrating parametric design and exchanging data with other CAD/BIM programs, modifying parametric objects and generating automatic 2D/3D architectural documentation. The lesson plan introduces students to...
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CAD. Integrated Architectural Design, BSc Arch (2023-24)
e-Learning CoursesThe programme will provide students with a solid grounding in BIM (Building Information Modelling) using Autodesks Revit Architecture. Students will review the advanced features of Revit for Architecture, a tool to support BIM (Building Information Modelling) and delivery of 3D digital models and related documentation. The lesson plans will specifically introduce students to common workflows and problem-solving skills while creating...
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Understanding the Dominant Physics Mechanisms on the p-i-n Perovskite Solar Cells Fabricated by Scalable Slot-Die Coating Process in Ambient Air
PublicationPerovskite solar cells (PSC) are emerging technologies that have shown continuous improvement in power conversion efficiency (PCE) and stability. However, a very important aspect that has been seldom considered is the reproducibility of PCE of PSC devices. It is possible to achieve PCE from 10.21% to 17.05% using scalable slot-die-coating technique. However, a spatial distribution of performance is clearly observed for device samples...
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Antibacterial Activity and Cytocompatibility of Bone Cement Enriched with Antibiotic, Nanosilver, and Nanocopper for Bone Regeneration
PublicationBacterial infections due to bone replacement surgeries require modifications of bone cement with antibacterial components. This study aimed to investigate whether the incorporation of gentamicin or nanometals into bone cement may reduce and to what extent bacterial growth without the loss of overall cytocompatibility and adverse effects in vitro. The bone cement Cemex was used as the base material, modified either with gentamicin...
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1 kapitola: Status report on frame sawing machines for narrow-kerf sawing
PublicationW opracowaniu przedstawiono genezę pilarek ramowych oraz przecinania drewna cienkimi piłami. Omówiono ekonomiczne i ekologiczne zalety tego typu obróbki. Zaprezentowano kinematykę współczesnych pilarek dostępnych na rynkach światowych: Orbit, Mamuth oraz DSG Sonic. Szczegółowo opisano układ napędowy pilarek DTPX-30 i PRW15 z hybrydowym napędem głównym i całkowitym wyrównoważeniem dynamicznym układu.
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Analiza stateczności walcowego pionowego zbiornika dwupłaszczowego posadowionego na fundamencie gruntowym
PublicationOmówiono wpływ nierównomiernego osiadania płaszcza wewnętrznego i zewnętrznego na nośność stalowego zbiornika dwupłaszczowego posadowionego za pośrednictwem podsypki piaskowej na uwarstwionym podłożu gruntowym. Analizę obliczeniową wykonano numerycznie przy zastosowaniu systemu komputerowego MSC Visual Nastran for Windows, version 2001. Stwierdzono, że przy zastosowaniu w obliczeniach podłoża typu Winklera otrzymuje się zbyt duże...